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Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen

Manufacturer Supply High Quality 5-Methoxyindole

Cas:1006-94-6

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Trading Company

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

5-Methoxyindole Manufacturer/High quality/Best price/In stock

Cas:1006-94-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Wuhan Fortuna Chemical Co.,Ltd

Unique advantages of 5-Methoxyindole Cas 1006-94-6 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Off-white crystalline powder Storage:Cool dry place Package:1kg/foil b

Top quality 5-Methoxyindole Cas 1006-94-6 with reasonable price and fast delivery

Cas:1006-94-6

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Chemwill Asia Co., Ltd.

5-Methoxyindole CAS 1006-94-6 Indol-5-yl methyl ether CAS no 1006-94-6 5-methoxy-1H-indole 5-Methoxyindole Manufacturer High quality Best price In stock factory CAS 1006-94-6 5-Methoxyindole COA TDS price MSDS highly quality and immedaite d

5-Methoxyindole CAS 1006-94-6 Indol-5-yl methyl ether CAS no 1006-94-6 5-methoxy-1H-indole

Cas:1006-94-6

Min.Order:5 Kiloliter

FOB Price: $3.5 / 5.0

Type:Manufacturers

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Leader Biochemical Group

About Product Details

China Biggest factory Manufacturer Supply High Quality 5-Methoxyindole CAS 1006-94-6

Cas:1006-94-6

Min.Order:1 Kilogram

FOB Price: $1.0 / 5.0

Type:Lab/Research institutions

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LIDE PHARMACEUTICALS LIMITED

LIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.

5-Methoxyindole

Cas:1006-94-6

Min.Order:1 Kilogram

FOB Price: $0.9 / 1.0

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

5-Methoxyindole Basic information Product Name: 5-Methoxyindole Synonyms: 5-METHOXYINDOLE;AKOS JY2082918;5-METHOXY-1H-INDOLE;RARECHEM AH BS 0117;TIMTEC-BB SBB004094;1H-Indol-5-yl methyl

5-Methoxyindole 1006-94-6

Cas:1006-94-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

5-Methoxyindole

Cas:1006-94-6

Min.Order:1 Kilogram

FOB Price: $100.0 / 150.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 1006-94-6 with best quality

Cas:1006-94-6

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name: 5-Methoxyindole Synonyms: 5-METHOXYINDOLE;AKOS JY2082918;5-METHOXY-1H-INDOLE;RARECHEM AH BS 0117;TIMTEC-BB SBB004094;1H-Indol-5-yl methyl ether;5-methoxy-indol;Femedol CAS:

5-Methoxyindole CAS: 1006-94-6

Cas:1006-94-6

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Hangzhou Sartort Biopharma Co., Ltd

Appearance:Yellowish crystalline powder Storage:R.T Package:5kg/drum Application:Pharma intermediate Transportation:Express/Sea/Air Port:Any port in China

5-Methoxyindole cas 1006-94-6

Cas:1006-94-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Langyou International Trading Co., Ltd

1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:Powder Storage:Store in sealed containers at cool & dry pla

5-Methoxyindole CAS:1006-94-6

Cas:1006-94-6

Min.Order:100 Gram

Negotiable

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

5-Methoxyindole 1006-94-6

Cas:1006-94-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Pharmaceutical Intermediate, 5-Methoxyindole CAS:1006-94-6

Cas:1006-94-6

Min.Order:1 Kilogram

FOB Price: $148.0 / 156.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

5-Methoxyindole CAS:1006-94-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia

5-Methoxyindole CAS:1006-94-6

Cas:1006-94-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

5-Methoxyindole

Cas:1006-94-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

5-Methoxyindole

Cas:1006-94-6

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures

5-Methoxyindole

Cas:1006-94-6

Min.Order:1 Kilogram

FOB Price: $35.0 / 50.0

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

5-Methoxyindole

Cas:1006-94-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

5-Methoxyindole

Cas:1006-94-6

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

5-METHOXYINDOLE

Cas:1006-94-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

5-methoxyindole

Cas:1006-94-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Miheng Trading Co., Ltd.

5-Methoxyindole CAS 1006-94-6 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to assembly.

5-Methoxyindole CAS 1006-94-6

Cas:1006-94-6

Min.Order:1 Kilogram

FOB Price: $50.0 / 100.0

Type:Trading Company

inquiry

Hefei Zhaobo Technology Co., Ltd.

