Jinan Finer Chemical Co., Ltd
Product Description Name 4-Bromoanisole CAS 104-92-7 Assay 99% Appearance C
Dayang Chem (Hangzhou) Co.,Ltd.
DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:104-92-7
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryHenan Allgreen Chemical Co.,Ltd
high quality Appearance:Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Intermediates Transportation:by air or by sea Port:Shanghai, Qingdao Port
Ality Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Hebei yanxi chemical co.,LTD.
Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
Cas:104-92-7
Min.Order:1 Metric Ton
FOB Price: $1.0 / 2.0
Type:Trading Company
inquiryHenan Tianfu Chemical Co., Ltd.
TIANFUCHEM--104-92-7--High purity 4-Bromoanisole factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business
Cas:104-92-7
Min.Order:1 Metric Ton
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryHenan Sinotech Import&Export Corporation
Product Name 4-bromoanisole CAS No 104-92-7 Formula C7H7BrO Molecular Weight 187.03400
Cas:104-92-7
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiryHubei Langyou International Trading Co., Ltd
Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is
LIDE PHARMACEUTICALS LIMITED
Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:104-92-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryChangchun Artel lmport and Export trade company
Product Detail Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,
Cas:104-92-7
Min.Order:20 Metric Ton
Negotiable
Type:Trading Company
inquiryTriumph International Development Limilted
Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
Wuhan Zenuo Biological Medicine Technology Co Ltd
Product Name: 4-Bromoanisole Synonyms: Bromophenol methyl ether;4-Bromoanisole,98%;4-Bromoanisole,1-Bromo-4-methoxybenzene;Of BroMoanisole;p-BroMophenol Methyl ether;4-BroMoanisole, 98% 100ML;4-BROMOANISOLE FOR SYNTHESIS 100 ML;4-BROMOANISOLE F
Cas:104-92-7
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:104-92-7
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Afine Chemicals Limited
Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Hangzhou Lingrui Chemical Co.,Ltd.
4-BromoanisoleAppearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:according to customers' requirements Application:Used for research and industrial manufacture. Transpor
HANGZHOU YUNUO CHEMICAL CO.,LTD
Superior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:In Room Temperature Package:25kg/drum, or as per your request. Application:For medicine , pesticide intermediates Transportation:as per your request. Po
Henan Wentao Chemical Product Co., Ltd.
We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:104-92-7
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquirySiwei Development Group Ltd.
Product name: P-Bromoanisole CAS No.：104-92-7 Molecule Formula：C7H7BrO Molecule Weight：187.03 Purity: 99.0% Package: 200kg/drum Description：Light yellow liquid Manufacture Standards：Enterprise Standard TESTING ITEM
Cas:104-92-7
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryHangzhou Zhongqi chem Co.,Ltd.
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
Hunan chemfish Pharmaceutical co.,Ltd
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
SAGECHEM LIMITED
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
GIHI CHEMICALS CO.,LIMITED
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
JINHUA HUAYI CHEMICAL CO., LTD.
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Wuhan Fortuna Chemical Co.,Ltd
1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers160.Safe and fa
Hangzhou ZeErRui Chemical Co., Ltd.
Hangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech bar
Cas:104-92-7
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryAecochem Corp.
