hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryUnique advantages of 5-Methoxyindole Cas 1006-94-6 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Off-white crystalline powder Storage:Cool dry place Package:1kg/foil b
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inquiry5-Methoxyindole CAS 1006-94-6 Indol-5-yl methyl ether CAS no 1006-94-6 5-methoxy-1H-indole 5-Methoxyindole Manufacturer High quality Best price In stock factory CAS 1006-94-6 5-Methoxyindole COA TDS price MSDS highly quality and immedaite d
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inquiryAbout Product Details
Cas:1006-94-6
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
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inquiry5-Methoxyindole Basic information Product Name: 5-Methoxyindole Synonyms: 5-METHOXYINDOLE;AKOS JY2082918;5-METHOXY-1H-INDOLE;RARECHEM AH BS 0117;TIMTEC-BB SBB004094;1H-Indol-5-yl methyl
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct Name: 5-Methoxyindole Synonyms: 5-METHOXYINDOLE;AKOS JY2082918;5-METHOXY-1H-INDOLE;RARECHEM AH BS 0117;TIMTEC-BB SBB004094;1H-Indol-5-yl methyl ether;5-methoxy-indol;Femedol CAS:
Cas:1006-94-6
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inquiryAppearance:Yellowish crystalline powder Storage:R.T Package:5kg/drum Application:Pharma intermediate Transportation:Express/Sea/Air Port:Any port in China
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:Powder Storage:Store in sealed containers at cool & dry pla
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
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inquiry5-Methoxyindole CAS:1006-94-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
5-Methoxyindole CAS 1006-94-6 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to assembly.
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inquiry5-Methoxyindole CAS 1006-94-6 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality control s
Cas:1006-94-6
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:1006-94-6
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:1006-94-6
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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inquiryProduct name: 5-Methoxyindole CAS No.:1006-94-6 Molecule Formula:C9H9NO Molecule Weight:147.17 Purity: 98.0% Package: 25kg/drum Description:White to light yellow crystalline powder Manufacture Standards:Enterprise Standard
Cas:1006-94-6
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
5-methoxy-N-(4-toluenesulfonyl)-1H-indole
5-methoxylindole
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl acetamide at 60℃; for 5h; Inert atmosphere; | 90% |
With formic acid; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; N-ethyl-N,N-diisopropylamine In acetonitrile at 20℃; for 24h; Inert atmosphere; Sealed tube; Irradiation; | 85% |
With caesium carbonate In tetrahydrofuran; methanol at 64℃; for 2.5h; | |
With cetyltrimethylammonim bromide; potassium hydroxide In tetrahydrofuran; water for 120h; Reflux; Green chemistry; |
5-methoxyindole-3-carboxaldehyde
5-methoxylindole
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate In ethyl acetate at 150℃; under 12929 Torr; for 0.833333h; Microwave irradiation; Molecular sieve; | 90% |