5-Methoxyindole CAS 1006-94-6 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality control s

5-Methoxyindole CAS 1006-94-6

Cas:1006-94-6

Min.Order:1 Kilogram

FOB Price: $10.0 / 50.0

Type:Trading Company

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

5-Methoxyindole

Cas:1006-94-6

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 5-Methoxyindole

Cas:1006-94-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

5-Methoxyindole

Cas:1006-94-6

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: 5-Methoxyindole CAS No.:1006-94-6 Molecule Formula:C9H9NO Molecule Weight:147.17 Purity: 98.0% Package: 25kg/drum Description:White to light yellow crystalline powder Manufacture Standards:Enterprise Standard

High Quality 5-Methoxyindole

Cas:1006-94-6

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

5-Methoxyindole

Cas:1006-94-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

5-Methoxyindole

Cas:1006-94-6

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Synthetic route

5-methoxy-N-(4-toluenesulfonyl)-1H-indole
139717-71-8

5-methoxy-N-(4-toluenesulfonyl)-1H-indole

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl acetamide at 60℃; for 5h; Inert atmosphere;90%
With formic acid; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 24h; Inert atmosphere; Sealed tube; Irradiation;85%
With caesium carbonate In tetrahydrofuran; methanol at 64℃; for 2.5h;
With cetyltrimethylammonim bromide; potassium hydroxide In tetrahydrofuran; water for 120h; Reflux; Green chemistry;
5-methoxyindole-3-carboxaldehyde
10601-19-1

5-methoxyindole-3-carboxaldehyde

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With palladium diacetate; potassium carbonate In ethyl acetate at 150℃; under 12929 Torr; for 0.833333h; Microwave irradiation; Molecular sieve;90%
With perchloric acid adsorbed on silica gel; anthranilic acid amide In acetonitrile at 80℃; for 6h;74%
5-Methoxyindole-3-carboxylic acid
10242-01-0

5-Methoxyindole-3-carboxylic acid

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With potassium carbonate In ethanol at 140℃; Schlenk technique;99%
4-methoxy-trans-2-[β-(dimethylamino)vinyl]-nitrobenzene
32989-62-1

4-methoxy-trans-2-[β-(dimethylamino)vinyl]-nitrobenzene

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In benzene at 25℃; under 2280 Torr; for 27h;68%
palladium In benzene
1-(5-methoxy-1H-indol-1-yl)-2,2-dimethylpropan-1-one
845619-77-4

1-(5-methoxy-1H-indol-1-yl)-2,2-dimethylpropan-1-one

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With water; 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran for 18h; Reflux;99%
With lithium diisopropyl amide In tetrahydrofuran; hexane at 40 - 45℃; for 2h;92%
2-vinyl-4-methoxynitrobenzene
126759-31-7

2-vinyl-4-methoxynitrobenzene

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With carbon monoxide; triphenylphosphine; palladium diacetate In acetonitrile under 3040 Torr; for 19h; Heating;63%
Multi-step reaction with 2 steps
1: 50 percent / O2 (1 atm) / Na2PdCl4 / methanol / 24 h / Ambient temperature
2: 63 percent / Fe, acetic acid, 10percent HCl / ethanol / Temp. 70 - 75 deg C, 1 h. Temp. 85 deg C, 2 h
View Scheme
Multi-step reaction with 2 steps
1: 85 percent / oxygen / palladium(II) chloride, copper(I) chloride / 1,2-dimethoxy-ethane / 24 h / 50 - 60 °C
2: 1.) H2, 2.) aq. HCl / 10percent rhodium-carbon / 1.) ethanol, room temperature, 1 atmosphere, 3 h, 2.) room temperature, 3 h
View Scheme
5-methoxy-2-nitro-benzaldehyde
20357-24-8

5-methoxy-2-nitro-benzaldehyde

(tert-Butoxycarbonylmethylene)triphenylphosphorane
86302-43-4

(tert-Butoxycarbonylmethylene)triphenylphosphorane

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With triphenylphosphine In diphenylether at 260℃; for 1h;51%
5-methoxy-2-nitro-β-dimethylaminostyrene

5-methoxy-2-nitro-β-dimethylaminostyrene

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With hydrogen In N,N-dimethyl-formamide at 330 - 340℃; under 15001.5 Torr; for 10h; Pressure; Temperature;
2-(5-methoxy-2-nitrophenyl)acetonitrile
89302-15-8

