Items Standard Result Description Light yellow transparent liquid Pass Assay 99%min 99.69% 2,6-Dimethylphenol
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryItems Standard Result Description Light yellow transparent liquid Pass Assay 99%min
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 1-Amino-2,6-dimethylbenzene CAS No. 87-62-7 Appearance
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inquiryHebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
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inquiryhigh quality Appearance:Liquid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryCompetitive Price High Quality Fast Delivery custom-made Welcome to Henan Tianfu Chemical Co., Ltd. website. Our company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble me
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inquiryDescription of 2,6-Dimethyl aniline Product name: 2,6-Dimethyl aniline CAS NO.: 87-62-7 MF: C8H11N Structural formula: Specification of 2,6-Dimethyl aniline Appearance: Colorless or light brown liquid Purity: 99.8%min 2,4-D
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting 2,6-Dimethylaniline;2,6-xylidine CAS:87-62-7, Please contact us by email freely. We are leading exporter in China. If you really need
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inquiryAppearance: light yellow liquid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Sea/Ai
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiry2,6-DimethylanilineAppearance:Pls see the Details Storage:Keep away of light, hot, water, Store in dry, dark and ventilated place Package:according to customers' requirements Application:Steroids, Cosmetics Ingredients, APIs, Intermediates, OLED&Batt
Product name: 2,6-Dimethylaniline CAS No.:87-62-7 Molecule Formula:C8H11N Molecule Weight:121.18 Purity: 99.0% Package: 200kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard TESTING ITEM
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryProductName:2,6-dimethylaniline CAS:87-62-7 Molecular Formula:C8H11N Molecular Weight:121.18000 Appearance: Colorless or light brown liquid Assay:≥99.8% Water content:≤0.10% Appearance:Colorless transparent liquid Storage:keep
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
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SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
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inquiryCapability on chemical synthesis1. Beijing High-Tech Enterprises2. Strong R&D Team3. 8 years of experiences in R & D of high-tech Catalyst;4. 5000 production techniques, 69 items of national patents, and 360 kinds of products on sales;5. The producti
Superior quality, moderate price & quick delivery. Appearance:Colorless or light yellow liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmac
High purity, high success rate, short cycle and moderate priceAppearance:White powder solid Storage:Negative 20 degrees Celsius Package:5mg, 10mg 100mg, 1gram Application:Applied to various scientific research
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers327.Safe and fa
Conditions | Yield |
---|---|
With potassium fluoride; polymethylhydrosiloxane; palladium diacetate In tetrahydrofuran; water at 20℃; for 3h; | 100% |
With potassium fluoride; polymethylhydrosiloxane; palladium diacetate In tetrahydrofuran at 20℃; for 0.5h; | 100% |
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; for 10h; | 100% |
2,6-dimethylphenylazide
2,6-dimethylaniline