With perchloric acid adsorbed on silica gel; anthranilic acid amide In acetonitrile at 80℃; for 6h; | 74% |
5-Methoxyindole-3-carboxylic acid
5-methoxylindole
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 140℃; Schlenk technique; | 99% |
4-methoxy-trans-2-[β-(dimethylamino)vinyl]-nitrobenzene
5-methoxylindole
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In benzene at 25℃; under 2280 Torr; for 27h; | 68% |
palladium In benzene |
1-(5-methoxy-1H-indol-1-yl)-2,2-dimethylpropan-1-one
5-methoxylindole
Conditions | Yield |
---|---|
With water; 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran for 18h; Reflux; | 99% |
With lithium diisopropyl amide In tetrahydrofuran; hexane at 40 - 45℃; for 2h; | 92% |
2-vinyl-4-methoxynitrobenzene
5-methoxylindole
Conditions | Yield |
---|---|
With carbon monoxide; triphenylphosphine; palladium diacetate In acetonitrile under 3040 Torr; for 19h; Heating; | 63% |
Multi-step reaction with 2 steps 1: 50 percent / O2 (1 atm) / Na2PdCl4 / methanol / 24 h / Ambient temperature 2: 63 percent / Fe, acetic acid, 10percent HCl / ethanol / Temp. 70 - 75 deg C, 1 h. Temp. 85 deg C, 2 h View Scheme | |
Multi-step reaction with 2 steps 1: 85 percent / oxygen / palladium(II) chloride, copper(I) chloride / 1,2-dimethoxy-ethane / 24 h / 50 - 60 °C 2: 1.) H2, 2.) aq. HCl / 10percent rhodium-carbon / 1.) ethanol, room temperature, 1 atmosphere, 3 h, 2.) room temperature, 3 h View Scheme |
5-methoxy-2-nitro-benzaldehyde
(tert-Butoxycarbonylmethylene)triphenylphosphorane
5-methoxylindole
Conditions | Yield |
---|---|
With triphenylphosphine In diphenylether at 260℃; for 1h; | 51% |
5-methoxylindole
Conditions | Yield |
---|---|
With hydrogen In N,N-dimethyl-formamide at 330 - 340℃; under 15001.5 Torr; for 10h; Pressure; Temperature; |
2-(5-methoxy-2-nitrophenyl)acetonitrile
5-methoxylindole
Conditions | Yield |
---|---|
With hydrogen In methanol at 20℃; under 760.051 Torr; for 12h; | 88% |
With hydrogen; acetic acid; 10% palladium on active carbon In ethanol under 2280 Torr; for 2h; Ambient temperature; | 83% |
With hydrogen at 20℃; under 760.051 Torr; for 24h; Schlenk technique; | 68% |
Conditions | Yield |
---|---|
With copper(l) iodide In N,N-dimethyl-formamide for 6h; Reflux; | 98% |
(E)-5-methoxy-2-nitro-β-morpholinestyrene
5-methoxylindole
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In benzene at 50℃; under 4560 Torr; for 8h; | 72% |
1-(tert-butyloxycarbonyl)-5-methoxyindole
5-methoxylindole
Conditions | Yield |
---|---|
In various solvent(s) at 150℃; for 0.25h; microwave irradiation; | 98% |
With 1,1,1,3',3',3'-hexafluoro-propanol at 150℃; for 0.25h; Product distribution / selectivity; Microwave irradiation; | 98% |
With 1,1,1,3',3',3'-hexafluoro-propanol at 150℃; for 0.25h; Product distribution / selectivity; Microwave irradiation; | 98% |
Conditions | Yield |
---|---|
With tin(ll) chloride; dihydridotetrakis(triphenylphosphine)ruthenium In 1,4-dioxane; water at 180℃; for 20h; | 80% |
With triphenylphosphine; tin(ll) chloride; ruthenium trichloride In 1,4-dioxane; water at 180℃; for 20h; Cyclization; | 43% |
5-methoxyindoline
5-methoxylindole
Conditions | Yield |
---|---|
With H8O20P8Pt2(4-)*4C34H72N(1+) In methanol Inert atmosphere; Irradiation; | 99% |