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Enke Pharma-tech Co.,Ltd. （Cangzhou, China ）
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Synthetic route
| Conditions | Yield |
|---|---|
| With benzyltriphenylphosphonium peroxodisulfate; potassium bromide In acetonitrile for 3.5h; Heating; | 100% |
| With Selectfluor; sodium bromide In acetonitrile at 20℃; for 21h; | 100% |
| With bis[1-methyl-3-(3-sulfopropyl)imidazolium] hexafluorotitanate; dihydrogen peroxide; sodium bromide In water at 25℃; for 3h; Reagent/catalyst; Concentration; Solvent; Temperature; Green chemistry; | 100% |
| Conditions | Yield |
|---|---|
| With N,N'-dimethylimidazolium-2-carboxylate In acetonitrile at 160℃; for 2h; Microwave irradiation; Green chemistry; | 100% |
| With layered double hydroxide - supported L-methionine at 180℃; for 6h; Autoclave; chemoselective reaction; | 95% |
| With magnesium oxide In N,N-dimethyl-formamide at 170℃; for 0.5h; Microwave irradiation; Green chemistry; | 95% |
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide In dichloromethane at 20℃; for 0.166667h; | 100% |
| With N-Bromosuccinimide In acetonitrile at 80℃; for 12h; | 96% |
| With tetrabutylammomium bromide; copper(ll) bromide In water at 100℃; Sealed tube; | 85% |
| With N-Bromosuccinimide In acetonitrile at 81℃; for 1.5h; | 82% |
| With 1,10-Phenanthroline; oxygen; potassium bromide; copper(ll) bromide In N,N-dimethyl-formamide at 130℃; for 20h; | 70% |
-
-
19231-06-2
4,4'-dimethoxy-diphenyliodonium bromide
-
-
104-92-7
1-bromo-4-methoxy-benzene
| Conditions | Yield |
|---|---|
| In benzene-d6 at 120℃; for 5h; Sealed tube; | 100% |
| Conditions | Yield |
|---|---|
| With lithium bromide monohydrate; [bis(acetoxy)iodo]benzene In 2,2,2-trifluoroethanol at 20℃; for 0.166667h; regiospecific reaction; | 100% |
| Conditions | Yield |
|---|---|
| With potassium carbonate In diethyl ether; acetone | 99.5% |
| Stage #1: 4-bromo-phenol With potassium carbonate In acetone for 0.25h; Stage #2: dimethyl sulfate In acetone for 12h; Reflux; | 95% |
| With aluminum oxide; potassium hydroxide for 6h; microwave irradiation; | 87% |
| With sodium hydroxide In diethyl ether for 2h; Heating; | 59% |
-
-
100-66-3
methoxybenzene
-
A
-
104-92-7
1-bromo-4-methoxy-benzene
-
B
-
578-57-4
2-bromoanisole
-
C
-
21702-84-1
2,4-dibromoanisole
| Conditions | Yield |
|---|---|
| With bromine; tetramethylammonium bromide In liquid sulphur dioxide at -23℃; Rate constant; Product distribution; Thermodynamic data; in H2O at 25 deg C, NaBr, HClO4; ΔH (excit), -ΔS (excit); | A 98.99% B 0.56% C 0.43% |
| With (CH3)4Br In liquid sulphur dioxide at -23℃; Kinetics; Thermodynamic data; Product distribution; ΔH(excit.); ΔS(excit.); | A 98.99% B 0.56% C 0.43% |
| With (CH3)4Br In liquid sulphur dioxide at -23℃; | A 98.99% B 0.56% C 0.43% |
| Conditions | Yield |
|---|---|
| With potassium phosphate; tetrabuthylammonium tribromide In acetonitrile at 100℃; for 16h; | 98% |
| With 2,2'-azobis(isobutyronitrile); Bromotrichloromethane; 2,2’-disulfanediyldipyridine-1-oxide 2.) 100 deg C; Yield given. Multistep reaction; | |
| With potassium phosphate; tetra-N-butylammonium tribromide In acetonitrile at 100℃; for 16h; |
| Conditions | Yield |
|---|---|
| In methanol for 0.4h; Methylation; | 98% |