Conditions | Yield |
---|---|
With sodium hydrogen telluride In diethyl ether; ethanol for 0.25h; Ambient temperature; | 100% |
With aluminium(III) iodide In benzene for 0.166667h; Reduction; Heating; | 90% |
With diphosphorus tetraiodide In benzene for 11h; Heating; | 40% |
Conditions | Yield |
---|---|
With dichloro(dimethylglyoxime)(dimethylglyoximato)cobalt(III); (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; triethylamine In acetonitrile at -78℃; for 24h; Reagent/catalyst; Sealed tube; Inert atmosphere; Irradiation; | 100% |
Conditions | Yield |
---|---|
With sodium hydroxide In water at 60 - 130℃; under 4560.31 Torr; for 3.5h; Temperature; | 99.1% |
2,6-dimethylaniline
Conditions | Yield |
---|---|
With ethylenediamine In ethanol at 65℃; for 14h; | 99% |
Conditions | Yield |
---|---|
With 2-((dicyclohexylphosphino)methyl)-1,3-bis(2,6-diisopropylphenyl)-4,5-dimethyl-1H-imidazol-3-ium iodide; ammonia; palladium diacetate; sodium t-butanolate In 1,4-dioxane at 120℃; under 7500.75 Torr; for 24h; Autoclave; Inert atmosphere; | 98% |
With C28H30Cl5N3Pd; ammonia; lithium isopropoxide; sodium t-butanolate In 1,4-dioxane at 100℃; for 2h; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 91% |
With bis(tri-ortho-tolylphosphine)palladium(0); (R)-(-)-1-[(S)-2-(dicyclohexylphosphino)ferrocenyl]ethyl-di-tert-butylphosphine; ammonia; sodium t-butanolate In 1,4-dioxane at 100℃; for 24h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With potassium hydroxide In water at 60 - 125℃; under 2280.15 Torr; for 3h; | 97.5% |
1,2-dimethoxybenzene
N-(2,6-diimethylphenyl)benzamide
A
3,4-dimethoxybenzophenone
B
2,6-dimethylaniline
Conditions | Yield |
---|---|
Stage #1: N-(2,6-diimethylphenyl)benzamide With 2-fluoropyridine; trifluoromethylsulfonic anhydride In dichloromethane at -78 - 0℃; for 0.166667h; Inert atmosphere; Stage #2: 1,2-dimethoxybenzene In dichloromethane at 0 - 20℃; Inert atmosphere; Stage #3: With hydrogenchloride; water In ethanol for 2h; Inert atmosphere; Reflux; chemoselective reaction; | A 97% B 90% |
Conditions | Yield |
---|---|
With 2,6-dimethylcyclohexanone; ammonium hydroxide; 5%-palladium/activated carbon at 180℃; for 5h; Concentration; Temperature; | 95.62% |
With ammonia; hydrogen In 1,4-dioxane at 230℃; under 760.051 Torr; | 86.56% |
With ammonia |
2,6-dimethylphenyl diethyl phosphate
2,6-dimethylaniline
Conditions | Yield |
---|---|
With potassium; potassium amide In diethyl ether; ammonia at -78℃; 1.0-1.2 h; | 95% |
2,6-dimethylbenzene boronic acid
2,6-dimethylaniline
Conditions | Yield |
---|---|
With copper(I) oxide; ammonium hydroxide; air In methanol at 20℃; for 12h; | 92% |
With potassium carbonate; ammonium hydroxide In methanol at 60℃; for 13h; | 87% |
With copper(ll) sulfate pentahydrate; ammonia; sodium hydroxide In water at 20℃; under 760.051 Torr; for 4h; | 58% |
Multi-step reaction with 2 steps 1: potassium hydrogenfluoride / methanol; water / 0.5 h / 0 °C 2: ammonium hydroxide; copper(ll) sulfate pentahydrate; sodium hydroxide / water / 24 h / 25 °C View Scheme |
Conditions | Yield |
---|---|
With bis(tri-ortho-tolylphosphine)palladium(0); (R)-(-)-1-[(S)-2-(dicyclohexylphosphino)ferrocenyl]ethyl-di-tert-butylphosphine; ammonia; sodium t-butanolate In 1,4-dioxane at 80℃; for 15h; Inert atmosphere; | 88% |
With magnesium In diethyl ether Ambient temperature; | 79% |
With [N,N'-bis(5-sulfonatosalicylidene)-1,2-diaminoethane]copper disodium salt; ammonia; sodium hydroxide In water at 120℃; for 12h; sealed tube; | 64% |