With 6C44H32N6O4Ru(2+)*12Hf(2+)*8O(2-)*14HO(1-)*6C16H22ClCoN5O6(1-) In 2,2,2-trifluoroethanol; acetonitrile at 20℃; for 12h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Irradiation; | 96% |
With C21H21ClIrNO2 In tetrahydrofuran; 2,2,2-trifluoroethanol for 20h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
In quinoline for 0.2h; microwave; | 100% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In sulfolane at 300℃; for 0.333333h; Inert atmosphere; | 87% |
With quinoline; copper Heating; | 77% |
With quinoline; copper oxide-chromium oxide at 200 - 210℃; |
Conditions | Yield |
---|---|
With tin(ll) chloride; ruthenium trichloride; triphenylphosphine In 1,4-dioxane at 180℃; for 20h; | 33% |
5-methoxylindole
Conditions | Yield |
---|---|
With silica gel In 5,5-dimethyl-1,3-cyclohexadiene at 170℃; Retro Diels-Alder reaction; Inert atmosphere; | 97% |
5-methoxy-1-[(2-nitrophenyl)methyl]-1H-indole
5-methoxylindole
Conditions | Yield |
---|---|
With hydrazine In 1,4-dioxane; water for 0.333333h; Inert atmosphere; UV-irradiation; | 30% |
Conditions | Yield |
---|---|
With nickel-nitrogen-doped carbon framework In water at 145℃; for 18h; Inert atmosphere; Sealed tube; Green chemistry; | A 68% B 71% |
5-methoxyindoline
5-nitro-m-xylene
A
5-methoxylindole
B
3,5-dimethylaminoaniline
Conditions | Yield |
---|---|
With nickel-nitrogen-doped carbon framework In water at 145℃; for 18h; Inert atmosphere; Sealed tube; Green chemistry; | A 62% B 61% |
2-(2-amino-5-methoxyphenyl)ethyl alcohol
5-methoxylindole
Conditions | Yield |
---|---|
tris(triphenylphosphine)ruthenium(II) chloride In toluene for 6h; Heating; | 94% |
tris(triphenylphosphine)ruthenium(II) chloride In toluene for 6h; Rate constant; Heating; | 94% |
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; potassium carbonate In toluene at 111℃; for 20h; | 68% |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 2.89 g / 7 h / 148 - 150 °C 2: 72 percent / H2 / Pd/C / benzene / 8 h / 50 °C / 4560 Torr View Scheme | |
Multi-step reaction with 5 steps 1: N-bromosuccinimide (NBS), azoisobutyronitrile (AIBN) / CCl4 / 3 h / Heating 2: toluene / 1.) 6 h, RT; 2.) 3 h, 100 deg C 3: 74 percent / 48percent HBr, Zn / ethanol / 2 h / Heating 4: 87 percent / 2.5 h / Heating 5: 82 percent / t-BuOK / toluene / 0.25 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 4 h / 110 °C 2: TiCl3, 4M NH4OAc / acetone View Scheme |
2-chloro-5-methoxy-1H-indole
5-methoxylindole
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethyl acetate Ambient temperature; | 93% |
5-methoxyindoline
2,6-dimethylnitrobenzene
A
5-methoxylindole
B
2,6-dimethylaniline
Conditions | Yield |
---|---|
With nickel-nitrogen-doped carbon framework In water at 145℃; for 18h; Inert atmosphere; Sealed tube; Green chemistry; | A 40% B 41% |
1-[(E)-2-(5-methoxy-2-nitrophenyl)vinyl]pyrrolidine
5-methoxylindole
Conditions | Yield |
---|---|
With iron(III) chloride hexahydrate; pyrographite; hydrazine hydrate In ethanol at 75℃; for 5h; | 91% |
1-(Methylsulfonyl)-5-methoxyindole
5-methoxylindole
Conditions | Yield |
---|---|
With potassium hydroxide In methanol for 18h; Heating; | 91% |
Conditions | Yield |
---|---|
