Simagchem Corporation
Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:100-66-3
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryDayang Chem (Hangzhou) Co.,Ltd.
DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:100-66-3
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryHenan Allgreen Chemical Co.,Ltd
he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality se T rvice Appearance:
EAST CHEMSOURCES LIMITED
Anisole CAS No.: 100-66-3 Molecular Formula: C7H8O Molecular Weight: 108.13 Structural formula： A. Physical & Chemical Properties 1.Density:0.995 2.Melting point:-37℃ 3.Boiling point: 154℃ 4.Refractive lndex: 1.516-1.519 5.Solubilit
Ality Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Henan Tianfu Chemical Co., Ltd.
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.
Cas:100-66-3
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryJinan Finer Chemical Co., Ltd
Product Description Product website: http://www.finerchem.com Product Name Anisole CAS No. 100-66-3 Appea
Henan Sinotech Import&Export Corporation
Product Name Anisole Synonyms Methoxybenzine;Anisole, SuperDry, J&KSeal;Anisole, 99%, SpcDry, Water≤50 ppM (by K.F.), SpcSeal;Anisole ReagentPlus(R), 99%;ANISOL;ANISOLE;METHOXYBENZENE;METHYL PHENY
Baoji Guokang Healthchem co.,ltd
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:100-66-3
Min.Order:1 Kilogram
FOB Price: $16.0 / 20.0
Type:Trading Company
inquiryTriumph International Development Limilted
Appearance:white powder/crystal Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Sea/Ai
Hangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Hangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Shanghai Massive Chemical Technology Co., Ltd.
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:100-66-3
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHangzhou Lingrui Chemical Co.,Ltd.
AnisoleAppearance:Pls see the Details Storage:Keep away of light, hot, water, Store in dry, dark and ventilated place Package:according to customers' requirements Application:teroids, Cosmetics Ingredients, APIs, Intermediates, OLED&Battery Ingredien
HANGZHOU YUNUO CHEMICAL CO.,LTD
Clear straw colored liquid Appearance:Clear straw colored liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Used for analysis of reagents, s
Zibo Dorne chemical technology co. LTD
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Henan Wentao Chemical Product Co., Ltd.
We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:100-66-3
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquirySiwei Development Group Ltd.
Product name: Anisole CAS No.：100-66-3 Molecule Formula：C7H8O Molecule Weight：108.14 Purity: 99.5% Package: 200kg/drum Description：Clear colorless liquid Manufacture Standards：Enterprise Standard TESTING ITEMS
Hunan chemfish Pharmaceutical co.,Ltd
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Wuhan Fortuna Chemical Co.,Ltd
1.Product name:Anisole 2.CAS:100-66-3 3.MF:C7H8O 4.MW:108.1378 5.Appearance;Colorless to yellowish liquid 6.Assay:99%MIN Appearance:yellowish liquid Package:as celient requirement Port:ANY PORT OF CHINA
SAGECHEM LIMITED
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
JINHUA HUAYI CHEMICAL CO., LTD.
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Hangzhou Dingyan Chem Co., Ltd
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Aecochem Corp.
