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TIANFU-CHEM - Diisopropyl peroxydicarbonate Application:TIANFU-CHEM - Diisopropyl peroxydicarbonate
TIANFU-CHEM - Diisopropyl peroxydicarbonateAppearance:Solid Storage:In Room Temperature Package:IN 25kg drums Application:Organic synthesis Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport)
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inquiryDiisopropyl peroxydicarbonate Basic information Product Name: Diisopropyl peroxydicarbonate Synonyms: Diisopropyl peroxydicarbonate;bisisopropyl peroxydicarbonate;Isopropyl Peroxydic
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Peroxydicarbonic acid,C,C'-bis(1-methylethyl) ester Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:
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inquiryConditions | Yield |
---|---|
With sodium hydroxide; dihydrogen peroxide | 99% |
With sodium hydroxide; dihydrogen peroxide In water at 15℃; Product distribution / selectivity; | 94% |
With dihydrogen peroxide; potassium hydroxide In water at 5 - 50℃; for 0.0766667h; Flow reactor; | 74.7% |
With sodium peroxide | |
With sodium hydroxide; dihydrogen peroxide |
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical
diisopropyl peroxydicarbonate
1,4-Divinylbenzene
2-(isopropyloxycarbonyloxy)-1-(2',2',6',6'-tetramethyl-1'-piperidinyloxy)-1-(4'-vinylphenyl)ethane
Conditions | Yield |
---|---|
at 55℃; for 5h; | 76.1% |
4-acetoxy-2,2,6,6-tetramethylpiperidine-1-oxyl
diisopropyl peroxydicarbonate
1,4-Divinylbenzene
Conditions | Yield |
---|---|
at 0 - 55℃; for 5h; | 73% |
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical
diisopropyl peroxydicarbonate
1,3-divinylbenzene
Conditions | Yield |
---|---|
70.5% |
4-(benzyloxycarbonyl)-2,2,6,6-tetramethylpiperidine-1-oxyl
diisopropyl peroxydicarbonate
1,4-Divinylbenzene
Conditions | Yield |
---|---|
at 0 - 55℃; for 5h; | 62.1% |
diisopropyl peroxydicarbonate
N-(4-chlorophenylmethylene)-2-methylthiobenzenamine
A
2-(4-chlorophenyl)benzothiazole
B
4-chlorobenzaldehyde
C
(2-aminophenyl)thiomethyl isopropyl carbonate
Conditions | Yield |
---|---|
In benzene at 60℃; for 5h; | A 36% B 48% C 54% |
diisopropyl peroxydicarbonate
1,4-Divinylbenzene
di-tert-butyl nitroxide
Conditions | Yield |
---|---|
at 0 - 55℃; for 5h; | 53.2% |
diisopropyl peroxydicarbonate
benzylidene-(2-methylsulfanyl-phenyl)-amine
A
2-Phenylbenzothiazole
B
benzaldehyde
C
(2-aminophenyl)thiomethyl isopropyl carbonate
Conditions | Yield |
---|---|
In benzene at 60℃; for 5h; | A 17% B 35% C 53% |
diisopropyl peroxydicarbonate
N-(3-nitrophenylmethylene)-2-methylthiobenzenamine
A
2-(3-nitrophenyl)benzothiazole
B
3-nitro-benzaldehyde
C
(2-aminophenyl)thiomethyl isopropyl carbonate
D
<(2-(3-nitrophenyl)methylenamino)phenyl>thiomethyl isopropyl carbonate
Conditions | Yield |
---|---|
With 2,6-di-tert-butylphenol In benzene at 60℃; for 5h; | A 3% B 13% C 10% D 50% |
diisopropyl peroxydicarbonate
[4-(benzylideneamino)phenyl]methanol
A
methyl 6-methoxy-2-phenylquinoline-4-carboxylate
B
carbamic acid, (4-methoxyphenyl)-, 1-methylethyl ester
Conditions | Yield |
---|---|
With acrylic acid methyl ester In benzene at 60℃; for 4h; | A 49% B 14% |
diisopropyl peroxydicarbonate
N-(4-methoxyphenylmethylene)-2-methylthiobenzenamine
A
2-(4-methoxy-phenyl)-benzothiazole
B
4-methoxy-benzaldehyde
C
(2-aminophenyl)thiomethyl isopropyl carbonate
Conditions | Yield |
---|---|
In benzene at 60℃; for 5h; | A 28% B 48% C 39% |
diisopropyl peroxydicarbonate
N-(phenylmethylene)-5-amino-2-methoxypyridine
diethylazodicarboxylate
A
diethyl hydrazodicarboxylate
Conditions | Yield |
---|---|