With phosphomolybdic acid In chloroform at 20 - 60℃; Fischer indole synthesis; | 88% |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; sodium methylate; copper(I) bromide at 120℃; for 10h; Time; Reagent/catalyst; Temperature; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) LiAlH4 / tetrahydrofuran / 0 °C / 1.) 15 min, 2.) 45 min 2: MnO2 / CH2Cl2 / 1 h / 25 °C 3: 95 percent / Rh(dppp)2Cl / 18 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: aq.-ethanolic KOH 2: quinoline; copper oxide-chromium oxide / 200 - 210 °C View Scheme | |
Stage #1: ethyl 5-methoxy-1H-indole-2-carboxylate With sodium hydroxide In ethanol at 40℃; Stage #2: With quinoline; copper at 250℃; for 0.416667h; Microwave irradiation; |
(4-Methoxy-2-trimethylsilanylethynyl-phenyl)-carbamic acid tert-butyl ester
5-methoxylindole
Conditions | Yield |
---|---|
With potassium tert-butylate In tert-butyl alcohol for 17h; Heating; | 67% |
5-methoxylindole
N,N-dimethyl-formamide
5-methoxyindole-3-carboxaldehyde
Conditions | Yield |
---|---|
With trichlorophosphate at 0 - 20℃; | 100% |
With sodium hydroxide; trichlorophosphate Vilsmeier-Haack reaction; | 98% |
Stage #1: N,N-dimethyl-formamide With trichlorophosphate at 0℃; for 0.333333h; Stage #2: 5-methoxylindole at 0 - 20℃; for 1.5h; | 98% |
Conditions | Yield |
---|---|
In 1,4-dioxane for 2h; Ambient temperature; | 100% |
In 1,4-dioxane at 20℃; for 0.5h; |
5-methoxylindole
5-methoxyindoline
Conditions | Yield |
---|---|
With sodium cyanoborohydride; acetic acid at 0 - 20℃; for 2h; | 100% |
With platinum/carbon xerogel catalyst; hydrogen; toluene-4-sulfonic acid In water at 25℃; under 22502.3 Torr; for 3h; regioselective reaction; | 96% |
With C26H29ClIrNO3; hydrogen In 2,2,2-trifluoroethanol at 20℃; under 760.051 Torr; for 3h; | 95% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 95 - 100℃; for 2h; | 100% |
5-methoxylindole
di-tert-butyl dicarbonate
1-(tert-butyloxycarbonyl)-5-methoxyindole
Conditions | Yield |
---|---|
With dmap In tetrahydrofuran at 20℃; for 16h; Acylation; | 100% |
With dmap; triethylamine In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran at 20℃; for 19h; | 99% |
dmap In acetonitrile at 20℃; | 97% |
5-methoxylindole
3,5-dimethylphenyl iodide
2,3-dihydro-5-methoxy-1-(3,5-dimethylphenyl)-1H-indole
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane In 1,4-dioxane; dodecane at 110℃; for 24h; | 100% |
5-methoxylindole
3,5-dimethylphenyl iodide
(S,S)-1,2-diaminocyclohexane
2,3-dihydro-5-methoxy-1-(3,5-dimethylphenyl)-1H-indole
Conditions | Yield |
---|---|
With potassium phosphate; CuI In 1,4-dioxane | 100% |
5-methoxylindole
bromoacetic acid methyl ester
methyl 2-(5-methoxy-1H-indol-1-yl)acetate
Conditions | Yield |
---|---|
Stage #1: 5-methoxylindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.75h; Stage #2: bromoacetic acid methyl ester In N,N-dimethyl-formamide; mineral oil at 20℃; for 15h; | 100% |
Stage #1: 5-methoxylindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.75h; Stage #2: bromoacetic acid methyl ester In N,N-dimethyl-formamide; mineral oil at 20℃; for 15h; | 100% |
(E)-3-(4-methoxyphenyl)-1-(1-methyl-1H-imidazol-2-yl)prop-2-en-1-one
5-methoxylindole
3-(5-methoxy-1H-indol-3-yl)-3-(4-methoxyphenyl)-1-(1-methyl-1H-imidazol-2-yl)propan-1-one
Conditions | Yield |
---|---|
With 4,4'-dimethyl-2,2'-bipyridines; copper(II) nitrate trihydrate In acetonitrile at 20℃; for 72h; Friedel-Crafts Alkylation; Inert atmosphere; | 100% |