| Conditions | Yield |
|---|---|
| With sodium chlorite; silica gel; manganese(III) acetylacetonate; sodium bromide In dichloromethane at 25℃; for 2h; | A 97% B 3% |
| With tetraethylammonium chloride; tetraethylammonium bromide Product distribution; 1.) CH2Cl2, RT, 1 h, electrolysis, 2.) CH2Cl2, RT, 24 h; other halogenating agents; other benzene derivatives and olefins; |
| Conditions | Yield |
|---|---|
| With Oxone; potassium bromide In methanol at 20℃; for 1h; | A 97% B 2% |
| With Oxone; potassium bromide In acetonitrile at 20℃; for 24h; | A 84% B 15% |
| With PyHBrCl2 In methanol at 20℃; for 0.0833333h; | A 78% B 18% |
| Conditions | Yield |
|---|---|
| With dibenzo-18-crown-6; potassium bromide; copper(ll) bromide; 1,10-Phenanthroline; copper(I) bromide In acetonitrile at 20℃; for 0.333333h; Sandmeyer bromination; | 97% |
| With dibenzo-18-crown-6; N,N,N,N,-tetramethylethylenediamine; potassium bromide; copper(I) bromide; copper(ll) bromide In acetonitrile at 20℃; for 1h; Sandmeyer Reaction; | 90% |
| With potassium bromide In acetonitrile at 20℃; for 1h; Sandmeyer Reaction; Inert atmosphere; | 87% |
| With (triphenylphosphine)gold(I) chloride; sodium bromide In acetonitrile at 50℃; for 5h; Sandmeyer Reaction; | 67 %Chromat. |
| With Bromotrichloromethane; tetrabutylammonium perchlorate In N,N-dimethyl-formamide at 20℃; for 2h; Sandmeyer Reaction; Electrochemical reaction; | 55 %Chromat. |
| Conditions | Yield |
|---|---|
| Stage #1: 4-bromo-phenol With potassium carbonate In acetone for 0.166667h; Stage #2: methyl iodide In acetone for 16h; Reflux; | 95% |
| With potassium carbonate In acetonitrile at 20 - 50℃; for 6h; | 84% |
| With sodium hexamethyldisilazane In tetrahydrofuran at 20℃; for 22h; Inert atmosphere; | 83% |
-
-
70744-47-7
(p-methoxyphenyl)tri-n-butylstannane
-
-
104-92-7
1-bromo-4-methoxy-benzene
| Conditions | Yield |
|---|---|
| With hydrogenchloride; chloroamine-T; sodium bromide In ethanol; water at 0℃; for 0.25h; | 95% |
-
-
128-08-5
N-Bromosuccinimide
-
-
171364-79-7
2-(4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
-
-
104-92-7
1-bromo-4-methoxy-benzene
| Conditions | Yield |
|---|---|
| In N,N-dimethyl-formamide at 20℃; for 14h; | 95% |
-
-
171364-79-7
2-(4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
-
-
104-92-7
1-bromo-4-methoxy-benzene
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; for 14h; | 95% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
| Conditions | Yield |
|---|---|
| With tetra-N-butylammonium tribromide In tetrahydrofuran; water at 20℃; for 0.333333h; chemoselective reaction; | 94% |
| Conditions | Yield |
|---|---|
| With lithium bromide monohydrate; [bis(acetoxy)iodo]benzene In 2,2,2-trifluoroethanol at 20℃; for 0.166667h; Solvent; regiospecific reaction; | 91% |
| With bis(collidine)bromine(I) hexafluorophosphate In dichloromethane at 20℃; for 3h; | 70% |
| Conditions | Yield |
|---|---|
| With bis(collidine)bromine(I) hexafluorophosphate In dichloromethane at 20℃; for 1.5h; | A n/a B 91% |
-
-
106-41-2
4-bromo-phenol
-
-
4637-24-5
N,N-dimethyl-formamide dimethyl acetal
-
-
104-92-7
1-bromo-4-methoxy-benzene
| Conditions | Yield |
|---|---|
| In N,N-dimethyl-formamide at 140℃; for 0.5h; Microwave irradiation; | 89% |
-
-
67963-68-2
t-butyldimethylsilyl-4-bromophenol
