Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:103-67-3
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:103-67-3
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryhe company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality se T rvice Appearance:whit
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:103-67-3
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryTIANFUCHEM--103-67-3--N-Methylbenzylamine in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relation
Cas:103-67-3
Min.Order:1 Metric Ton
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:103-67-3
Min.Order:1 Kilogram
FOB Price: $15.0 / 50.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:103-67-3
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
Cas:103-67-3
Min.Order:1 Kilogram
FOB Price: $4.0 / 5.0
Type:Trading Company
inquiryProduct Name:N-Methylbenzylamine Formula:C8H11N Molecular Weight:121.18 CAS No.:103-67-3 EINECS:203-133-4 Density:0.939 g/mL at 25 °C(lit.) Solubility:Water: 65 g/L (20°C ) Melting Point:-24 °C Boiling Point:180.5 °C
Cas:103-67-3
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiryAppearance:Colorless to light yellow liquid Storage:room temperature Package:200kg/drum Application:N-Benzylmethylamine is used in the production of dyes. It can be also used as catalytic agent, Petrochemical additive Transportation:Express/Sea/Air
Cas:103-67-3
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:Colorless Clear Liquid Storage:Store in sealed containers at
Cas:103-67-3
Min.Order:100 Gram
Negotiable
Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:103-67-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:103-67-3
Min.Order:1 Kilogram
FOB Price: $15.0 / 22.0
Type:Trading Company
inquiryN-Methylbenzylamine CAS:103-67-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
Cas:103-67-3
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:103-67-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHebei Mojin Biotechnology Co., Ltd,Our business covers more than 30 countries, most of the big customers come from Europe, America and other countries in the world, we can guarantee the quality and price. In recent decades, with the efforts of all em
Cas:103-67-3
Min.Order:1 Gram
FOB Price: $100.0
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:103-67-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryAppearance:white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:packaged in foil bags or tins Application:Use only for laboratory research Transportation:Sea,Air,DHL/TNT/FEdex/UPS/EMS Por
Cas:103-67-3
Min.Order:10 Gram
FOB Price: $1.0 / 10.0
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:103-67-3
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
advantage: 1. The best price, satisfactory quality; 2. customers have the right to choose the delivery of parcels (EMS, DHL, FedEx, UPS); 3. customers have the right to choose from the recent effective packaging methods of their products packaging
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:103-67-3
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryProduct name: N-Methylbenzylamine CAS No.:103-67-3 Molecule Formula:C8H11N Molecule Weight:121.18 Purity: 99.0% Package:180kg/drum Description:Colorless to pale yellow liquid Manufacture Standards:Enterprise Standard
Cas:103-67-3
