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Cas:104-46-1
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquirySpecifications CAS No.: 104-46-1 Other Names: / MF: C10H12O EINECS No.: 224-052-0 Place of Origin: Shaanxi, China (Mainland)
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inquiryHebei yanxi chemical co., LTD is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carb
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inquiryCis-Anethol CAS 104-46-1 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additives, Fine chemicals in distributing th
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inquiryAnethole Product Name Anethole Content ≥99.5% Molecular formula C10H12O CAS No 104-46-1 12002-40-3 EINEC 203-205-5
Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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High purity CAS 104-46-1 cis-Anethol in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business relationships wi
Cas:104-46-1
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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inquiryAppearance:Colorless to light yellow liquid Storage:R.T Package:25kg/Barrel Application:Food flavor Transportation:Express/Sea/Air Port:Any port in China
Cas:104-46-1
Min.Order:25 Kilogram
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inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
Cas:104-46-1
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
cis-Anethol CAS:104-46-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
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Min.Order:1 Gram
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Type:Lab/Research institutions
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Min.Order:20 Metric Ton
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:104-46-1
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
cis-Anethol CAS 104-46-1 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality control system
Cas:104-46-1
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Conditions | Yield |
---|---|
With bis(triphenylphosphine)nickel(II) chloride In diethyl ether for 12h; Heating; | 90% |
Conditions | Yield |
---|---|
With organo lithium reagent In hexane at 20℃; for 24h; | A 80% B 86% |
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; cobalt acetylacetonate In tetrahydrofuran at 15 - 20℃; for 0.25h; | 80% |
Conditions | Yield |
---|---|
With C68H72Cl2N6NiP2 In tetrahydrofuran at 50℃; for 12h; Inert atmosphere; | 77% |
1-propenylboronic acid
4-chloromethoxybenzene
anethole
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium (0); caesium carbonate In 1,4-dioxane for 24h; Suzuki-Miyaura cross-coupling; Heating; | 58% |
(E)-methyl 3-(3-bromo-4-hydroxyphenyl)acrylate
A
Estragole
B
trans-2-bromo-4-(3-hydroxypropen-1-yl)phenol
C
anethole
Conditions | Yield |
---|---|
With aluminium hydride In diethyl ether for 1h; Ambient temperature; Yields of byproduct given; | A n/a B 48% C n/a |
ethyl p-methoxycinnamate
A
Estragole
B
p-methoxycinnamyl alcohol
C
anethole
Conditions | Yield |
---|---|
With aluminium hydride In diethyl ether for 0.5h; Ambient temperature; Yields of byproduct given; | A n/a B 47% C n/a |
anethole
Conditions | Yield |
---|---|
Stage #1: carbonic acid 1-(4-methoxy-phenyl)-allyl ester methyl ester With bis(1,5-cyclooctadiene)diiridium(I) dichloride; dibenzyl ether; N-isopropylidene-N’-2-nitrobenzenesulfonyl hydrazine In acetonitrile for 18h; Sealed tube; Inert atmosphere; Glovebox; Stage #2: With acetic acid In tetrahydrofuran; 2,2,2-trifluoroethanol; water for 2h; Sealed tube; Inert atmosphere; Glovebox; regioselective reaction; | 45% |