2-(5-methoxy-2-nitrophenyl)acetonitrile

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With hydrogen In methanol at 20℃; under 760.051 Torr; for 12h;88%
With hydrogen; acetic acid; 10% palladium on active carbon In ethanol under 2280 Torr; for 2h; Ambient temperature;83%
With hydrogen at 20℃; under 760.051 Torr; for 24h; Schlenk technique;68%
5-bromo-1H-indole
10075-50-0

5-bromo-1H-indole

sodium methylate
124-41-4

sodium methylate

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With copper(l) iodide In N,N-dimethyl-formamide for 6h; Reflux;98%
(E)-5-methoxy-2-nitro-β-morpholinestyrene
107127-61-7

(E)-5-methoxy-2-nitro-β-morpholinestyrene

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In benzene at 50℃; under 4560 Torr; for 8h;72%
1-(tert-butyloxycarbonyl)-5-methoxyindole
99275-47-5

1-(tert-butyloxycarbonyl)-5-methoxyindole

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
In various solvent(s) at 150℃; for 0.25h; microwave irradiation;98%
With 1,1,1,3',3',3'-hexafluoro-propanol at 150℃; for 0.25h; Product distribution / selectivity; Microwave irradiation;98%
With 1,1,1,3',3',3'-hexafluoro-propanol at 150℃; for 0.25h; Product distribution / selectivity; Microwave irradiation;98%
triethanolamine hydrochloride
637-39-8

triethanolamine hydrochloride

4-methoxy-aniline
104-94-9

4-methoxy-aniline

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With tin(ll) chloride; dihydridotetrakis(triphenylphosphine)ruthenium In 1,4-dioxane; water at 180℃; for 20h;80%
With triphenylphosphine; tin(ll) chloride; ruthenium trichloride In 1,4-dioxane; water at 180℃; for 20h; Cyclization;43%
5-methoxyindoline
21857-45-4

5-methoxyindoline

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With H8O20P8Pt2(4-)*4C34H72N(1+) In methanol Inert atmosphere; Irradiation;99%
With 6C44H32N6O4Ru(2+)*12Hf(2+)*8O(2-)*14HO(1-)*6C16H22ClCoN5O6(1-) In 2,2,2-trifluoroethanol; acetonitrile at 20℃; for 12h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Irradiation;96%
With C21H21ClIrNO2 In tetrahydrofuran; 2,2,2-trifluoroethanol for 20h; Inert atmosphere;95%
5-methoxy-1H-indole-2-carboxylic acid
4382-54-1

5-methoxy-1H-indole-2-carboxylic acid

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
In quinoline for 0.2h; microwave;100%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In sulfolane at 300℃; for 0.333333h; Inert atmosphere;87%
With quinoline; copper Heating;77%
With quinoline; copper oxide-chromium oxide at 200 - 210℃;
triethanolamine
102-71-6

triethanolamine

4-methoxy-aniline
104-94-9

4-methoxy-aniline

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With tin(ll) chloride; ruthenium trichloride; triphenylphosphine In 1,4-dioxane at 180℃; for 20h;33%
C19H23NO3

C19H23NO3

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With silica gel In 5,5-dimethyl-1,3-cyclohexadiene at 170℃; Retro Diels-Alder reaction; Inert atmosphere;97%
5-methoxy-1-[(2-nitrophenyl)methyl]-1H-indole
261762-11-2

5-methoxy-1-[(2-nitrophenyl)methyl]-1H-indole

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With hydrazine In 1,4-dioxane; water for 0.333333h; Inert atmosphere; UV-irradiation;30%
5-methoxyindoline
21857-45-4

5-methoxyindoline

nitrobenzene
98-95-3

nitrobenzene

A

5-methoxylindole
1006-94-6

5-methoxylindole

B

aniline
62-53-3

aniline

Conditions
ConditionsYield
With nickel-nitrogen-doped carbon framework In water at 145℃; for 18h; Inert atmosphere; Sealed tube; Green chemistry;A 68%
B 71%
5-methoxyindoline
21857-45-4

5-methoxyindoline

5-nitro-m-xylene
99-12-7

5-nitro-m-xylene

A

5-methoxylindole
1006-94-6

5-methoxylindole

B

3,5-dimethylaminoaniline
108-69-0

3,5-dimethylaminoaniline

Conditions
ConditionsYield
With nickel-nitrogen-doped carbon framework In water at 145℃; for 18h; Inert atmosphere; Sealed tube; Green chemistry;A 62%
B 61%
2-(2-amino-5-methoxyphenyl)ethyl alcohol
124043-85-2