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:103-67-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1.High purity, like 99%, 99.9%, 99.95%, 99.99% 2.Quality control, test sample before shipping and keep sample for 3 years after shipping; 3. Prompt shipment with professional documents; 4. Packing as your request, with photo before shipment;
Cas:103-67-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryN-Methylbenzylamine Basic information Product Name: N-Methylbenzylamine Synonyms: Benzenemethanamine,N-methyl-;Benzylamine, N-methyl-;N-Methyl(phenyl)methanamine;n-methyl-benzenemethanamin;N-methyl-Benzenemethanamine;N-Methy-N-benzylamine;Meth
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:103-67-3
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Conditions | Yield |
---|---|
With poly(p-aminostyrene)-palladium(II); hydrogen In N,N-dimethyl-formamide at 25℃; under 760 Torr; | 100% |
With potassium hydroxide; isopropyl alcohol; chelating Rh(III) bis-carbene for 18h; Heating; | 98% |
With bis(pentamethylcyclopentadienyl)zinc; hydrogen; 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene In benzene-d6 at 25℃; under 51005.1 Torr; for 24h; Reagent/catalyst; Inert atmosphere; | 98% |
N-allyloxycarbonyl-N-methylbenzylamine
benzyl-methyl-amine
Conditions | Yield |
---|---|
With diethylamine; palladium diacetate; trisodium tris(3-sulfophenyl)phosphine In water for 0.25h; Ambient temperature; | 100% |
With 1,3-dimethylbarbituric acid; tetrakis(triphenylphosphine) palladium(0) In dichloromethane at 20℃; deallylation; | 100 % Chromat. |
Conditions | Yield |
---|---|
With Thiosalicylic acid; 1,4-di(diphenylphosphino)-butane; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran at 20℃; for 0.416667h; | 100% |
With Thiosalicylic acid; 1,4-di(diphenylphosphino)-butane; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran at 20℃; for 0.416667h; | 100% |
With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); diisobutylaluminium hydride In toluene for 1h; Ambient temperature; | 84% |
Grubbs catalyst first generation In toluene at 110℃; for 1.5h; | 78% |
Grubbs catalyst first generation In toluene for 1.5h; Heating; | 78% |
(N-benzyl, N-methyl) 2,4-dinitrophenylsulfonamide
A
S-(2,4-Dinitrophenyl)-cystein
B
sulfur dioxide
C
benzyl-methyl-amine
Conditions | Yield |
---|---|
In aq. phosphate buffer for 0.5h; pH=7.4; | A n/a B 100% C n/a |
Benzyl isocyanide
benzyl-methyl-amine
Conditions | Yield |
---|---|
With Zr12(μ3-O)5[(μ3-O)CoCl]8[(μ2-O)2(μ3-O)CoCl]3Li3(triphenyldicarboxylate)9; hydrogen In toluene at 110℃; under 30003 Torr; for 42h; Catalytic behavior; Inert atmosphere; Schlenk technique; | 100% |
(N-benzyl-N-methylamino)acetonitrile
benzyl-methyl-amine
Conditions | Yield |
---|---|
With hydrogen; platinum(IV) oxide In ethanol | 98% |
benzyl-methyl-amine
Conditions | Yield |
---|---|
With potassium carbonate; mercaptoacetic acid In methanol at 0 - 25℃; Inert atmosphere; chemoselective reaction; | 98% |
methyl N-benzyl,N-methyl carbamate
benzyl-methyl-amine
Conditions | Yield |
---|---|
Stage #1: methyl N-benzyl,N-methyl carbamate With 3-azapentane-1,5-diamine at 140℃; for 48h; Sealed tube; Stage #2: With hydrogenchloride In diethyl ether at 0 - 20℃; | 98% |
Conditions | Yield |
---|---|
Stage #1: benzaldehyde; methylamine In methanol at 20℃; Stage #2: With sodium tetrahydroborate In methanol for 6h; | 96.6% |
Stage #1: benzaldehyde; methylamine With titanium(IV) isopropylate In methanol at 20℃; for 5h; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 2h; | 92% |