Conditions | Yield |
---|---|
With (2,2'-bipyridine)nickel(II) dibromide; tetrabutylammonium tetrafluoroborate In N,N-dimethyl-formamide at 70℃; i = 250 mA, nickel-sponge cathode; | 44% |
Estragole
A
1-methoxy-4-(4-(p-methoxyphenyl)but-3-enyl)benzene
B
4,4'-dimethoxystilbene
C
1,3-bis(4-methoxyphenyl)prop-1-ene
D
anethole
Conditions | Yield |
---|---|
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride In toluene at 40℃; Inert atmosphere; Schlenk technique; | A n/a B n/a C n/a D n/a E 41% |
Conditions | Yield |
---|---|
With trityl tetrafluoroborate In dichloromethane at -78℃; for 30h; | 15% |
Conditions | Yield |
---|---|
With infusorial earht at 500℃; | |
iridium(III) chloride; β‐cyclodextrin In water at 95℃; for 2.5h; | |
PEG-KOH In potassium hydroxide; toluene at 65℃; Mechanism; Rate constant; variations of stirring rate, aqueous KOH concentration, and catalyst (7-130 oxyethylene units / PEG monomethyl, dimethyl, and dibenzyl ethers), other temp.; activation energy; |
acetic anhydride
A
N,N-dimethyl acetamide
B
1-(4-methoxyphenyl)prop-1-yl acetate
C
anethole
Conditions | Yield |
---|---|
With sodium proprionate |
propene
(4-Methoxyphenyl)mercuric acetate
A
Estragole
B
1-isopropenyl-4-methoxybenzene
C
anethole
Conditions | Yield |
---|---|
(i) Pd(OAc)2, MeCN, (ii) /BRN= 1696878/; Multistep reaction; |
Conditions | Yield |
---|---|
With H2O2 or O2; copper dichloride; palladium dichloride In ethanol |
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane Yield given; | |
Stage #1: ethyltriphenylphosphonium bromide With potassium tert-butylate In tetrahydrofuran at 0℃; for 0.5h; Stage #2: 4-methoxy-benzaldehyde In tetrahydrofuran at 20℃; for 12h; |
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 1h; | 52 % Chromat. |
A
1-isopropenyl-4-methoxybenzene
B
4-methoxyphenylcyclopropane
C
anethole
Conditions | Yield |
---|---|
at 160℃; Yield given. Yields of byproduct given; |
anethole
anethole
Conditions | Yield |
---|---|
With sulfuric acid durch Destillation; |
anethole
Conditions | Yield |
---|---|
With potassium carbonate | |
With pyridine |
anethole
Conditions | Yield |
---|---|
With potassium hydroxide |
Conditions | Yield |
---|---|
at 500℃; |
1-(4-methoxyphenyl)prop-1-yl acetate
anethole
Conditions | Yield |
---|---|
With C28H18Co(1-)*K(1+)*2C4H10O2; hydrogen In toluene at 60℃; under 7500.75 Torr; for 24h; chemoselective reaction; | 99% |
With sodium hydrogen telluride In ethanol Heating; overnight; | 94% |
With formic acid; Pd(SIPr)(PCy3) In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With iodic acid; potassium bromide In dichloromethane; water at 20℃; for 0.166667h; | 99% |
With periodic acid; potassium bromide In dichloromethane; water at 20℃; for 0.133333h; | 98% |
With diethyl ether; bromine |
2-(2-phenylethynyl)-1,4-benzoquinone
anethole
2-(4-methoxyphenyl)-2-methyl-7-(phenylethynyl)-2,3-dihydrobenzofuran-5-ol
Conditions | Yield |
---|---|
With bismuth(lll) trifluoromethanesulfonate In acetonitrile at 0℃; Inert atmosphere; Schlenk technique; | 99% |
Conditions | Yield |
---|---|
Stage #1: propionic acid With 2,6-dimethylpyridine; 10-methyl-9-(2,4,6-trimethylphenyl) acridinium tetrafluoroborate; thiophenol In 1,2-dichloro-ethane at 0 - 23℃; for 0.25h; Inert atmosphere; Stage #2: anethole In 1,2-dichloro-ethane for 30h; Inert atmosphere; Irradiation; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