2-(2-amino-5-methoxyphenyl)ethyl alcohol

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
tris(triphenylphosphine)ruthenium(II) chloride In toluene for 6h; Heating;94%
tris(triphenylphosphine)ruthenium(II) chloride In toluene for 6h; Rate constant; Heating;94%
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; potassium carbonate In toluene at 111℃; for 20h;68%
5-methoxy-2-nitrotoluene
5367-32-8

5-methoxy-2-nitrotoluene

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 2.89 g / 7 h / 148 - 150 °C
2: 72 percent / H2 / Pd/C / benzene / 8 h / 50 °C / 4560 Torr
View Scheme
Multi-step reaction with 5 steps
1: N-bromosuccinimide (NBS), azoisobutyronitrile (AIBN) / CCl4 / 3 h / Heating
2: toluene / 1.) 6 h, RT; 2.) 3 h, 100 deg C
3: 74 percent / 48percent HBr, Zn / ethanol / 2 h / Heating
4: 87 percent / 2.5 h / Heating
5: 82 percent / t-BuOK / toluene / 0.25 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: 4 h / 110 °C
2: TiCl3, 4M NH4OAc / acetone
View Scheme
2-chloro-5-methoxy-1H-indole
119730-01-7

2-chloro-5-methoxy-1H-indole

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In ethyl acetate Ambient temperature;93%
5-methoxyindoline
21857-45-4

5-methoxyindoline

2,6-dimethylnitrobenzene
81-20-9

2,6-dimethylnitrobenzene

A

5-methoxylindole
1006-94-6

5-methoxylindole

B

2,6-dimethylaniline
87-62-7

2,6-dimethylaniline

Conditions
ConditionsYield
With nickel-nitrogen-doped carbon framework In water at 145℃; for 18h; Inert atmosphere; Sealed tube; Green chemistry;A 40%
B 41%
1-[(E)-2-(5-methoxy-2-nitrophenyl)vinyl]pyrrolidine
61293-32-1

1-[(E)-2-(5-methoxy-2-nitrophenyl)vinyl]pyrrolidine

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With iron(III) chloride hexahydrate; pyrographite; hydrazine hydrate In ethanol at 75℃; for 5h;91%
1-(Methylsulfonyl)-5-methoxyindole
88131-62-8

1-(Methylsulfonyl)-5-methoxyindole

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With potassium hydroxide In methanol for 18h; Heating;91%
4-methoxyphenylhydrazine hydrochloride
19501-58-7

4-methoxyphenylhydrazine hydrochloride

acetaldehyde
75-07-0

acetaldehyde

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With phosphomolybdic acid In chloroform at 20 - 60℃; Fischer indole synthesis;88%
methanol
67-56-1

methanol

5-bromo-1H-indole
10075-50-0

5-bromo-1H-indole

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With 1,10-Phenanthroline; sodium methylate; copper(I) bromide at 120℃; for 10h; Time; Reagent/catalyst; Temperature;
ethyl 5-methoxy-1H-indole-2-carboxylate
4792-58-9

ethyl 5-methoxy-1H-indole-2-carboxylate

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) LiAlH4 / tetrahydrofuran / 0 °C / 1.) 15 min, 2.) 45 min
2: MnO2 / CH2Cl2 / 1 h / 25 °C
3: 95 percent / Rh(dppp)2Cl / 18 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: aq.-ethanolic KOH
2: quinoline; copper oxide-chromium oxide / 200 - 210 °C
View Scheme
Stage #1: ethyl 5-methoxy-1H-indole-2-carboxylate With sodium hydroxide In ethanol at 40℃;
Stage #2: With quinoline; copper at 250℃; for 0.416667h; Microwave irradiation;
(4-Methoxy-2-trimethylsilanylethynyl-phenyl)-carbamic acid tert-butyl ester
194869-21-1

(4-Methoxy-2-trimethylsilanylethynyl-phenyl)-carbamic acid tert-butyl ester

5-methoxylindole
1006-94-6

5-methoxylindole

Conditions
ConditionsYield
With potassium tert-butylate In tert-butyl alcohol for 17h; Heating;67%
5-methoxylindole
1006-94-6