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Enke Pharma-tech Co.,Ltd. （Cangzhou, China ）
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Zhuozhou Wenxi import and Export Co., Ltd
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:100-66-3
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAntimex Chemical Limied
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Synthetic route
| Conditions | Yield |
|---|---|
| With potassium hydroxide; acyclic polyethylene oxides In dichloromethane; water for 0.5h; | 100% |
| With aluminum oxide; potassium fluoride In N,N-dimethyl-formamide for 1h; Product distribution; Ambient temperature; other phenols and alcohols, other alkylating agents, other reagents and solvents, var. time; | 100% |
| With potassium hydroxide; Aliquat 336 at 20℃; for 5h; | 99% |
-
-
17743-22-5
5-(2-methoxy-phenoxy)-1-phenyl-1H-tetrazole
-
A
-
5097-82-5
1-phenyl-5-hydroxytetrazole
-
B
-
100-66-3
methoxybenzene
| Conditions | Yield |
|---|---|
| With hydrazine hydrate; palladium on activated charcoal In ethanol; water; benzene for 1.83333h; Ambient temperature; | A n/a B 100% |
| palladium on activated charcoal In ethanol; benzene Mechanism; Product distribution; various reagents, temperatures and reaction times; | |
| With sodium hypophosphite; palladium on activated charcoal In ethanol; benzene at 80℃; Relative steady-state rates, relative extrapolated intercepts; |
| Conditions | Yield |
|---|---|
| With hydrogen In methanol at 70℃; under 750.075 Torr; for 0.333333h; | 100% |
| With LiCrH4*2LiCl*2THF In tetrahydrofuran at 25℃; for 12h; | 98% |
| Stage #1: 1-bromo-4-methoxy-benzene With n-butyllithium In tetrahydrofuran; hexane at -58℃; for 0.000861111h; Stage #2: With methanol In tetrahydrofuran; hexane at -58℃; for 0.000436111h; | 92% |
| Conditions | Yield |
|---|---|
| With tetraphenyldisilane; cesium fluoride In acetonitrile at 100℃; for 0.0833333h; | 100% |
| With tetrakis(triphenylphosphine) palladium(0); formaldehyd; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h; | 85% |
| With N,N,N,N,-tetramethylethylenediamine; C39H46IrN4 In acetonitrile at 45℃; for 48h; Sealed tube; Glovebox; Inert atmosphere; | 80% |
| Conditions | Yield |
|---|---|
| With lithium aluminium tetrahydride; di-tert-butyl peroxide In tetrahydrofuran for 1.5h; Irradiation; | 100% |
| With potassium phosphate In N,N-dimethyl-formamide; cyclohexanol at 110℃; for 12h; | 96% |
| With formaldehyd; palladium diacetate; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h; | 95% |
| Conditions | Yield |
|---|---|
| With pyridinium chlorochromate In dichloromethane at 25℃; for 1h; | 100% |
| In acetone at 0℃; for 1h; | 90% |
| With manganese(IV) oxide In methyl cyclohexane at 70℃; for 16h; | 43% |
| With tris(1,10-phenantholine)iron(III) perchlorate In acetonitrile at -30℃; Rate constant; other reagent; |
| Conditions | Yield |
|---|---|
| N,N,N',N'-tetrabutyl-N''-methylguanidine at 160℃; for 4.5h; | 100% |
| N,N,N',N'-tetrabutyl-N''-methylguanidine at 160℃; for 4.5h; Product distribution; other catalysts, other reaction conditions, other phenols; | 100% |
| With tetrabutylammomium bromide; potassium carbonate at 93℃; for 5h; | 99% |