-
-
74-88-4
methyl iodide
-
-
104-92-7
1-bromo-4-methoxy-benzene
| Conditions | Yield |
|---|---|
| With cesium fluoride In N,N-dimethyl-formamide for 12h; Ambient temperature; | 88% |
-
-
106-41-2
4-bromo-phenol
-
-
121-45-9
phosphorous acid trimethyl ester
-
-
104-92-7
1-bromo-4-methoxy-benzene
| Conditions | Yield |
|---|---|
| With boron trifluoride In diethyl ether for 0.0333333h; microwave irradiation; | 86% |
| Conditions | Yield |
|---|---|
| In methanol Product distribution; Heating; | 85% |
| In methanol at 110℃; for 0.5h; | 85% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
| Conditions | Yield |
|---|---|
| With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; for 4h; | 85% |
| Conditions | Yield |
|---|---|
| Stage #1: 4-methoxy-aniline With Bromotrichloromethane; sodium nitrite In dichloromethane; water at 23℃; for 0.0833333h; Sealed tube; Stage #2: With acetic acid In dichloromethane; water at 70℃; for 24h; Temperature; Sealed tube; | 84% |
| With N-Bromosuccinimide; sodium nitrite In N,N-dimethyl-formamide at 20℃; for 6h; | 80% |
| Stage #1: 4-methoxy-aniline With boron trifluoride diethyl etherate; lithium bromide In acetonitrile at 0℃; for 0.166667h; Stage #2: With tert.-butylnitrite In acetonitrile at 0 - 20℃; for 1h; | 80% |
| Conditions | Yield |
|---|---|
| With sodium methylate In N,N-dimethyl-formamide for 0.5h; Ambient temperature; | 84% |
| Conditions | Yield |
|---|---|
| Stage #1: 1,4-bromoiodobenzene With copper(l) iodide; 1,10-Phenanthroline; potassium hydroxide In water; dimethyl sulfoxide at 20 - 100℃; Inert atmosphere; Stage #2: methyl iodide With tetra-(n-butyl)ammonium iodide; potassium hydroxide In water; dimethyl sulfoxide at 20 - 100℃; Inert atmosphere; | 84% |
| Conditions | Yield |
|---|---|
| With bis(collidine)bromine(I) hexafluorophosphate In dichloromethane at 20℃; for 1.5h; | A n/a B 83% |
-
-
106-41-2
4-bromo-phenol
-
-
431-47-0
trifluoroacetic acid-methyl ester
-
-
104-92-7
1-bromo-4-methoxy-benzene
| Conditions | Yield |
|---|---|
| Stage #1: 4-bromo-phenol With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: trifluoroacetic acid-methyl ester In N,N-dimethyl-formamide for 10h; | 83% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
20938-43-6
(4-D)-Anisol
| Conditions | Yield |
|---|---|
| Stage #1: 1-bromo-4-methoxy-benzene With n-butyllithium In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; Stage #2: With d(4)-methanol In tetrahydrofuran at -78 - 0℃; Inert atmosphere; | 100% |
| With tetrahydrofuran-d8; 2,2'-azobis-(2,4-dimethylvaleronitrile); tri-n-butyl-tin hydride for 5h; Reflux; regioselective reaction; | 94% |
| With sodium amalgam; deuteromethanol for 2h; Heating; | 90% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
98273-59-7
4-bromo-2-iodo-anisole
| Conditions | Yield |
|---|---|
| Stage #1: 1-bromo-4-methoxy-benzene In tetrahydrofuran; hexane; pentane at -30℃; for 20h; Stage #2: With iodine In tetrahydrofuran; hexane; pentane at 20℃; for 1h; Further stages.; | 100% |
| With iodine; 1-(p-methylbenzenesulfonyloxy)-1,2-benziodoxol-3(1H)-one In acetonitrile for 16h; Ambient temperature; | 99% |
| With [bis(acetoxy)iodo]benzene; iodine In ethyl acetate at 60℃; for 5h; | 99% |
| Conditions | Yield |
|---|---|