5-methoxylindole

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

5-methoxyindole-3-carboxaldehyde
10601-19-1

5-methoxyindole-3-carboxaldehyde

Conditions
ConditionsYield
With trichlorophosphate at 0 - 20℃;100%
With sodium hydroxide; trichlorophosphate Vilsmeier-Haack reaction;98%
Stage #1: N,N-dimethyl-formamide With trichlorophosphate at 0℃; for 0.333333h;
Stage #2: 5-methoxylindole at 0 - 20℃; for 1.5h;
98%
5-methoxylindole
1006-94-6

5-methoxylindole

2,3-dicyano-5,6-dichloro-p-benzoquinone
84-58-2

2,3-dicyano-5,6-dichloro-p-benzoquinone

4,5-Dichloro-3-hydroxy-1-(5-methoxy-1H-indol-3-yl)-6-oxo-cyclohexa-2,4-diene-1,2-dicarbonitrile

4,5-Dichloro-3-hydroxy-1-(5-methoxy-1H-indol-3-yl)-6-oxo-cyclohexa-2,4-diene-1,2-dicarbonitrile

Conditions
ConditionsYield
In 1,4-dioxane for 2h; Ambient temperature;100%
In 1,4-dioxane at 20℃; for 0.5h;
5-methoxylindole
1006-94-6

5-methoxylindole

5-methoxyindoline
21857-45-4

5-methoxyindoline

Conditions
ConditionsYield
With sodium cyanoborohydride; acetic acid at 0 - 20℃; for 2h;100%
With platinum/carbon xerogel catalyst; hydrogen; toluene-4-sulfonic acid In water at 25℃; under 22502.3 Torr; for 3h; regioselective reaction;96%
With C26H29ClIrNO3; hydrogen In 2,2,2-trifluoroethanol at 20℃; under 760.051 Torr; for 3h;95%
5-methoxylindole
1006-94-6

5-methoxylindole

2-fluoropyridine
372-48-5

2-fluoropyridine

5-methoxy-1-(pyridine-2-yl)-1H-indole

5-methoxy-1-(pyridine-2-yl)-1H-indole

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 95 - 100℃; for 2h;100%
5-methoxylindole
1006-94-6

5-methoxylindole

di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

1-(tert-butyloxycarbonyl)-5-methoxyindole
99275-47-5

1-(tert-butyloxycarbonyl)-5-methoxyindole

Conditions
ConditionsYield
With dmap In tetrahydrofuran at 20℃; for 16h; Acylation;100%
With dmap; triethylamine In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran at 20℃; for 19h;99%
dmap In acetonitrile at 20℃;97%
5-methoxylindole
1006-94-6

5-methoxylindole

3,5-dimethylphenyl iodide
22445-41-6

3,5-dimethylphenyl iodide

2,3-dihydro-5-methoxy-1-(3,5-dimethylphenyl)-1H-indole
360045-08-5

2,3-dihydro-5-methoxy-1-(3,5-dimethylphenyl)-1H-indole

Conditions
ConditionsYield
With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane In 1,4-dioxane; dodecane at 110℃; for 24h;100%
5-methoxylindole
1006-94-6

5-methoxylindole

3,5-dimethylphenyl iodide
22445-41-6

3,5-dimethylphenyl iodide

(S,S)-1,2-diaminocyclohexane
21436-03-3

(S,S)-1,2-diaminocyclohexane

2,3-dihydro-5-methoxy-1-(3,5-dimethylphenyl)-1H-indole
360045-08-5

2,3-dihydro-5-methoxy-1-(3,5-dimethylphenyl)-1H-indole

Conditions
ConditionsYield
With potassium phosphate; CuI In 1,4-dioxane100%
5-methoxylindole
1006-94-6

5-methoxylindole

bromoacetic acid methyl ester
96-32-2

bromoacetic acid methyl ester

methyl 2-(5-methoxy-1H-indol-1-yl)acetate
885524-56-1

methyl 2-(5-methoxy-1H-indol-1-yl)acetate

Conditions
ConditionsYield
Stage #1: 5-methoxylindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.75h;
Stage #2: bromoacetic acid methyl ester In N,N-dimethyl-formamide; mineral oil at 20℃; for 15h;
100%
Stage #1: 5-methoxylindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.75h;
Stage #2: bromoacetic acid methyl ester In N,N-dimethyl-formamide; mineral oil at 20℃; for 15h;
100%
(E)-3-(4-methoxyphenyl)-1-(1-methyl-1H-imidazol-2-yl)prop-2-en-1-one
869789-68-4