Stage #1: isobutyric Acid With 2,6-dimethylpyridine; 10-methyl-9-(2,4,6-trimethylphenyl) acridinium tetrafluoroborate; thiophenol In 1,2-dichloro-ethane at 0 - 23℃; for 0.25h; Inert atmosphere; Stage #2: anethole In 1,2-dichloro-ethane for 62h; Inert atmosphere; Irradiation; regioselective reaction; | 99% |
Togni's reagent II
anethole
3,3,3-trifluoro-1-(4-methoxyphenyl)-2-methylpropan-1-one
Conditions | Yield |
---|---|
With tris[2-phenylpyridinato-C2,N]iridium(III); dimethyl sulfoxide at 20℃; for 2h; Irradiation; Green chemistry; | 99% |
With N9,N9,N10,N10-tetrakis(4-(tert-butyl)phenyl)anthracene-9,10-diamine; dimethyl sulfoxide In dichloromethane at 20℃; for 3h; Irradiation; | 75% |
With dmap; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; magnesium sulfate In dimethyl sulfoxide at 20℃; for 48h; Solvent; Reagent/catalyst; Inert atmosphere; Irradiation; | 40% |
anethole
isoprene
(1SR,2SR)-4'-methoxy-2,4-dimethyl-1,2,3,6-tetrahydro-1,1'-biphenyl
Conditions | Yield |
---|---|
With N,N’,N’’-tris(3,5-bis(trifluoromethyl)phenyl)thiophosphoramide; [Ru(4,4'-bis(trifluoromethyl)-2,2'-bipyridine)3](3,5-bis(trifluoromethyl)benzenesulfonate)2 In dichloromethane at 20℃; for 0.333333h; Quantum yield; Reagent/catalyst; Diels-Alder Cycloaddition; Inert atmosphere; Irradiation; | 99% |
With tris(4-bromophenyl)ammoniumyl hexafluoroantimonate In dichloromethane for 1h; Quantum yield; Reagent/catalyst; Diels-Alder Cycloaddition; Irradiation; | 35% |
Conditions | Yield |
---|---|
With copper(ll) bromide In acetonitrile at 20℃; for 2h; Schlenk technique; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With copper(ll) bromide In acetonitrile at 20℃; for 2h; Schlenk technique; Inert atmosphere; | 99% |
anethole
2-(4-methoxyphenyl)-3-methyloxirane
Conditions | Yield |
---|---|
With 3,3-dimethyldioxirane In acetone for 0.666667h; Ambient temperature; | 98% |
With dihydrogen peroxide; sodium hydrogencarbonate In acetonitrile | |
With oxidovanadium(IV)-β-octabromo-meso-tetrakis(2,6-dibromo-3,5-dimethoxyphenyl)porphyrin; dihydrogen peroxide; sodium hydrogencarbonate In water; acetonitrile at 60℃; for 0.5h; Catalytic behavior; Reagent/catalyst; |
Conditions | Yield |
---|---|
With tris(1,10-phenanthroline)iron(III) tris(hexafluorophosphate) In 1,2-dichloro-ethane at 0℃; for 6h; | 98% |
Conditions | Yield |
---|---|
Lewatit SP 120 (acid form) In 1,4-dioxane at 60℃; for 0.5h; | 97% |
With sulfuric acid |
4,4-dimethoxycyclohexa-2,5-dienone
anethole
2,3-dihydro-5-methoxy-2-(4-methoxyphenyl)-3-methylbenzofuran
Conditions | Yield |
---|---|
With polystyrene-supported perfluorobenzoic acid In dichloromethane; 1,1,1,3',3',3'-hexafluoro-propanol at 0℃; chemoselective reaction; | 97% |
With 1,1,1,3',3',3'-hexafluoro-propanol; Pentafluorobenzoic acid In dichloromethane at 25℃; for 0.166667h; | 93% |
Conditions | Yield |
---|---|
Stage #1: butyric acid With 2,6-dimethylpyridine; 10-methyl-9-(2,4,6-trimethylphenyl) acridinium tetrafluoroborate; thiophenol In 1,2-dichloro-ethane at 0 - 23℃; for 0.25h; Inert atmosphere; Stage #2: anethole In 1,2-dichloro-ethane for 48h; Inert atmosphere; Irradiation; regioselective reaction; | 97% |
Conditions | Yield |
---|---|
With copper(ll) bromide In acetonitrile at 20℃; for 2h; Solvent; Schlenk technique; Inert atmosphere; | 97% |
anethole
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
(S)-2-(1-(4-methoxyphenyl)propyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
Conditions | Yield |
---|---|
With C24H31Cl2FeN3O2; sodium triethylborohydride In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 97% |