| With n-butyllithium In tetrahydrofuran; hexane at 0 - 20℃; for 1h; Inert atmosphere; | 100% |
| Stage #1: 1-bromo-4-methoxy-benzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at -78 - 20℃; | 99% |
| Stage #1: 1-bromo-4-methoxy-benzene With n-butyllithium In tetrahydrofuran; hexane at -78℃; Inert atmosphere; Schlenk technique; Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at -78 - 20℃; for 18h; Inert atmosphere; Schlenk technique; | 96% |
| Conditions | Yield |
|---|---|
| With cis-(N,N'-bis(2,2-diethoxyethyl)imidazolin-2-ylidene)dichlorotriphenylphosphinepalladium(II); tetrabutylammomium bromide; potassium carbonate In N,N-dimethyl-formamide at 140℃; for 2h; Heck reaction; | 100% |
| With 1-naphthalenomethyl-3-benzylimidazolidinium chloride; palladium diacetate; potassium carbonate In water; N,N-dimethyl-formamide at 80℃; for 2h; Reagent/catalyst; Green chemistry; | 100% |
| With C180H144O4P8Pd4S4(4+)*4CF3O3S(1-); sodium acetate In N,N-dimethyl acetamide; water at 120℃; for 24h; Solvent; Reagent/catalyst; Temperature; Heck Reaction; Inert atmosphere; | 100% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
16419-60-6
2-Methylphenylboronic acid
-
-
92495-54-0
4'-methoxy-2-methylbiphenyl
| Conditions | Yield |
|---|---|
| With C31H26N6O4Pd; potassium carbonate In water at 100℃; for 3h; Suzuki-Miyaura coupling; | 100% |
| With C38H53Cl2N2O2PPd*CH2Cl2; tetrabutylammomium bromide; potassium hydroxide In water at 80℃; for 12h; Suzuki-Miyaura Coupling; Schlenk technique; | 100% |
| With potassium phosphate; (PdCl2)(2-pyridyl)-6-isopropyl cis piperidine complex In water; N,N-dimethyl-formamide at 110℃; for 2h; | 99% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
75467-36-6
5-O-(tert-butyldimethylsilyl)-2,3-O-isopropylidene-D-ribonolactone
-
-
115129-94-7, 115130-17-1
5-O-<(1,1-dimethylethyl)dimethylsilyl>-2,3-O-(1-methylethylidene)-1-C-(4-methoxyphenyl)-D-ribofuranose
| Conditions | Yield |
|---|---|
| With tert.-butyl lithium In tetrahydrofuran; pentane 1.) -78 to 0 deg C, 1 h, 2) -78 deg C, 6 h; | 100% |
| Conditions | Yield |
|---|---|
| With copper(l) iodide; N,N`-dimethylethylenediamine In 1,4-dioxane for 24h; Reflux; | 100% |
| With copper(l) iodide; trans-N,N'-dimethylcyclohexane-1,2-diamine; sodium iodide In acetonitrile at 100℃; for 1.25h; Buchwald's halogen exchange reaction; Inert atmosphere; Microwave irradiation; | 95% |
| With copper(I) oxide; L-proline; potassium iodide In ethanol at 110℃; for 30h; Schlenk technique; Inert atmosphere; Sealed tube; | 87% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
21702-84-1
2,4-dibromoanisole
| Conditions | Yield |
|---|---|
| With (CH3)4Br In liquid sulphur dioxide at -23℃; Rate constant; | 100% |
| With (CH3)4Br In liquid sulphur dioxide at -23℃; | 100% |
| With N-Bromosuccinimide; iodine In acetonitrile for 12h; Darkness; | 93% |
| Conditions | Yield |
|---|---|
| With hydrogen In methanol at 70℃; under 750.075 Torr; for 0.333333h; | 100% |
| With LiCrH4*2LiCl*2THF In tetrahydrofuran at 25℃; for 12h; | 98% |
| Stage #1: 1-bromo-4-methoxy-benzene With n-butyllithium In tetrahydrofuran; hexane at -58℃; for 0.000861111h; Stage #2: With methanol In tetrahydrofuran; hexane at -58℃; for 0.000436111h; | 92% |
| Conditions | Yield |
|---|---|