(E)-3-(4-methoxyphenyl)-1-(1-methyl-1H-imidazol-2-yl)prop-2-en-1-one

5-methoxylindole
1006-94-6

5-methoxylindole

3-(5-methoxy-1H-indol-3-yl)-3-(4-methoxyphenyl)-1-(1-methyl-1H-imidazol-2-yl)propan-1-one
1242049-84-8

3-(5-methoxy-1H-indol-3-yl)-3-(4-methoxyphenyl)-1-(1-methyl-1H-imidazol-2-yl)propan-1-one

Conditions
ConditionsYield
With 4,4'-dimethyl-2,2'-bipyridines; copper(II) nitrate trihydrate In acetonitrile at 20℃; for 72h; Friedel-Crafts Alkylation; Inert atmosphere;100%
With 4,4'-dimethyl-2,2'-bipyridines; copper(II) nitrate trihydrate In acetonitrile at 20℃; for 72h; Friedel-Crafts Alkylation; Inert atmosphere;100%
With copper(II) nitrate trihydrate In aq. buffer at 20℃; for 72h; pH=6.5; Friedel-Crafts Alkylation;85%
With copper(II) nitrate trihydrate In aq. buffer at 20℃; for 72h; pH=6.5; Reagent/catalyst; Friedel-Crafts Alkylation; enantioselective reaction;85%
(E)-3-(4-chlorophenyl)-1-(1-methyl-1H-imidazol-2-yl)prop-2-en-1-one
869789-69-5

(E)-3-(4-chlorophenyl)-1-(1-methyl-1H-imidazol-2-yl)prop-2-en-1-one

5-methoxylindole
1006-94-6

5-methoxylindole

3-(4-chlorophenyl)-3-(5-methoxy-1H-indol-3-yl)-1-(1-methyl-1H-imidazol-2-yl)propan-1-one
1242049-82-6

3-(4-chlorophenyl)-3-(5-methoxy-1H-indol-3-yl)-1-(1-methyl-1H-imidazol-2-yl)propan-1-one

Conditions
ConditionsYield
With 4,4'-dimethyl-2,2'-bipyridines; copper(II) nitrate trihydrate In acetonitrile at 20℃; for 72h; Friedel-Crafts Alkylation; Inert atmosphere;100%
With 4,4'-dimethyl-2,2'-bipyridines; copper(II) nitrate trihydrate In acetonitrile at 20℃; for 72h; Catalytic behavior; Reagent/catalyst; Friedel-Crafts Alkylation; Inert atmosphere;100%
With 4,4'-dimethyl-2,2'-bipyridines; copper(II) nitrate trihydrate In acetonitrile at 20℃; for 72h; Friedel-Crafts Alkylation; Inert atmosphere;100%
5-methoxylindole
1006-94-6

5-methoxylindole

sodium 1-(tert-butoxycarbonyl) azetidine-3-sulfinate

sodium 1-(tert-butoxycarbonyl) azetidine-3-sulfinate

tert-butyl 3-((5-methoxy-1H-indol-2-yl)sulfonyl)azetidine-1-carboxylate

tert-butyl 3-((5-methoxy-1H-indol-2-yl)sulfonyl)azetidine-1-carboxylate

Conditions
ConditionsYield
With iodine In methanol at 20℃; for 24h; regioselective reaction;100%
5-methoxylindole
1006-94-6

5-methoxylindole

sodium 1-(tert-butoxycarbonyl) azetidine-3-sulfinate

sodium 1-(tert-butoxycarbonyl) azetidine-3-sulfinate

C17H22N2O3S

C17H22N2O3S

Conditions
ConditionsYield
With iodine; triphenylphosphine In ethanol at 70℃; for 24h; regioselective reaction;100%
5-methoxylindole
1006-94-6

5-methoxylindole

Benzeneselenol
645-96-5

Benzeneselenol

5-methoxy-3-(phenylselanyl)-1H-indole
1599461-87-6

5-methoxy-3-(phenylselanyl)-1H-indole

Conditions
ConditionsYield
With caesium carbonate In N,N-dimethyl-formamide at 27℃; for 0.5h;100%
5-methoxylindole
1006-94-6