With C24H32N2*ClCu; ammonia; potassium carbonate In 1-methyl-pyrrolidin-2-one; methanol at 120℃; under 5171.62 Torr; for 48h; Inert atmosphere; | 7% |
With ammonium hydroxide; sodium hydroxide In water |
2,6-dimethylaniline
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal; palladium hydroxide - carbon In methanol; water at 20℃; under 3620.04 Torr; for 60h; Hydrogenolysis; | 86% |
N-methyl-N-allylamine
N-(2,6-dimethylphenyl)benzimidamide
B
2,6-dimethylaniline
Conditions | Yield |
---|---|
With bis(trimethylsilyl)amide yttrium(III) In neat (no solvent) at 100℃; for 120h; Inert atmosphere; | A 86% B n/a |
2,6-dimethylaniline
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal; palladium hydroxide - carbon In methanol; water under 3620.04 Torr; Ambient temperature; | 83% |
With hydrogen; palladium on activated charcoal; palladium hydroxide - carbon In methanol; water at 20℃; under 3620.04 Torr; for 64h; Hydrogenolysis; | 83% |
5-chloropentano-2',6'-xylidide
diethylamine
A
5-(diethylamino)pentano-2',6'-xylidide
B
2,6-dimethylaniline
Conditions | Yield |
---|---|
With sodium iodide In ethanol for 48h; Heating; | A 82% B n/a |
2,6-dimethyl-N-methylene benzamine
A
N-methyl-2,6-dimethylaniline
B
N,N,2,6-tetramethylaniline
C
2,6-dimethylaniline
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether Heating; | A 81% B 3% C 10% |
(E)-3-Phenyl-acrylic acid 1-(2,6-dimethyl-phenylcarbamoyl)-1-methyl-2-oxo-propyl ester
A
N-(2,6-dimethylphenyl) 2-acetyl 2-hydroxypropanamide
B
2,6-dimethylaniline
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride; cesium fluoride In tetrahydrofuran for 24h; Heating; | A 80% B n/a |
2,6-dimethylbenzene boronic acid
A
2.6-dimethylphenol
B
2,6-dimethylaniline
Conditions | Yield |
---|---|
With ammonium hydroxide; potassium nitrate In water at 20℃; for 2h; Electrochemical reaction; chemoselective reaction; | A n/a B 73% |
With ammonium hydroxide; potassium nitrate In water at 20℃; for 4h; Electrochemical reaction; chemoselective reaction; | A 70% B n/a |
2,6-dimethylaniline
Conditions | Yield |
---|---|
With O-Methylhydroxylamin; n-butyllithium In tetrahydrofuran; hexane at -78 - 60℃; for 24h; Inert atmosphere; Cooling with acetone-dry ice; stereospecific reaction; | 71% |
2,6-dimethylaniline
Conditions | Yield |
---|---|
66% |
Conditions | Yield |
---|---|
With ethene; 5%-palladium/activated carbon; ammonium acetate In acetonitrile at 90℃; under 760.051 Torr; for 15h; Schlenk technique; | 63% |
With urea In water; 1,3,5-trimethyl-benzene at 150℃; under 760.051 Torr; for 24h; Schlenk technique; Inert atmosphere; | 37 %Chromat. |
4-chlorobutyro-2',6'-xylidide
diethylamine
A
N-(2,6-dimethylphenylcarbamoylpropyl)diethylamine
B
1-(2,6-dimethylphenyl)pyrrolidin-2-one
C
2,6-dimethylaniline
Conditions | Yield |
---|---|
In toluene for 2h; Heating; | A 31% B 60% C n/a |
3-Methoxy-pyridine-2-carboxylic acid (2,6-dimethyl-phenyl)-amide
A
2,6-dimethylaniline
Conditions | Yield |
---|---|
With water In methanol at 25℃; electrochemical reduction; | A 60% B 5% |
2,6-dimethylaniline
Conditions | Yield |
---|---|
Sample heated for 1.0 h at 200-220°C and 1 torr.; | 60% |
N1,N2-bis(2,6-dimethylphenyl)ethane-1,2-diimine
1,2-phenylenediacetonitrile
A
naphthalene-1,4-dicarbonitrile
B
2,6-dimethylaniline
Conditions | Yield |
---|---|
With potassium hydroxide In N,N-dimethyl-formamide at 100℃; for 15h; | A 58% B n/a |
m-xylene
A
3,5-dimethylaminoaniline
B
2,4-Xylidine
C
2,6-dimethylaniline