| Conditions | Yield |
|---|---|
| acyclic polyethylene oxides In benzene at 25℃; | A 100% B n/a |
-
-
99506-45-3
4-methoxyphenyl(m-carboran-9-yl)iodonium tetrafluoroborate
-
-
7647-14-5
sodium chloride
-
A
-
17157-02-7
9-iodo-m-carborane
-
B
-
17819-85-1
9-chloro-m-carborane
-
C
-
696-62-8
para-iodoanisole
-
D
-
100-66-3
methoxybenzene
| Conditions | Yield |
|---|---|
| In chloroform; water mixt. of aryl(m-carboran-9-yl)iodonium tetrafluoroborate, NaCl, water and chloroform was vigorously stirred under reflux at 56°C, 2-2.5 h; internal standard (chlorobenzene) added and org. layer was analysed by GLC; | A 0% B 100% C 100% D 0% |
| Conditions | Yield |
|---|---|
| With tetrakis(triphenylphosphine) palladium(0); formaldehyd; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h; | 99% |
| With butyl magnesium bromide; zirconocene dichloride for 12h; Ambient temperature; | 98% |
| With lithium aluminium tetrahydride In 1,2-dimethoxyethane at 35℃; for 4h; ultrasonic acceleration of reduction; | 98% |
| Conditions | Yield |
|---|---|
| With triethylamine In water at 25℃; for 1h; UV-irradiation; | 99% |
| With formaldehyd; palladium diacetate; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h; | 98% |
| With potassium phosphate In N,N-dimethyl-formamide; cyclohexanol at 110℃; for 12h; | 95% |
| Conditions | Yield |
|---|---|
| With lithium borohydride; C22H19F3N4NiO2S In tetrahydrofuran at 70℃; for 24h; Reagent/catalyst; | 99% |
| With lithium borohydride; C30H21F6N2NiO2P In tetrahydrofuran at 70℃; for 3h; Reagent/catalyst; Concentration; Temperature; Time; Schlenk technique; Inert atmosphere; | 89% |
| With chloro(1,5-cyclooctadiene)rhodium(I) dimer; tri-n-butyl phosphite; chlorotriisopropylsilane In ethyl-cyclohexane at 130℃; for 15h; Inert atmosphere; | 74% |
| With chloro(1,5-cyclooctadiene)rhodium(I) dimer; tri-n-butyl phosphite; chlorotriisopropylsilane In ethylcyclohexane at 130℃; for 15h; Inert atmosphere; | 74 %Chromat. |
| With [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; ethanol; potassium hexamethylsilazane In toluene at 140℃; for 8h; Inert atmosphere; | 30 %Chromat. |
| Conditions | Yield |
|---|---|
| With ammonium formate In water at 20℃; for 3h; | 98% |
| With isopropyl alcohol; sodium hydroxide at 24.84℃; under 760.051 Torr; for 1h; Inert atmosphere; UV-irradiation; | 97% |
| With palladium on ceria; sodium hydroxide In isopropyl alcohol at 40℃; for 18h; Irradiation; Inert atmosphere; Sealed tube; | 94% |
-
-
132636-68-1
3-(4-methoxyphenoxy)-1,2-benzisothiazole 1,1-dioxide
-
A
-
100-66-3
methoxybenzene
-
B
-
81-07-2
saccharin
| Conditions | Yield |
|---|---|
| With sodium hypophosphite; palladium on activated charcoal In water; benzene for 3h; Heating; | A 98% B n/a |
| Conditions | Yield |
|---|---|
| With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride In 2-pentanol at 100℃; for 36h; Inert atmosphere; | A 1% B 98% |
| With 18-crown-6 ether; zinc; 10 percent Pd/C In water; acetone at 20℃; Product distribution; Further Variations:; Catalysts; Reagents; Solvents; Ullmann coupling; |
| Conditions | Yield |
|---|---|