5-methoxylindole

methyl iodide
74-88-4

methyl iodide

5-methoxy-N-methylindole
2521-13-3

5-methoxy-N-methylindole

Conditions
ConditionsYield
Stage #1: 5-methoxylindole With sodium hydride In acetonitrile at 0℃; for 0.5h;
Stage #2: methyl iodide In acetonitrile at 0 - 20℃; for 16h;
99%
Stage #1: 5-methoxylindole With Tris(3,6-dioxaheptyl)amine; potassium tert-butylate In benzene at 20℃; for 1h;
Stage #2: methyl iodide In benzene at 20℃; for 0.5h;
97%
With sodium hydroxide In dimethyl sulfoxide at 20℃;94%
5-methoxylindole
1006-94-6

5-methoxylindole

nitrostyrene
5153-67-3

nitrostyrene

5-methoxy-3-(2-nitro-1-phenylethyl)-1H-indole

5-methoxy-3-(2-nitro-1-phenylethyl)-1H-indole

Conditions
ConditionsYield
Stage #1: nitrostyrene With (S)-10,10'-bis[(S)-4-isopropyl-4,5-dihydrooxazol-2-yl]-9,9'-biphenanthrene; zinc(II) trifluoroacetate In diethyl ether at 20℃; for 0.25h; Inert atmosphere;
Stage #2: 5-methoxylindole In diethyl ether at 20℃; Friedel-Crafts alkylation; Inert atmosphere;
99%
With N,N'-bis(3,5-bis(trifluoromethyl)benzyl)-2-nitroethene-1,1-diamine In toluene at 20℃; for 24h; Michael Addition;99%
With [(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]methanesulfonic acid In water at 20℃; for 8h; Friedel-Crafts Alkylation; Green chemistry;94%
5-methoxylindole
1006-94-6

5-methoxylindole

ammonium thiocyanate
1147550-11-5

ammonium thiocyanate

3-thiocyanato-5-methoxy-1H-indole

3-thiocyanato-5-methoxy-1H-indole

Conditions
ConditionsYield
In acetonitrile at 20℃; for 3h; Electrochemical reaction; Inert atmosphere;99%
With Oxone In methanol at 20℃; for 0.35h;98%
With oxygen In tetrahydrofuran at 25℃; under 750.075 Torr; for 7h; Irradiation;98%
5-methoxylindole
1006-94-6

5-methoxylindole

benzyl bromide
100-39-0

benzyl bromide

1-benzyl-5-methoxyindole
16382-21-1

1-benzyl-5-methoxyindole

Conditions
ConditionsYield
Stage #1: 5-methoxylindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h;
Stage #2: benzyl bromide In N,N-dimethyl-formamide; mineral oil at 20℃;
99%
Stage #1: 5-methoxylindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere;
Stage #2: benzyl bromide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere;
97%
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; Inert atmosphere;94%
5-methoxylindole
1006-94-6

5-methoxylindole

ethyl-3,3,3-trifluoropyruvate
13081-18-0

ethyl-3,3,3-trifluoropyruvate

3,3,3-trifluoro-2-hydroxy-2-(5-methoxy-1H-indol-3-yl)-propionic acid ethyl ester

3,3,3-trifluoro-2-hydroxy-2-(5-methoxy-1H-indol-3-yl)-propionic acid ethyl ester

Conditions
ConditionsYield
With (SIr,RC)-[(η5-C5Me5)Ir{(R)-propane-1,2-diylbis(diphenylphosphane)}(H2O)][SbF6]2 In dichloromethane for 0.333333h; Friedel-Crafts Alkylation; Inert atmosphere; Schlenk technique; Optical yield = 71 %ee;99%
With K-10 montmorillonite In toluene at 60℃; for 0.0833333h; Friedel-Crafts hydroxyalkylation;97%
In 1,1,1,3,3-pentafluorobutane at 20℃; for 0.5h; Inert atmosphere;96%
5-methoxylindole
1006-94-6

5-methoxylindole

iodobenzene
591-50-4

iodobenzene

5-methoxy-2-phenylindole
5883-96-5

5-methoxy-2-phenylindole

Conditions
ConditionsYield
With norborn-2-ene; dichloro bis(acetonitrile) palladium(II); potassium carbonate In N,N-dimethyl acetamide; water at 70℃; regioselective reaction;99%
With potassium acetate; palladium diacetate; bis-diphenylphosphinomethane In water at 110℃; for 24h; regioselective reaction;79%
With bis(di-tert-butyl(4-dimethylaminophenyl)phosphine)dichloropalladium(II); tetrachlorophthalic anhydride; sodium hydroxide In ethanol; water at 80℃; for 24h; regioselective reaction;73%
With cesium acetate; palladium diacetate In N,N-dimethyl acetamide at 125℃; for 24h;64%
With norborn-2-ene; palladium diacetate; potassium carbonate In N,N-dimethyl acetamide; water at 70℃;
5-methoxylindole
1006-94-6