With 4,4'-dimethyl-2,2'-bipyridines; copper(II) nitrate trihydrate In acetonitrile at 20℃; for 72h; Friedel-Crafts Alkylation; Inert atmosphere; | 100% |
With copper(II) nitrate trihydrate In aq. buffer at 20℃; for 72h; pH=6.5; Friedel-Crafts Alkylation; | 85% |
With copper(II) nitrate trihydrate In aq. buffer at 20℃; for 72h; pH=6.5; Reagent/catalyst; Friedel-Crafts Alkylation; enantioselective reaction; | 85% |
(E)-3-(4-chlorophenyl)-1-(1-methyl-1H-imidazol-2-yl)prop-2-en-1-one
5-methoxylindole
3-(4-chlorophenyl)-3-(5-methoxy-1H-indol-3-yl)-1-(1-methyl-1H-imidazol-2-yl)propan-1-one
Conditions | Yield |
---|---|
With 4,4'-dimethyl-2,2'-bipyridines; copper(II) nitrate trihydrate In acetonitrile at 20℃; for 72h; Friedel-Crafts Alkylation; Inert atmosphere; | 100% |
With 4,4'-dimethyl-2,2'-bipyridines; copper(II) nitrate trihydrate In acetonitrile at 20℃; for 72h; Catalytic behavior; Reagent/catalyst; Friedel-Crafts Alkylation; Inert atmosphere; | 100% |
With 4,4'-dimethyl-2,2'-bipyridines; copper(II) nitrate trihydrate In acetonitrile at 20℃; for 72h; Friedel-Crafts Alkylation; Inert atmosphere; | 100% |
5-methoxylindole
Conditions | Yield |
---|---|
With iodine In methanol at 20℃; for 24h; regioselective reaction; | 100% |
Conditions | Yield |
---|---|
With iodine; triphenylphosphine In ethanol at 70℃; for 24h; regioselective reaction; | 100% |
5-methoxylindole
Benzeneselenol
5-methoxy-3-(phenylselanyl)-1H-indole
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 27℃; for 0.5h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 5-methoxylindole With sodium hydride In acetonitrile at 0℃; for 0.5h; Stage #2: methyl iodide In acetonitrile at 0 - 20℃; for 16h; | 99% |
Stage #1: 5-methoxylindole With Tris(3,6-dioxaheptyl)amine; potassium tert-butylate In benzene at 20℃; for 1h; Stage #2: methyl iodide In benzene at 20℃; for 0.5h; | 97% |
With sodium hydroxide In dimethyl sulfoxide at 20℃; | 94% |
Conditions | Yield |
---|---|
Stage #1: nitrostyrene With (S)-10,10'-bis[(S)-4-isopropyl-4,5-dihydrooxazol-2-yl]-9,9'-biphenanthrene; zinc(II) trifluoroacetate In diethyl ether at 20℃; for 0.25h; Inert atmosphere; Stage #2: 5-methoxylindole In diethyl ether at 20℃; Friedel-Crafts alkylation; Inert atmosphere; | 99% |
With N,N'-bis(3,5-bis(trifluoromethyl)benzyl)-2-nitroethene-1,1-diamine In toluene at 20℃; for 24h; Michael Addition; | 99% |
With [(1S)-7,7-dimethyl-2-oxobicyclo[2.2.1]hept-1-yl]methanesulfonic acid In water at 20℃; for 8h; Friedel-Crafts Alkylation; Green chemistry; | 94% |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 3h; Electrochemical reaction; Inert atmosphere; | 99% |
With Oxone In methanol at 20℃; for 0.35h; | 98% |
With oxygen In tetrahydrofuran at 25℃; under 750.075 Torr; for 7h; Irradiation; | 98% |
Conditions | Yield |
---|---|
Stage #1: 5-methoxylindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h; Stage #2: benzyl bromide In N,N-dimethyl-formamide; mineral oil at 20℃; | 99% |
Stage #1: 5-methoxylindole With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere; Stage #2: benzyl bromide In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere; | 97% |
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; Inert atmosphere; | 94% |