| With sodium hydroxide at 24.84℃; under 760.051 Torr; for 5h; Inert atmosphere; UV-irradiation; Sealed tube; | 98% |
| Conditions | Yield |
|---|---|
| With sodium hydroxide at 40℃; for 6h; also diethyl 2-oxo-1,3-propanedisulfonate; var. reaction time; other alkylating agents; | 97.2% |
| Conditions | Yield |
|---|---|
| With potassium hydroxide In 1,4-dioxane for 1.5h; | 97% |
| With potassium carbonate In acetone for 0.0833333h; Etherification; methylation; microwave irradiation; | 92% |
| With sodium hydroxide; N-butyl-N,N-dimethyl-(α-phenyl)ethylammonium bromide In 1,2-dichloro-ethane for 6h; Heating; | 85% |
| Conditions | Yield |
|---|---|
| With water; triphenylphosphine; sodium iodide; nickel dichloride; zinc In N,N-dimethyl-formamide at 70℃; for 2h; Rate constant; Product distribution; Mechanism; var. organic halides; other solvent; var. temp., and reaction times; | A 2.5% B 96.8% |
| With potassium hydroxide In water; N,N-dimethyl-formamide at 35℃; for 12h; Ullmann Condensation; Inert atmosphere; | A 92% B 6% |
| With NaH-t-AmONa-Ni(OAc)2-bpy In tetrahydrofuran at 63℃; for 8h; | A 73% B 16 % Chromat. |
-
-
36719-69-4
1-(4-Methoxyphenyl)-3,3-diethyl-1-triazene
-
A
-
696-62-8
para-iodoanisole
-
B
-
100-66-3
methoxybenzene
| Conditions | Yield |
|---|---|
| With cation exchange resin BioRad AG 50W-X12 (H+); sodium iodide In acetonitrile at 75℃; Product distribution; further solvent: THF, DMSO; | A 96% B 4% |
| Conditions | Yield |
|---|---|
| With 18-crown-6 ether; potassium carbonate at 150℃; for 2h; | 96% |
| Conditions | Yield |
|---|---|
| With potassium phosphate In N,N-dimethyl-formamide; cyclohexanol at 110℃; for 12h; | 96% |
| With formaldehyd; palladium diacetate; caesium carbonate In dimethyl sulfoxide at 80℃; for 12h; | 85% |
| With isopropyl alcohol at 20℃; for 18h; UV-irradiation; chemoselective reaction; | 78% |
| Conditions | Yield |
|---|---|
| With potassium phosphate; dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; palladium(II) acetylacetonate; isopropyl alcohol In 1,4-dioxane at 130℃; for 4h; Time; Reagent/catalyst; Solvent; Inert atmosphere; | 96% |
| With potassium phosphate; bis(acetylacetonato)palladium(II); dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine; isopropyl alcohol In 1,4-dioxane at 130℃; for 4h; | 96 %Chromat. |
-
-
100-66-3
methoxybenzene
| Conditions | Yield |
|---|---|
| With trifluoromethanesulfonyloxy(triphenylphosphine)gold(I) In 1,4-dioxane at 20℃; | 96% |
| Conditions | Yield |
|---|---|
| With 1,10-Phenanthroline; oxygen; copper diacetate; silver nitrate; sodium hydroxide In dimethyl sulfoxide at 140℃; under 3750.38 Torr; for 12h; Autoclave; Green chemistry; | 96% |
-
-
67-56-1
methanol
-
-
7719-12-2, 52843-90-0
phosphorus trichloride
-
A
-
18351-42-3
dimethyl phenylphosphonite
-
B
-
7526-26-3
diphenyl methylphosphonate
-
C
-
100-66-3
methoxybenzene
| Conditions | Yield |
|---|---|
| Stage #1: phosphorus trichloride; phenol at 65 - 250℃; for 4h; Stage #2: methanol at 204 - 260℃; for 2h; Product distribution / selectivity; | A n/a B 95.6% C n/a |
| Stage #1: phosphorus trichloride; phenol at 65 - 250℃; for 4h; Stage #2: methanol; methyl iodide at 210 - 250℃; Product distribution / selectivity; | A 7.14% B 92.86% C n/a |