Conditions | Yield |
---|---|
With tris-(2-chloro-ethyl)-amine; trifluorormethanesulfonic acid; trifluoroacetic acid In chloroform at 25℃; for 1h; | A 2% B 58% C 15% |
With hydrogenchloride; aluminium trichloride; sodium azide In various solvent(s) at 20℃; | |
With sodium azide; trifluorormethanesulfonic acid at 20℃; Ultrasonic irradiation; | |
Stage #1: m-xylene With sulfuric acid; hydroxylamine hydrochloride In acetonitrile at 25℃; for 0.166667h; Stage #2: With hydrogenchloride; titanium(III) chloride In water; acetonitrile at 25℃; Inert atmosphere; Sealed tube; Overall yield = 60 percent; Overall yield = 72 mg; |
Conditions | Yield |
---|---|
In neat (no solvent) at 100℃; for 120h; | A 57% B n/a |
Acetic acid 1-(2,6-dimethyl-phenylcarbamoyl)-1-methyl-2-oxo-propyl ester
A
N,N'-di (2,6-dimethylphenyl) urea
B
N-(2,6-dimethylphenyl) 2-acetyl 2-hydroxypropanamide
C
2,3-Dimethyl-5-oxo-2,5-dihydro-furan-2-carboxylic acid (2,6-dimethyl-phenyl)-amide
D
2,6-dimethylaniline
Conditions | Yield |
---|---|
With N-benzyl-N,N,N-triethylammonium chloride; cesium fluoride In tetrahydrofuran for 4h; Heating; | A n/a B 50% C 40% D n/a |
Conditions | Yield |
---|---|
In toluene Reflux; | 100% |
In toluene Reflux; | 100% |
In toluene Reflux; | 100% |
Conditions | Yield |
---|---|
In acetonitrile at 25℃; | 100% |
Carbonylbis(isocyaniddichlorid)
2,6-dimethylaniline
4,6-Dichlor-5-(2,6-dimethylphenyl)-1,3,5-triazin-2(5H)-on
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0℃; for 0.75h; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran at -20℃; for 0.25h; | 100% |
In tetrahydrofuran at 20℃; | |
In dichloromethane at 20℃; for 2h; |
2,6-dimethylaniline
Trimethylacetic acid
2,2-dimethyl-N-(2,6-dimethylphenyl)propionamide
Conditions | Yield |
---|---|
With diphosphorus tetraiodide In tetrachloromethane; dichloromethane Heating; | 100% |
1,2-dibromo-4,5-dimethylbenzene
2,6-dimethylaniline
Conditions | Yield |
---|---|
With ammonium chloride; sodium t-butanolate; palladium diacetate In water; argon; toluene | 100% |
With palladium diacetate; tri-tert-butyl phosphine; sodium t-butanolate In toluene at 110℃; for 14h; | 75% |
di-tert-butyl dicarbonate
2,6-dimethylaniline
Conditions | Yield |
---|---|
With indium(III) bromide at 30 - 35℃; for 0.5h; | 100% |
In ethanol at 30℃; for 48h; | 99% |
copper(II) bis(tetrafluoroborate) at 30 - 33℃; for 0.5h; | 98% |
With choline chloride; urea at 50℃; Green chemistry; | 90% |
In tetrahydrofuran; water for 0.5h; | 111 mg |
Conditions | Yield |
---|---|
In acetonitrile at 25℃; | 100% |
In acetonitrile at 25℃; Equilibrium constant; Kinetics; Further Variations:; title comp. concentration; |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; | 100% |
In dichloromethane at 20℃; |
2,6-dimethylaniline
3-(2,6-dimethyl phenyl carbamoyl)-5-acetoxymethyl isoxazole
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In tetrahydrofuran | 100% |
With triethylamine; trichlorophosphate In tetrahydrofuran | 100% |
Conditions | Yield |
---|---|
In acetonitrile at 25℃; Kinetics; | 100% |
1-(4-nitrophenoxy)-2,4,6-trinitrobenzene
2,6-dimethylaniline
Conditions | Yield |
---|---|
In acetonitrile at 25℃; Kinetics; Concentration; | 100% |
2-nitrophenyl 2,4,6-trinitrophenyl ether
2,6-dimethylaniline
Conditions | Yield |
---|---|
In acetonitrile at 25℃; Kinetics; Concentration; | 100% |
2,6-dinitrophenyl 2,4,6-trinitrophenyl ether
2,6-dimethylaniline
Conditions | Yield |
---|---|
In acetonitrile at 25℃; Kinetics; Concentration; | 100% |