| With copper(l) iodide; 1,2-bis(diphenylphosphino)-1'-(diisopropylphosphino)-3',4-di-tert-butyl ferrocene; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) In N,N-dimethyl-formamide at 130℃; for 20h; Sonogashira cross-coupling; | 100% |
| With copper(l) iodide; ethanolamine; bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran; water at 60℃; for 24h; Sonogashira coupling; | 99% |
| With copper(l) iodide; triethylamine; tris(dibenzylideneacetone)dipalladium (0) In toluene at 20℃; Sonogashira coupling; | 98% |
| Conditions | Yield |
|---|---|
| With potassium carbonate; {1,3-di[(R)-1-PhEt]imidazolin-2-ylidene}(PPh3)PdI2 In xylene at 130℃; for 14h; Suzuki-Miyaura cross-coupling reaction; | 100% |
| With 1,2-bis(diphenylphosphino)-1'-(diisopropylphosphino)-3',4-di-tert-butyl ferrocene; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) In xylene at 130℃; for 20h; Suzuki cross-coupling; | 100% |
| With 1,4-diaza-bicyclo[2.2.2]octane; PEG-400; potassium carbonate; palladium diacetate at 110℃; for 2h; Suzuki-Miyaura cross-coupling reaction; | 100% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
141-32-2
acrylic acid n-butyl ester
-
-
173464-57-8, 40458-52-4, 121725-19-7
(E)-3-(4-methoxyphenyl)acrylic acid butyl ester
| Conditions | Yield |
|---|---|
| With 1,2-bis(diphenylphosphino)-1'-(diisopropylphosphino)-3',4-di-tert-butyl ferrocene; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) In N,N-dimethyl-formamide at 130℃; for 20h; Heck cross-coupling; | 100% |
| With phenyl carbamate; tetrabutylammomium bromide; potassium carbonate; palladium diacetate In N,N-dimethyl-formamide at 130℃; for 2h; Heck-type reaction; | 99% |
| With potassium carbonate; di-μ-acetato-bis[2-[bis(1,1-dimethylethyl)phosphino]-2-methylpropyl-C,P]dipalladium In ISOPROPYLAMIDE | 99.2% |
-
-
292638-84-7
styrene
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
1694-19-5
E-1-(phenyl)-2-(4'-methoxyphenyl)ethene
| Conditions | Yield |
|---|---|
| With potassium phosphate; palladium diacetate In N,N-dimethyl acetamide at 140℃; for 42h; Heck reaction; | 100% |
| With 1,3-bis-(2-ethoxybenzyl)-3,4,5,6-tetrahydropyrimidinium chloride; palladium diacetate; potassium carbonate In water; N,N-dimethyl-formamide at 80℃; for 4h; Heck reaction; stereoselective reaction; | 99% |
| With C34H26Cl2N10Pd; tetrabutylammomium bromide; sodium acetate at 120℃; for 12h; Reagent/catalyst; Heck Reaction; | 99% |
| Conditions | Yield |
|---|---|
| With (55)Pd068(44)Ni032; potassium carbonate In water at 50℃; for 5h; Catalytic behavior; Buchwald-Hartwig Coupling; | 100% |
| With sodium t-butanolate; 1-(2-di-tert-butylphosphinophenyl)-3,5-diphenyl-1H-pyrazole; tris(dibenzylideneacetone)dipalladium (0) In tert-Amyl alcohol at 85℃; | 99% |
| With potassium hydroxide; bis(tri-tert-butylphosphine)palladium(0); cetyltrimethylammonim bromide In water; toluene at 90℃; for 3h; | 99% |
| Conditions | Yield |
|---|---|
| With [(di-tert-butylneopentylphosphine)PdCl2]2; sodium t-butanolate In toluene at 22℃; for 5h; Inert atmosphere; | 100% |
| With C16H14N6O4Pd; potassium tert-butylate In acetonitrile at 82℃; for 2h; Schlenk technique; Reflux; | 93% |
| With sodium t-butanolate; palladium diacetate; 2'-hydroxy-2-di-cyclohexylphosphinobiphenyl-4'-sulfonic acid In N,N-dimethyl-formamide at 80℃; for 14.75h; | 82% |
| Conditions | Yield |
|---|---|