With copper chromium spinel oxide; hydrogen; barium(II) oxide at 130℃; under 37503 Torr; for 1h; | 62% |
N-allyloxycarbonyl-N-methylbenzylamine
A
N-allyl-N-α-methylbenzylamine
B
benzyl-methyl-amine
Conditions | Yield |
---|---|
With diethylamine; palladium diacetate; trisodium tris(3-sulfophenyl)phosphine In water at 20℃; for 0.0833333h; | A n/a B 96% |
With diethylamine; palladium diacetate; trisodium tris(3-sulfophenyl)phosphine In water; acetonitrile for 0.0833333h; Ambient temperature; | A 70% B 30% |
With tetrabutylammonium borohydride; tetrakis(triphenylphosphine) palladium(0) In dichloromethane at 20℃; Product distribution; Further Variations:; Reagents; Decarboxylation; substitution; |
tert-butyl N-benzyl-N-methylcarbamate
benzyl-methyl-amine
Conditions | Yield |
---|---|
With nitric acid In dichloromethane at 0℃; for 1h; | 96% |
With methanol; Amberlyst 15; ammonia 1.) CH2Cl2, 25 deg C, 8 h, 2.) 50 min; Yield given. Multistep reaction; | |
With trifluoroacetic acid In dichloromethane at 20℃; for 16h; Inert atmosphere; | |
With 1,1,3,3-Tetramethyldisiloxane; pyrographite; palladium dichloride In 1,2-dimethoxyethane at 25 - 40℃; for 24h; | >99 %Spectr. |
Conditions | Yield |
---|---|
With butyl triphenylphosphonium tetraborate at 20℃; for 0.166667h; | 96% |
Stage #1: formaldehyd; benzylamine In methanol at 20℃; for 1h; Stage #2: With sodium tetrahydroborate In methanol at 0 - 20℃; for 1h; | 60% |
With formic acid In dimethyl sulfoxide for 0.0166667h; Eschweiler-Clarke methylation; microwave irradiation; | |
Stage #1: formaldehyd; benzylamine In tetrahydrofuran at 120℃; for 9h; Autoclave; Stage #2: With hydrogen In tetrahydrofuran at 140℃; under 3750.38 Torr; for 9h; Autoclave; |
N-benzyl-N-methyl-2-nitrobenzenesulfonamide
benzyl-methyl-amine
Conditions | Yield |
---|---|
With polystyrene-thiophenol; caesium carbonate; triphenylphosphine In tetrahydrofuran at 20℃; for 24h; | 96% |
N-methylbenzamide
benzyl-methyl-amine
Conditions | Yield |
---|---|
With triethyl borane; phenylsilane; sodium methylate In tetrahydrofuran at 50℃; Reagent/catalyst; Inert atmosphere; Schlenk technique; Sealed tube; chemoselective reaction; | 95% |
With triethyl borane; phenylsilane; sodium methylate In tetrahydrofuran at 50℃; Inert atmosphere; Schlenk technique; Glovebox; Sealed tube; | 95% |
Stage #1: N-methylbenzamide With triethyl borane; phenylsilane; sodium methylate In tetrahydrofuran; tert-butyl methyl ether at 20 - 50℃; for 48h; Sealed tube; Stage #2: With hydrogenchloride In tetrahydrofuran; tert-butyl methyl ether; ethyl acetate at 20℃; for 6h; | 95% |
N-benzyl-N-methylacetamide
benzyl-methyl-amine
Conditions | Yield |
---|---|
With ammonium bromide; ethylenediamine at 80℃; for 10h; Microwave irradiation; Inert atmosphere; neat (no solvent); | 95% |
4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl-amine
B
benzyl-methyl-amine
Conditions | Yield |
---|---|
A 94% B n/a |
4-(Methylthio)-N-methylbenzenemethanamine
benzyl-methyl-amine
Conditions | Yield |
---|---|
With sodium tetrahydroborate; nickel dichloride | 91% |
With sodium tetrahydroborate; nickel dichloride In methanol for 18h; Ambient temperature; |
N-benzyl-2,2,2,-trifluoro-N-methylacetamide
benzyl-methyl-amine
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol at 60℃; for 15h; | 90% |
(R,S)-N,N'-dimethyl-1,2-diphenylethylenediamine
(+/-)-N,N'-dimethyl-1,2-diphenyl-1,2-ethylenediamine
B
benzyl-methyl-amine
Conditions | Yield |
---|---|