phenylacetylene
2,6-dimethylaniline
2,6-dimethyl-N-(1-phenylethylidene)benzenamine
Conditions | Yield |
---|---|
With C30H36FeP2*2Au(1+)*Cl(1-)*C32H12BF24(1-) In (2)H8-toluene at 120℃; for 6h; Reagent/catalyst; Inert atmosphere; Schlenk technique; Sealed tube; Glovebox; | 100% |
With silver tetrafluoroborate; {(2,6-bis(1-isopropyl-2,3-dihydro-1H-imidazole-2-thione)pyridine)12Cu8}(PF6)8 In acetonitrile at 70℃; for 2h; Reagent/catalyst; Solvent; Temperature; Schlenk technique; Inert atmosphere; regioselective reaction; | 99% |
With silver tetrafluoroborate; C57H72Au4I4N12O4 In [D3]acetonitrile at 70℃; for 6h; Reagent/catalyst; Inert atmosphere; | 93% |
[RuVI(5,10,15,20-tetrakis(4-methylphenyl)porphyrinato(2-))O2]
2,6-dimethylaniline
[Ru(IV)(ttp)(NQu)(OH)]
Conditions | Yield |
---|---|
Stage #1: [RuVI(5,10,15,20-tetrakis(4-methylphenyl)porphyrinato(2-))O2]; 2,6-dimethylaniline In ethanol for 8h; Stage #2: With water In dichloromethane for 0.5h; | 100% |
[Ru(VI)(O)2(5,10,15,20-tetrakis(4-methoxyphenyl)porphyrinate)]
2,6-dimethylaniline
[Ru(IV)(4-OMe-ttp)(NQu)(OH)]
Conditions | Yield |
---|---|
Stage #1: [Ru(VI)(O)2(5,10,15,20-tetrakis(4-methoxyphenyl)porphyrinate)]; 2,6-dimethylaniline In ethanol for 8h; Stage #2: With water In dichloromethane for 0.5h; | 100% |
[Ru(VI)(meso-tetrakis(p-chlorophenyl)porphyrinato)O2]
2,6-dimethylaniline
[Ru(IV)(4-Cl-ttp)(NQu)(OH)]
Conditions | Yield |
---|---|
Stage #1: [Ru(VI)(meso-tetrakis(p-chlorophenyl)porphyrinato)O2]; 2,6-dimethylaniline In ethanol for 8h; Stage #2: With water In dichloromethane for 0.5h; | 100% |
salicylaldehyde
2,6-dimethylaniline
2-(((2,6-dimethylphenyl)imino)methyl)phenol
Conditions | Yield |
---|---|
In ethanol at 80℃; for 2h; Inert atmosphere; | 100% |
With magnesium sulfate In toluene for 4h; Inert atmosphere; Reflux; | 98% |
In isopropyl alcohol at 80℃; for 24h; Inert atmosphere; |
5-Nitrosalicylaldehyde
2,6-dimethylaniline
2-[(2,6-dimethylphenylimino)methyl]-4-nitrophenol
Conditions | Yield |
---|---|
In ethanol at 80℃; for 2h; Inert atmosphere; | 100% |
In isopropyl alcohol at 80℃; for 24h; Inert atmosphere; |
2,6-dimethylaniline
Conditions | Yield |
---|---|
In toluene at 20℃; for 48h; | 100% |
2,6-dimethylaniline
Conditions | Yield |
---|---|
In toluene at 20℃; for 48h; | 100% |
Conditions | Yield |
---|---|
With triethylamine In toluene Heating; | 99% |
With triethylamine In acetone at 20℃; Cooling with ice; | 93% |
With triethylamine In dichloromethane for 48h; Reflux; | 67% |
2-Bromoacetyl bromide
2,6-dimethylaniline
2-bromo-N-(2,6-dimethyl-phenyl)-acetamide
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane; water at 0℃; for 1h; | 99% |
With sodium carbonate In water pH=9 - 10; | 99% |
With triethylamine In chloroform at -10℃; for 2.25h; | 88% |
Conditions | Yield |
---|---|
99% | |
Stage #1: 2,6-dimethylaniline With n-butyllithium In hexane at -20 - 20℃; for 3h; Inert atmosphere; Stage #2: methyl iodide In diethyl ether at -20 - 20℃; Inert atmosphere; | 94% |
Stage #1: 2,6-dimethylaniline With n-butyllithium In hexane at -20 - 20℃; for 3h; Inert atmosphere; Stage #2: methyl iodide In diethyl ether at -20 - 20℃; Inert atmosphere; | 85% |
2,6-dimethylaniline
2,6-dimethyl-N-sulfinyl-benzenamine
Conditions | Yield |
---|---|
With thionyl chloride In benzene for 16h; Reflux; | 99% |
With thionyl chloride | |
With thionyl chloride In benzene Heating; | |
Multistep reaction; | |
With thionyl chloride In toluene Reflux; |
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