| With 1,1-Dimethylurea; ammonium chloride; LACTOSE; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenyl-arsane at 90℃; for 6h; Stille coupling; | 100% |
| With cesium fluoride; palladium(II) trifluoroacetate In 1,4-dioxane at 100℃; for 6h; Stille cross-coupling; | 99% |
| With potassium fluoride; tetrabutylammomium bromide; tris-(o-tolyl)phosphine; copper(I) oxide at 125 - 130℃; for 30h; Stille cross-coupling; | 96% |
| Conditions | Yield |
|---|---|
| With C27H22N4O2Pd; potassium acetate In N,N-dimethyl acetamide at 140℃; for 18h; Catalytic behavior; Schlenk technique; Inert atmosphere; | 100% |
| With palladium diacetate; potassium carbonate; tricyclohexylphosphine; Trimethylacetic acid In N,N-dimethyl-formamide at 180℃; for 0.5h; Inert atmosphere; Microwave irradiation; | 85% |
| With C24H22ClN3OPdSe; potassium carbonate; Trimethylacetic acid In dimethyl amine at 110℃; for 10h; Reagent/catalyst; regioselective reaction; | 84% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
106-49-0
p-toluidine
-
-
39253-43-5
N-(4-methylphenyl)-4-methoxyaniline
| Conditions | Yield |
|---|---|
| With di-tert-butyl(2,2-diphenyl-1-methyl-1-cyclopropyl)phosphine; bis(η3-allyl-μ-chloropalladium(II)); potassium tert-butylate In water at 20℃; Temperature; Buchwald-Hartwig Coupling; Inert atmosphere; | 100% |
| With di-tert-butyl(2,2-diphenyl-1-methyl-1-cyclopropyl)phosphine; bis(η3-allyl-μ-chloropalladium(II)); potassium tert-butylate In water at 20℃; for 21h; Inert atmosphere; Micellar solution; | 99% |
| With caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate In toluene at 110℃; for 144h; Buchwald-Hartwig amination; | 97% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
5720-05-8
4-methylphenylboronic acid
-
-
53040-92-9
4-(4-tolyl)anisole
| Conditions | Yield |
|---|---|
| With potassium carbonate; palladium dichloride In ethanol; water at 20℃; for 0.166667h; Suzuki-Miyaura reaction; | 100% |
| With sodium carbonate; polystyrene-supported N-heterocyclic carbene-Pd catalyst In N,N-dimethyl-formamide at 20℃; for 24h; Suzuki reaction; | 99% |
| With C28H38Cl2N2O6PdS2(2-)*2Na(1+); potassium carbonate In ethanol; water at 70℃; for 1.5h; Suzuki coupling; | 99% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
93-55-0
1-phenyl-propan-1-one
-
-
35572-38-4, 35572-40-8, 84839-92-9, 35572-39-5
2-(4-methoxyphenyl)-1-phenylpropan-1-one
| Conditions | Yield |
|---|---|
| With [(di-tert-butylneopentylphosphine)PdCl2]2; sodium t-butanolate In toluene at 22℃; for 5h; Inert atmosphere; | 100% |
| With diaminochlorophosphine ligand; sodium t-butanolate; [Pd(dibenzylideneacetone)2] In toluene at 105℃; for 24h; | 98% |
| With sodium t-butanolate; (1,1'-bis(di-tert-butylphosphino)ferrocene)PdCl2 In tetrahydrofuran at 20℃; | 97% |
| Conditions | Yield |
|---|---|
| Stage #1: 1-bromo-4-methoxy-benzene; tri-n-butyllithium magnesate complex In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: heptanal In tetrahydrofuran; hexane at -78℃; for 0.5h; Further stages.; | 100% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
13922-41-3
1-Naphthylboronic acid
-
-
27331-33-5
1-(4-methoxyphenyl)naphthalene
| Conditions | Yield |
|---|---|
| With di-tert-butyl(4-sulfonatobenzyl)phosphonium; palladium diacetate; sodium carbonate In water; acetonitrile at 50℃; Reagent/catalyst; Suzuki Coupling; Inert atmosphere; Glovebox; | 100% |