With C26H28N4O; cobalt(II) acetate In diethyl ether at 20℃; for 18h; enantioselective reaction; | 87% |
C12H12O2
anethole
7-(3,3-dimethylbut-1-ynyl)-2-(4-methoxyphenyl)-2-methyl-2,3-dihydrobenzofuran-5-ol
Conditions | Yield |
---|---|
With bismuth(lll) trifluoromethanesulfonate In acetonitrile at 0℃; Inert atmosphere; Schlenk technique; | 96% |
Conditions | Yield |
---|---|
With C18H22N2O; copper(II) bis(trifluoromethanesulfonate) In toluene at -80℃; for 36h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 96% |
anethole
2-(4-methoxyphenyl)propanal
Conditions | Yield |
---|---|
With iodine; silver(l) oxide In 1,4-dioxane; water for 4h; Ambient temperature; | 95% |
With N-iodo-succinimide; water; cetyltrimethylammonim bromide In 1,4-dioxane at 20 - 105℃; for 0.333333h; Microwave irradiation; | 78% |
With N-Bromosuccinimide; water; cetyltrimethylammonim bromide In dimethyl sulfoxide at 200℃; for 0.2h; Microwave irradiation; | 65% |
anethole
A
2-(4-methoxyphenyl)-3-methyloxirane
B
2-(4-methoxyphenyl)propanal
Conditions | Yield |
---|---|
With iodine; silver(l) oxide In 1,4-dioxane; water for 4h; Product distribution; Ambient temperature; various bases, solvents and temp.; | A n/a B 95% |
With sodium hydroxide; iodine for 2h; Ambient temperature; | A 10 % Chromat. B n/a |
anethole
1,2-bis(4-methoxyphenyl)ethene
Conditions | Yield |
---|---|
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride In neat (no solvent) at 90℃; for 1.33333h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With copper(ll) bromide In acetonitrile at 20℃; for 2h; Schlenk technique; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With C18H22N2O; copper(II) bis(trifluoromethanesulfonate) In toluene at -80℃; for 36h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 95% |
Conditions | Yield |
---|---|
With C18H22N2O; copper(II) bis(trifluoromethanesulfonate) In toluene at -80℃; for 36h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 95% |
Conditions | Yield |
---|---|
With aluminum oxide; potassium permanganate In dichloromethane at 20℃; for 4h; | 94% |
With disodium hydrogenphosphate; oxygen; cobalt(II) acetate In methanol at 50℃; for 6h; | 89.9% |
With oxygen; ozone In water; ethyl acetate at 20℃; for 1.66667h; | 81.7% |
Conditions | Yield |
---|---|
Stage #1: benzoic acid With 2,6-dimethylpyridine; 10-methyl-9-(2,4,6-trimethylphenyl) acridinium tetrafluoroborate; thiophenol In 1,2-dichloro-ethane at 0 - 23℃; for 0.25h; Inert atmosphere; Stage #2: anethole In 1,2-dichloro-ethane for 30h; Inert atmosphere; Irradiation; regioselective reaction; | 94% |
Conditions | Yield |
---|---|
With trimethylsilylazide; water; dimethylglyoxal In toluene at 20℃; for 8h; Inert atmosphere; Schlenk technique; | 94% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide In water; acetonitrile at 100℃; for 2h; | 93% |
Conditions | Yield |
---|---|
With C18H22N2O; copper(II) bis(trifluoromethanesulfonate) In toluene at -80℃; for 36h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 93% |
anethole
2-bromo-1-(4-methoxyphenyl)-1-propanone
Conditions | Yield |
---|---|
With N-Bromosuccinimide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide at 25 - 35℃; for 0.3h; regioselective reaction; | 92% |
With dipotassium peroxodisulfate; potassium bromide In water at 60℃; for 12h; Green chemistry; | 21% |
With bromine; ethyl acetate for 2h; | 3.9% |
Multi-step reaction with 2 steps 1: absolute diethyl ether; bromine 2: CrO3; glacial acetic acid View Scheme |
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