With lithium; isoprene In tetrahydrofuran at 35℃; for 1h; Yields of byproduct given; | A 89% B n/a |
methanol
N-methyl-N-benzylformamide
β-naphthol
A
1-methyl-2-naphthol
B
benzyl-methyl-amine
Conditions | Yield |
---|---|
With pyrrolidine; tris(2,4-pentanedionato)ruthenium(III); [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In tetrahydrofuran at 150℃; for 20h; | A 89% B 10% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; 1,2-dimethoxybenzene In ethanol for 1h; Irradiation; | 87% |
With sodium tetrahydroborate; 1,2-dimethoxybenzene In ethanol Irradiation; | 87% |
With titanium tetrachloride In tetrahydrofuran for 6h; Heating; | 45% |
N-benzyl-N-methylbenzenesulfonamide
benzyl-methyl-amine
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; sodium iodide In acetonitrile for 3h; Heating; | 86% |
With hydrogenchloride at 160 - 180℃; |
benzyl-methyl-amine
Conditions | Yield |
---|---|
With magnesium In methanol at 0℃; for 1.5h; | 86% |
N-Benzylidenemethylamine
allyl bromide
A
N-methyl-α-2-propenylbenzemethanamine
B
benzyl-methyl-amine
Conditions | Yield |
---|---|
With bismuth; tetrabutylammomium bromide In acetonitrile for 0.166667h; Ambient temperature; | A 85% B n/a |
β,β,β-Trichloroethyl Benzylmethylaminoformate
benzyl-methyl-amine
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; mischmetal (50 percent Ce, 25 percent La, 16 percent Nd, 6 percent Pr) In tetrahydrofuran for 2h; Heating; | 85% |
benzyl-methyl-amine
Conditions | Yield |
---|---|
With water In ethanol at 60℃; for 48h; | 84% |
benzyl-methyl-amine
Conditions | Yield |
---|---|
Stage #1: N-benzyl-N-methyltritylamine With naphthalene; lithium In tetrahydrofuran at 0℃; for 1h; Stage #2: With water In tetrahydrofuran at 0 - 20℃; | 84% |
methanol
benzylamine
A
N-methyl-N-benzylformamide
B
benzyl-methyl-amine
Conditions | Yield |
---|---|
With carbonylhydrido(tetrahydroborato)[bis(2-diphenylphosphinoethyl)amino]ruthenium(II); hydrogen at 120℃; under 30003 Torr; for 24h; Temperature; Reagent/catalyst; Glovebox; | A 6% B 82% |
methanol
N-benzyl-N,4-dimethylbenzenesulfinamide
A
methyl p-toluene sulfinate
B
benzyl-methyl-amine
Conditions | Yield |
---|---|
With tetraethylammonium tosylate Electrochemical reaction; reticulated vitreous carbon anode; Pt cathode; | A 80% B n/a |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 3h; Inert atmosphere; | 100% |
With triethylamine In tetrahydrofuran at 0℃; | 74% |
benzyl-methyl-amine
2-chloro-ethanol
2-(N-benzyl-N-methyl)amino-1-ethanol
Conditions | Yield |
---|---|
In acetonitrile Heating; | 100% |
With potassium carbonate; potassium iodide In acetonitrile for 48h; Heating / reflux; | 63% |
With toluene | |
at 110℃; im Rohr; |
Conditions | Yield |
---|---|
With 4-hydroperoxy-5-ethyl-3-methyllumiflavine In tert-butyl alcohol at 30℃; Rate constant; | 100% |
Stage #1: benzyl-methyl-amine With REM resin In N,N-dimethyl-formamide at 20℃; for 20h; Michael addition; Stage #2: With 3-chloro-benzenecarboperoxoic acid In chloroform at 20℃; for 12h; Cope elimination; | 47% |
With dihydrogen peroxide | |
Multi-step reaction with 2 steps 1: tetrahydrofuran / 25 °C 2: mCPBA; DBU / methanol; H2O / 25 °C View Scheme | |
Multi-step reaction with 2 steps 1: dipotassium hydrogenphosphate; dicyclohexyl phthalate / N,N-dimethyl-formamide / 10 h / 20 °C / Inert atmosphere 2: diisobutylaluminium hydride / dichloromethane; hexane / 0.25 h / 0 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; for 24h; | 100% |