| Conditions | Yield |
|---|---|
| copper(I) bromide In methanol; N,N-dimethyl-formamide at 110℃; for 0.75h; | 95% |
| copper(I) bromide In methanol for 6h; Product distribution; Mechanism; Rate constant; Heating; by investigating the influence of several reaction parameters (the nature and concentration of the copper catalyst, the cosolvents, the concentration and number of equivalents of the nucleophile, the bromide concentration, the aryl bromide subst. effect; | 95% |
| With methanol; Methyl formate; copper(l) chloride at 115℃; for 2h; Reagent/catalyst; Autoclave; Green chemistry; | 80% |
| With hemicucurbituril supported [Bmim]Cl In toluene for 9h; Reflux; | 78% |
| With ethyl acetate; copper(I) bromide In methanol for 2h; Heating; Yield given; |
-
-
107-31-3
Methyl formate
-
-
696-62-8
para-iodoanisole
-
-
124-41-4
sodium methylate
-
A
-
121-98-2
methyl 4-methoxybenzoate
-
B
-
100-66-3
methoxybenzene
| Conditions | Yield |
|---|---|
| bis-triphenylphosphine-palladium(II) chloride In dichloromethane at 40℃; under 11250.9 Torr; for 7h; | A 95% B 5% |
-
-
13509-27-8
methyl phenyl carbonate
-
-
100-66-3
methoxybenzene
| Conditions | Yield |
|---|---|
| dmap at 130℃; for 2h; other catalysts; | 95% |
| N,N,N',N'-tetrabutyl-N''-methylguanidine at 110℃; for 1h; Product distribution; other catalysts, other reaction conditions, other aryl methyl carbonates; | 93 % Chromat. |
-
-
18412-81-2
dodecyl-dimethylsulphonium iodide
-
-
108-95-2
phenol
-
A
-
1187-84-4
S-methyl-L-cysteine
-
B
-
100-66-3
methoxybenzene
| Conditions | Yield |
|---|---|
| With potassium hydroxide In water at 70℃; for 5h; pH = 9; | A n/a B 95% |
| Conditions | Yield |
|---|---|
| With Noccaea caerulescens extract supported in montmorillonite K10 at 60℃; for 6h; Friedel Crafts acylation; Inert atmosphere; regioselective reaction; | 100% |
| With aluminum (III) chloride In dichloromethane at 5 - 20℃; for 2.5h; | 98% |
| With benzyltributylammonium tetrachloroferrate at 50℃; for 0.1h; Friedel-Crafts reaction; | 93% |
| Conditions | Yield |
|---|---|
| With polystyrene-bound tetrafluorophenylbis(triflyl)methane In nitromethane at 50℃; for 2h; Friedel-Crafts acylation; | 100% |
| With lithium perchlorate at 60℃; for 1h; | 100% |
| With Sulfate; zirconium(IV) oxide at 110℃; | 100% |
| Conditions | Yield |
|---|---|
| With hafnium(IV) trifluoromethanesulfonate; lithium perchlorate In nitromethane for 6h; Ambient temperature; | 100% |
| With lithium perchlorate at 60℃; for 1.5h; | 99% |
| With trifluorormethanesulfonic acid; titanium(IV) chloride tris(trifluoromethanesulfonate) In acetonitrile for 12h; Ambient temperature; | 90% |
| Conditions | Yield |
|---|---|
| Stage #1: acetic acid; methoxybenzene With trifluoroacetic anhydride In dichloromethane at 20℃; for 0.25h; Stage #2: With trifluorormethanesulfonic acid In dichloromethane at 20℃; for 1h; | 100% |
| With methanesulfonic acid; pyrographite at 80℃; for 0.333333h; Friedel-Crafts acylation; | 98% |
| With aluminum oxide; trifluoroacetic anhydride for 0.166667h; Ambient temperature; | 96% |
| Conditions | Yield |
|---|---|
| With aluminium trichloride In dichloromethane for 15h; Ambient temperature; | 100% |