5-methoxylindole

(2-nitroethenyl)benzene
102-96-5

(2-nitroethenyl)benzene

5-methoxy-3-(2-nitro-1-phenylethyl)-1H-indole

5-methoxy-3-(2-nitro-1-phenylethyl)-1H-indole

Conditions
ConditionsYield
With di(naphthalen-1-yl)silanediol In dichloromethane at 23℃; for 48h; Inert atmosphere;99%
With 2,6-bis(2,2-dimethylpropionylamino)benzoic acid In chloroform at 40℃; for 24h; Friedel-Crafts Alkylation;99%
With 1,1,1,3',3',3'-hexafluoro-propanol at 20℃; for 2h; Friedel-Crafts Alkylation;96%
5-methoxylindole
1006-94-6

5-methoxylindole

2,2,2-trifluoro-1-methoxy-ethanol
431-46-9

2,2,2-trifluoro-1-methoxy-ethanol

3,4,5-Trimethoxyaniline
24313-88-0

3,4,5-Trimethoxyaniline

N-((R)-2,2,2-trifluoro-1-(5-methoxy-1H-indol-3-yl)ethyl)-3,4,5-trimethoxybenzenamine
1132829-45-8

N-((R)-2,2,2-trifluoro-1-(5-methoxy-1H-indol-3-yl)ethyl)-3,4,5-trimethoxybenzenamine

Conditions
ConditionsYield
With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In dichloromethane at 20℃; for 24h; Friedel Crafts aminoalkylation; Molecular sieve; optical yield given as %ee; enantioselective reaction;99%
5-methoxylindole
1006-94-6

5-methoxylindole

diethyl m-methylbenzylidenemalonate
15725-33-4

diethyl m-methylbenzylidenemalonate

ethyl 2-ethoxycarbonyl-3-[3-(5-methoxyindolyl)]-3-(m-methylphenyl)propanoate

ethyl 2-ethoxycarbonyl-3-[3-(5-methoxyindolyl)]-3-(m-methylphenyl)propanoate

Conditions
ConditionsYield
Stage #1: 5-methoxylindole With C45H52N4O4; scandium tris(trifluoromethanesulfonate) In tert-butyl alcohol at 35℃; for 1h; Inert atmosphere;
Stage #2: diethyl m-methylbenzylidenemalonate In diethyl ether at -20℃; for 118h; Friedel Crafts alkylation; Inert atmosphere; optical yield given as %ee; enantioselective reaction;
99%
5-methoxylindole
1006-94-6

5-methoxylindole

1,1,1-trifluoroacetophenone
434-45-7

1,1,1-trifluoroacetophenone

2,2,2-trifluoro-1-(5-methoxy-1H-indol-3-yl)-1-phenylethan-1-ol
1150561-10-6

2,2,2-trifluoro-1-(5-methoxy-1H-indol-3-yl)-1-phenylethan-1-ol

Conditions
ConditionsYield
With tetrabutyl phosphonium bromide; potassium carbonate In water at 20℃; for 12h; Reagent/catalyst; regioselective reaction;99%
With N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; water at 20℃; for 16h; Friedel-Crafts type alkylation;98%
With TMG In dichloromethane at 20℃;
With diphenyl hydrogen phosphate In dichloromethane at 0℃; for 20h; Friedel-Crafts Alkylation; Molecular sieve; Inert atmosphere; Sealed tube;
5-methoxylindole
1006-94-6

5-methoxylindole

1,1,1-trifluoroacetophenone
434-45-7

1,1,1-trifluoroacetophenone

(R)-2,2,2-trifluoro-1-(5-methoxy-1H-indol-3-yl)-1-phenylethanol
1160936-79-7

(R)-2,2,2-trifluoro-1-(5-methoxy-1H-indol-3-yl)-1-phenylethanol

Conditions
ConditionsYield
With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In dichloromethane at 25℃; for 48h; optical yield given as %ee; enantioselective reaction;99%

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