imidazolium-based polymer supported Gd(OTf)3 at 20℃; for 1h; Michael addition; | 96% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; for 4h; aza-Michael addition; | 95% |
benzyl-methyl-amine
phenylacetyl chloride
N-benzyl-N-methyl-2-phenylacetamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 14h; Inert atmosphere; | 100% |
In diethyl ether | |
With sodium hydroxide In dichloromethane for 1h; Yield given; | |
With TEA; N-methylglycine potassium salt 1.) DMF, 4 h; 2.) DMF, 0.5 h; Yield given. Multistep reaction; |
formaldehyd
potassium cyanide
benzyl-methyl-amine
(N-benzyl-N-methylamino)acetonitrile
Conditions | Yield |
---|---|
With hydrogenchloride for 16h; Ambient temperature; | 100% |
isopropyl S-3,6-diisopropylpyrazin-2-ylthiolcarbonate
benzyl-methyl-amine
propan-2-yl benzyl(methyl)carbamate
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 0.166667h; Ambient temperature; | 100% |
isobutyl S-3,6-diisopropylpyrazin-2-ylthiolcarbonate
benzyl-methyl-amine
isobutyl benzyl(methyl)carbamate
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 0.166667h; Ambient temperature; | 100% |
2-t-butoxycarbonyloxy-3,6-diisopropylpyrazine
benzyl-methyl-amine
tert-butyl N-benzyl-N-methylcarbamate
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 0.166667h; Ambient temperature; | 100% |
benzyl-methyl-amine
2-phenyl-1-(2-thioxothiazolidin-3-yl)ethan-1-one
N-benzyl-N-methyl-2-phenylacetamide
Conditions | Yield |
---|---|
In dichloromethane for 0.0166667h; Ambient temperature; | 100% |
4-(bromomethyl)benzene-1-sulfonyl chloride
benzyl-methyl-amine
N-benzyl-4-(bromomethyl)-N-methylbenzenesulfonamide
Conditions | Yield |
---|---|
With triethylamine In diethyl ether at 20℃; for 3h; Substitution; | 100% |
In dichloromethane at 20℃; | 20% |
chloroacetonitrile
benzyl-methyl-amine
(N-benzyl-N-methylamino)acetonitrile
Conditions | Yield |
---|---|
100% | |
Stage #1: benzyl-methyl-amine With triethylamine In acetone at 20℃; for 0.166667h; Stage #2: chloroacetonitrile In acetone at 20℃; Inert atmosphere; | 99% |
With potassium carbonate; potassium iodide In acetone at 20℃; for 24h; Reflux; | 93% |
hydratropic acid
benzyl-methyl-amine
Conditions | Yield |
---|---|
With O,O'-di(2-pyridyl) thiocarbonate; dmap In diethyl ether at 20℃; | 100% |
With dmap; 2-methyl-6-nitrobenzoic anhydride In dichloromethane at 20℃; | 93% |
benzyl-methyl-amine
3-Phenylpropionic acid
N-benzyl-N-methyl-3-phenylpropionamide
Conditions | Yield |
---|---|
With 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride In methanol at 20℃; for 3h; | 100% |
With tetrakis(2-methylimidazol-1-yl)silane In tetrahydrofuran at 20℃; for 12h; | 99% |
Stage #1: 3-Phenylpropionic acid With 1,1'-carbonyldioxydi[2(1H)-pyridone] In dichloromethane at 20℃; for 1h; Stage #2: benzyl-methyl-amine In dichloromethane at 20℃; | 97% |
benzyl-methyl-amine
5-bromomethyl-1-(2,6-difluorobenzyl)-6-(4-nitrophenyl)-3-phenylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione
5-(N-benzyl-N-methylaminomethyl)-1-(2,6-difluorobenzyl)-6-(4-nitrophenyl)-3-phenylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N-methyl-acetamide | 100% |
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide | 100% |
With N-ethyl-N,N-diisopropylamine In N-methyl-acetamide | 100% |
benzyl-methyl-amine
wortmannin
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; | 100% |
crotonic acid methyl ester
benzyl-methyl-amine
methyl 3-(N-benzyl-N-methylamino)-3-methylpropionate
Conditions | Yield |
---|---|
100% | |
100% | |