| (p-MeOC6H4)2BSbCl6 In dichloromethane for 24h; Ambient temperature; | 88% |
| With aluminium trichloride In tetrachloromethane at 0℃; for 2h; | 87% |
-
-
36854-57-6
2-Phenylbutyryl chloride
-
-
100-66-3
methoxybenzene
-
-
78423-10-6
1-(4-methoxyphenyl)-2-phenylbutan-1-one
| Conditions | Yield |
|---|---|
| aluminum (III) chloride at 0 - 20℃; for 2h; Friedel Crafts Acylation; | 100% |
| Stage #1: 2-Phenylbutyryl chloride; methoxybenzene With aluminum (III) chloride In carbon disulfide at 10 - 20℃; for 20h; Inert atmosphere; Cooling with ice; Stage #2: With water In carbon disulfide | 94% |
| With aluminum (III) chloride In dichloromethane at 0 - 20℃; for 2.5h; Friedel-Crafts Acylation; | 76% |
| Conditions | Yield |
|---|---|
| With gallium(III) trichloride; silver hexafluoroantimonate In 1,2-dichloro-ethane for 7h; Heating; | 100% |
| With trifluoroacetic acid at 20℃; for 1.5h; Friedel-Crafts Acylation; | 98% |
| With lithium perchlorate In nitromethane at 100℃; for 4h; | 97% |
| Conditions | Yield |
|---|---|
| aluminum (III) chloride In dichloromethane at 5 - 20℃; for 3h; Friedel Crafts Acylation; | 100% |
| With aluminum (III) chloride In dichloromethane at 0℃; for 3h; | 99% |
| With aluminum (III) chloride In dichloromethane for 3h; | 99% |
| Conditions | Yield |
|---|---|
| With benzyltriphenylphosphonium peroxodisulfate; potassium bromide In acetonitrile for 3.5h; Heating; | 100% |
| With Selectfluor; sodium bromide In acetonitrile at 20℃; for 21h; | 100% |
| With bis[1-methyl-3-(3-sulfopropyl)imidazolium] hexafluorotitanate; dihydrogen peroxide; sodium bromide In water at 25℃; for 3h; Reagent/catalyst; Concentration; Solvent; Temperature; Green chemistry; | 100% |
| Conditions | Yield |
|---|---|
| With hydrogen; [(norbornadiene)rhodium(I)chloride]2; phosphinated polydiacetylene In n-heptane at 30℃; under 60800 Torr; for 0.7h; | 100% |
| With hydrogen; Rh on carbon In methanol at 20℃; under 760.051 Torr; for 1h; | 100% |
| With hydrogen In hexane at 24.84℃; under 750.075 Torr; for 3h; | 100% |
| Conditions | Yield |
|---|---|
| With IPy2BF4*2HBF4 In dichloromethane for 0.25h; Ambient temperature; | 100% |
| With iodine; n-butyltriphenylphosphonium peroxodisulfate In acetonitrile for 0.5h; Heating; | 100% |
| With ammonium iodide; 3-chloro-benzenecarboperoxoic acid for 2h; | 100% |
| Conditions | Yield |
|---|---|
| With molybdenum hexacarbonyl Sealed tube; regioselective reaction; | 100% |
| With potassium carbonate; palladium on activated charcoal at 120℃; for 12h; | 91% |
| With palladium 10% on activated carbon; potassium carbonate for 20h; Heating; | 82.65% |
-
-
69435-89-8
trimethylsilyl cyclohexanecarboxylate
-
-
100-66-3
methoxybenzene
-
-
7469-80-9
cyclohexyl 4-methoxyphenyl ketone
| Conditions | Yield |
|---|---|
| With tetrachlorosilane; 4-(trifluoromethyl)benzoic anhydride; silver perchlorate In dichloromethane for 25h; Ambient temperature; | 100% |
-
-
21273-15-4
trimethylsilyl ester of hydrocinnamic acid
-
-
100-66-3
methoxybenzene
-
-
5739-38-8
1-(4-methoxyphenyl)-3-phenylpropan-1-one
| Conditions | Yield |
|---|---|