5-methoxylindole
ethyl-3,3,3-trifluoropyruvate
Conditions | Yield |
---|---|
With (SIr,RC)-[(η5-C5Me5)Ir{(R)-propane-1,2-diylbis(diphenylphosphane)}(H2O)][SbF6]2 In dichloromethane for 0.333333h; Friedel-Crafts Alkylation; Inert atmosphere; Schlenk technique; Optical yield = 71 %ee; | 99% |
With K-10 montmorillonite In toluene at 60℃; for 0.0833333h; Friedel-Crafts hydroxyalkylation; | 97% |
In 1,1,1,3,3-pentafluorobutane at 20℃; for 0.5h; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With norborn-2-ene; dichloro bis(acetonitrile) palladium(II); potassium carbonate In N,N-dimethyl acetamide; water at 70℃; regioselective reaction; | 99% |
With potassium acetate; palladium diacetate; bis-diphenylphosphinomethane In water at 110℃; for 24h; regioselective reaction; | 79% |
With bis(di-tert-butyl(4-dimethylaminophenyl)phosphine)dichloropalladium(II); tetrachlorophthalic anhydride; sodium hydroxide In ethanol; water at 80℃; for 24h; regioselective reaction; | 73% |
With cesium acetate; palladium diacetate In N,N-dimethyl acetamide at 125℃; for 24h; | 64% |
With norborn-2-ene; palladium diacetate; potassium carbonate In N,N-dimethyl acetamide; water at 70℃; |
Conditions | Yield |
---|---|
With di(naphthalen-1-yl)silanediol In dichloromethane at 23℃; for 48h; Inert atmosphere; | 99% |
With 2,6-bis(2,2-dimethylpropionylamino)benzoic acid In chloroform at 40℃; for 24h; Friedel-Crafts Alkylation; | 99% |
With 1,1,1,3',3',3'-hexafluoro-propanol at 20℃; for 2h; Friedel-Crafts Alkylation; | 96% |
5-methoxylindole
2,2,2-trifluoro-1-methoxy-ethanol
3,4,5-Trimethoxyaniline
N-((R)-2,2,2-trifluoro-1-(5-methoxy-1H-indol-3-yl)ethyl)-3,4,5-trimethoxybenzenamine
Conditions | Yield |
---|---|
With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In dichloromethane at 20℃; for 24h; Friedel Crafts aminoalkylation; Molecular sieve; optical yield given as %ee; enantioselective reaction; | 99% |
5-methoxylindole
diethyl m-methylbenzylidenemalonate
Conditions | Yield |
---|---|
Stage #1: 5-methoxylindole With C45H52N4O4; scandium tris(trifluoromethanesulfonate) In tert-butyl alcohol at 35℃; for 1h; Inert atmosphere; Stage #2: diethyl m-methylbenzylidenemalonate In diethyl ether at -20℃; for 118h; Friedel Crafts alkylation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
5-methoxylindole
1,1,1-trifluoroacetophenone
2,2,2-trifluoro-1-(5-methoxy-1H-indol-3-yl)-1-phenylethan-1-ol
Conditions | Yield |
---|---|
With tetrabutyl phosphonium bromide; potassium carbonate In water at 20℃; for 12h; Reagent/catalyst; regioselective reaction; | 99% |
With N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; water at 20℃; for 16h; Friedel-Crafts type alkylation; | 98% |
With TMG In dichloromethane at 20℃; | |
With diphenyl hydrogen phosphate In dichloromethane at 0℃; for 20h; Friedel-Crafts Alkylation; Molecular sieve; Inert atmosphere; Sealed tube; |
5-methoxylindole
1,1,1-trifluoroacetophenone
(R)-2,2,2-trifluoro-1-(5-methoxy-1H-indol-3-yl)-1-phenylethanol
Conditions | Yield |
---|---|
With (S)-3,3'-bis(2,4,6-tri-iso-propylphenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In dichloromethane at 25℃; for 48h; optical yield given as %ee; enantioselective reaction; | 99% |
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