100% | |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 50℃; for 14h; aza-Michael addition; | 77% |
benzyl-methyl-amine
Chloroacetic anhydride
N-benzyl-N-methyl-α-chloroacetamide
Conditions | Yield |
---|---|
With dmap In tetrahydrofuran at 20℃; for 0.166667h; | 100% |
6-(2-hydroxyethyl)-2-(methylthio)-4-pyrimidinyl 4-methyl-1-benzenesulfonate
benzyl-methyl-amine
Conditions | Yield |
---|---|
In tetrahydrofuran at 70℃; for 48h; | 100% |
1,2,3-Benzotriazole
formaldehyd
benzyl-methyl-amine
N-((1H-benzo[d][1,2,3]triazol-1-yl)methyl)-N-methyl-1-phenylmethanamine
Conditions | Yield |
---|---|
In methanol; diethyl ether; water Reflux; | 100% |
In methanol; water at 50℃; for 15h; | 85% |
In water |
8-bromooctanol
benzyl-methyl-amine
8-(N-Benzyl-N-methylamino)octan-1-ol
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 35℃; for 7h; | 100% |
With potassium carbonate In acetonitrile at 35 - 40℃; for 5h; | 79% |
With potassium carbonate In acetonitrile at 35 - 40℃; for 5h; | 79% |
Stage #1: 8-bromooctanol; benzyl-methyl-amine With potassium carbonate In acetonitrile at 35℃; for 7h; Stage #2: With 2-pyrrolidinon In tert-butyl methyl ether |
3-benzyl-6-bromo-2-methoxyquinoline
3-chloro-1-(naphthalen-1-yl)-propan-1-one
benzyl-methyl-amine
2-(N-methylbenzyl)aminoethyl-1-naphthylketone
Conditions | Yield |
---|---|
In acetonitrile at 80℃; for 2h; | 100% |
1H-pyrazole-1-carboximidamide hydrochloride
benzyl-methyl-amine
N-benzyl-N-methylguanidine hydrochloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; | 100% |
With N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide) at 20℃; | 100% |
3-chloro-1-(naphthalen-1-yl)-propan-1-one
benzyl-methyl-amine
2-(N-methylbenzyl)aminoethyl-1-naphthylketone
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 80℃; for 2h; | 100% |
With potassium carbonate In acetonitrile at 80℃; for 2h; | 100% |
In acetonitrile at 80℃; for 2h; | |
In acetonitrile at 80℃; for 2h; |
benzyl-methyl-amine
3-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester
tert-butyl 3-(benzyl(methyl)amino)pyrrolidine-1-carboxylate
Conditions | Yield |
---|---|
Stage #1: benzyl-methyl-amine; 3-oxo-pyrrolidine-1-carboxylic acid tert-butyl ester With sodium tris(acetoxy)borohydride In dichloromethane at 0 - 20℃; for 2h; Stage #2: With water; sodium hydrogencarbonate In dichloromethane | 100% |
With sodium tris(acetoxy)borohydride; acetic acid In dichloromethane at 20℃; Inert atmosphere; | 76% |
With sodium tris(acetoxy)borohydride; acetic acid In dichloromethane at 25℃; |
benzyl-methyl-amine
5-bromomethyl-1-(2,6-difluorobenzyl)-6-(4-nitrophenyl)-3-phenylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione
B
5-(N-benzyl-N-methylaminomethyl)-1-(2,6-difluorobenzyl)-6-(4-nitrophenyl)-3-phenylthieno[2,3-d]pyrimidine-2,4(1H,3H)-dione
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine In N-methyl-acetamide | A n/a B 100% |
With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine In N-methyl-acetamide | A n/a B 100% |
Conditions | Yield |
---|---|
With dirhodium tetraacetate; carbon monoxide In tetrahydrofuran; water at 140℃; under 15001.5 Torr; for 12h; Autoclave; | 100% |
With formic acid; 4-methoxy-N-(1-(naphthalen-2-yl)ethylidene)aniline; sodium formate In water at 80℃; for 2h; pH=4.8; Sealed tube; Inert atmosphere; | 98% |
With cobalt(II) phthalocyanine; diphenylsilane In ethanol at 70℃; for 12h; chemoselective reaction; | 93% |
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