| With SiClO4; 4-(trifluoromethyl)benzoic anhydride; silver perchlorate In dichloromethane for 63h; Ambient temperature; | 100% |
-
-
100-66-3
methoxybenzene
-
-
84858-88-8
1-(2,3,4,5,6-pentamethylphenyl)butan-1-one
-
A
-
13404-83-6
1-(2-methoxyphenyl)butan-1-one
-
B
-
700-12-9
pentamethylbenzene,
-
C
-
4160-51-4
1-(4-methoxyphenyl)-1-butanone
| Conditions | Yield |
|---|---|
| trifluoroacetic acid for 5h; Heating; | A n/a B 100% C n/a |
| Conditions | Yield |
|---|---|
| With silver hexafluoroantimonate; antimonypentachloride In 1,2-dichloro-ethane for 3h; Heating; | 100% |
| With dipotassium peroxodisulfate In trifluoroacetic acid at 20℃; for 16h; | 89% |
| Stage #1: diphenyldisulfane With thionyl chloride In 1,2-dichloro-ethane at 5 - 30℃; for 4h; Stage #2: With aluminum (III) chloride In 1,2-dichloro-ethane at 5 - 10℃; for 1h; Stage #3: methoxybenzene In 1,2-dichloro-ethane for 4h; | 88.5% |
| With silver hexafluoroantimonate; antimonypentachloride In 1,2-dichloro-ethane for 3h; Product distribution; Heating; effect of Lewis acid and silver salt; |
-
-
100-66-3
methoxybenzene
-
-
79562-11-1
N,N-diacetyl-p-nitrophenylsulphenamide
-
A
-
22865-50-5
4-(4-methoxyphenylsulfanyl)nitrobenzene
-
B
-
100-06-1
1-(4-methoxyphenyl)ethanone
| Conditions | Yield |
|---|---|
| With trifluoroacetic acid at 190 - 200℃; | A 100% B 21% |
| Conditions | Yield |
|---|---|
| With aluminium(III) iodide; tetra-(n-butyl)ammonium iodide In cyclohexane for 0.3h; Heating; | 100% |
| With water; hydrogen bromide; Aliquat 336 at 105℃; for 5h; Catalytic behavior; | 96% |
| With monochloroborane dimethyl sulfide complex In benzene Heating; | 95% |
-
-
6223-78-5
2,5-dichloro-2,5-dimethyl hexane
-
-
100-66-3
methoxybenzene
-
-
51510-70-4
1,2,3,4-tetrahydro-1,1,4,4-tetramethyl-6-methoxynaphthalene
| Conditions | Yield |
|---|---|
| aluminum (III) chloride at 0℃; for 2h; | 100% |
| With aluminium trichloride 1.) RT, 30 min, 2.) reflux, 15 min; | 86% |
| With aluminium trichloride Heating; |
| Conditions | Yield |
|---|---|
| With nitric oxide; trifluoroacetic anhydride for 0.133333h; Product distribution; Ambient temperature; | 100% |
| With hydrogenchloride; 1-(4-(nitrosooxy)butyl)-3-methylimidazolium chloride In water at 0 - 5℃; for 1.08333h; regioselective reaction; | 88% |
| With nitrosonium tetrafluoroborate In acetonitrile at 25℃; for 0.5h; | 87% |
-
-
4509-90-4
5-bromovaleroyl chloride
-
-
100-66-3
methoxybenzene
-
-
69287-12-3
5-bromo-1-(4-methoxyphenyl)pentan-1-one
| Conditions | Yield |
|---|---|
| With aluminum (III) chloride In dichloromethane at 0 - 20℃; for 2h; | 100% |
| With aluminium trichloride Friedel-Crafts acylation; | 85% |
| With aluminum (III) chloride In dichloromethane at 0 - 20℃; for 2h; Friedel-Crafts Acylation; | |
| With metallic chloride at 50℃; Friedel-Crafts Acylation; | |
| With aluminum (III) chloride In dichloromethane at 0 - 20℃; Inert atmosphere; |
-
-
27607-77-8
trimethylsilyl trifluoromethanesulfonate
-
-
100-66-3
methoxybenzene
-
-
350693-36-6
1,1-diphenyl-3-(trimethylsilyl)-1-(trimethylsilyloxy)prop-2-yne
| Conditions | Yield |
|---|---|
| In dichloromethane at -78℃; for 3h; Friedel-Crafts reaction; | 100% |
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