| With di-tert-butyl(4-sulfonatobenzyl)phosphonium; palladium diacetate; sodium carbonate In water; acetonitrile at 50℃; Reagent/catalyst; Suzuki Coupling; Inert atmosphere; Glovebox; | 100% |
| With C38H53Cl2N2O2PPd*CH2Cl2; tetrabutylammomium bromide; potassium hydroxide In water at 80℃; for 12h; Suzuki-Miyaura Coupling; Schlenk technique; | 100% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
5720-07-0
4-methoxyphenylboronic acid
-
-
2132-80-1
4,4'-Dimethoxybiphenyl
| Conditions | Yield |
|---|---|
| With air; potassium carbonate; [Pd(Cl)κ2N,C,-CH2C6H2(4,6-Me)2CH=NC6H3(2,6-iPr)2]2 In ethanol for 2h; Suzuki-Miyaura coupling reaction; Heating; | 100% |
| With sodium carbonate; palladium on activated charcoal In ethanol at 20℃; for 5h; Suzuki-Miyaura cross-coupling; | 100% |
| With potassium carbonate In water at 50℃; for 1h; Suzuki-Miyaura Coupling; Green chemistry; | 100% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
149104-90-5
4-acetylphenylboronic acid
-
-
13021-18-6
1-(4'-methoxy-biphenyl-4-yl)-ethanone
| Conditions | Yield |
|---|---|
| With sodium phosphate; palladium on activated charcoal In water; isopropyl alcohol at 20℃; for 48h; Suzuki-Miyaura coupling reaction; | 100% |
| With potassium carbonate In ethanol; water at 50℃; for 2.5h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 98% |
| With trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); potassium carbonate In water for 8h; Catalytic behavior; Suzuki-Miyaura Coupling; Sealed tube; Inert atmosphere; Reflux; | 97% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
98-80-6
phenylboronic acid
-
A
-
92-52-4
biphenyl
-
B
-
613-37-6
4-methoxylbiphenyl
| Conditions | Yield |
|---|---|
| With potassium hydroxide In toluene at 100℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | A n/a B 100% |
| With C34H28Cl2N2P2Pd(2+); potassium carbonate In isopropyl alcohol at 20℃; for 4h; Reagent/catalyst; Suzuki-Miyaura Coupling; | A 3% B 98% |
| With potassium carbonate In ethanol; water at 60℃; for 5h; Catalytic behavior; Suzuki-Miyaura Coupling; | A 6.3% B 87% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
5720-06-9
2-Methoxyphenylboronic acid
-
-
49602-47-3
2,4'-dimethoxybiphenyl
| Conditions | Yield |
|---|---|
| With sodium phosphate; palladium on activated charcoal In water; isopropyl alcohol at 20℃; for 5h; Suzuki-Miyaura reaction; | 100% |
| With sodium hydrogencarbonate; palladium on activated charcoal In methanol at 20℃; for 8h; Suzuki-Miyaura coupling reaction; | 100% |
| With sodium phosphate dodecahydrate In isopropyl alcohol at 20℃; for 7h; Suzuki-Miyaura coupling reaction; Inert atmosphere; | 100% |
-
-
104-92-7
1-bromo-4-methoxy-benzene
-
-
95-51-2
2-Chloroaniline
-
-
53595-99-6
2-chloro-N-(4-methoxyphenyl)aniline
| Conditions | Yield |
|---|---|
| With tri-tert-butyl phosphine; sodium t-butanolate; palladium diacetate In toluene for 22h; Heating; | 100% |
| With sodium t-butanolate; palladium diacetate; (2,2-dimethylpropane-1,3-diyl)bis(diphenylphosphane) In 1,4-dioxane at 80℃; for 72h; Heating / reflux; | 73% |
| With C22H26Cl2NPPd; sodium t-butanolate In toluene at 110℃; for 22h; Inert atmosphere; |
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