In benzene at 60℃; | A n/a B n/a C 47% |
diisopropyl peroxydicarbonate
N-(2-thienylmethylene)-2-methylthiobenzenamine
A
thiophene-2-carbaldehyde
B
2-thiophen-2-yl-benzothiazole
C
(2-aminophenyl)thiomethyl isopropyl carbonate
Conditions | Yield |
---|---|
In benzene at 60℃; for 5h; | A 40% B 13% C 45% |
TEMPOL
diisopropyl peroxydicarbonate
1,4-Divinylbenzene
2-(isopropyloxycarbonyloxy)-1-(4'-hydroxy-2',2',6',6'-tetramethyl-1'-piperidinyloxy)-1-(4'-vinylphenyl)ethane
Conditions | Yield |
---|---|
at 0 - 55℃; for 5h; | 41% |
diisopropyl peroxydicarbonate
[4-(benzylideneamino)phenyl]methanol
A
carbamic acid, (4-methoxyphenyl)-, 1-methylethyl ester
Conditions | Yield |
---|---|
With (E)-1,2-diphenyl-ethene In benzene at 60℃; for 4h; | A 15% B 40% C 20% |
diisopropyl peroxydicarbonate
N-(3-nitrophenylmethylene)-2-methylthiobenzenamine
A
2-(3-nitrophenyl)benzothiazole
B
3-nitro-benzaldehyde
C
(2-aminophenyl)thiomethyl isopropyl carbonate
Conditions | Yield |
---|---|
In benzene at 60℃; for 5h; | A 38% B 40% C 35% |
diisopropyl peroxydicarbonate
(E)-N-benzylidenebenzenamine
A
carbamic acid, phenyl-, 1-methylethyl ester
B
2-phenyl-quinoline-3,4-dicarbonitrile
Conditions | Yield |
---|---|
With 1,2-Dicyanoethylene In benzene at 60℃; for 4h; | A 20% B 38% |
diisopropyl peroxydicarbonate
N-(3-phenyl-2-propenylidene)-2-methylthiobenzenamine
A
2-styrylbenzothiazole
B
(2-aminophenyl)thiomethyl isopropyl carbonate
C
3-phenyl-propenal
Conditions | Yield |
---|---|
In benzene at 60℃; for 5h; | A 24% B 30% C 36% |
diisopropyl peroxydicarbonate
diethylazodicarboxylate
A
diethyl hydrazodicarboxylate
Conditions | Yield |
---|---|
In benzene at 60℃; | A n/a B n/a C 36% |
diisopropyl peroxydicarbonate
9-methylene-fluorene
polymer, Mn 1070 by SEC with oligostyrene as standard, Mn 1560 by SEC with oligo(dibenzofulvene) as standard; monomer(s): dibenzofulvene; 2,9-dimethyl-3,5,6,8-tetraoxadeca-4,7-dione
Conditions | Yield |
---|---|
In toluene at 40℃; for 24h; | 33% |
Conditions | Yield |
---|---|
In benzene at 60℃; for 18h; | A 16% B 28% C 11% |
diisopropyl peroxydicarbonate
N-(4-chlorobenzylidene)aniline
A
Isopropyl N-4-chlorophenylcarbamate
Conditions | Yield |
---|---|
With acrylic acid methyl ester In benzene at 60℃; for 4h; | A 27% B 16% |
diisopropyl peroxydicarbonate
N-benzylidene-4-acetylaniline
A
isopropyl (4-acetylphenyl)carbamate
Conditions | Yield |
---|---|
With acrylonitrile In benzene at 60℃; for 4h; | A 23% B 27% |
diisopropyl peroxydicarbonate
A
triphenylmethyl alcohol
B
2-(4-chlorophenyl)benzoxazole
C
triphenylmethyl iso-propyl ether
Conditions | Yield |
---|---|
In benzene at 60℃; for 24h; Further byproducts given; | A 23% B 23% C 6% D 6% |
diisopropyl peroxydicarbonate
A
triphenylmethyl alcohol
B
2-(4-chlorophenyl)benzoxazole
C
triphenylmethyl iso-propyl ether
Conditions | Yield |
---|---|
In benzene at 60℃; for 24h; Product distribution; Mechanism; | A 23% B 23% C 6% D 6% E 3% |
diisopropyl peroxydicarbonate
C
2-(4-methoxyphenyl)-1-phenyl-1H-benzo[d]imidazole
Conditions | Yield |
---|---|
In benzene at 60℃; for 18h; | A 18% B 21% C 13% |
diisopropyl peroxydicarbonate
phenylacetylene
A
(1-isopropoxyethyl)benzene
B
1-Phenylethanol
Conditions | Yield |
---|---|
In benzene at 60℃; Product distribution; Mechanism; same produts were determined by GC; | A n/a B n/a C 21% D n/a E n/a F n/a |
diisopropyl peroxydicarbonate
(E)-N-benzylidenebenzenamine
A
Benzoyl-phenyl-carbamic acid isopropyl ester
B
2-phenyl-4-(trimethylsilyl)quinoline
Conditions | Yield |
---|---|
With ethenyltrimethylsilane In benzene at 60℃; for 4h; | A 20% B 7% |
diisopropyl peroxydicarbonate
A
1,2-diphenyl-1H-benzoimidazole
C
1,3-diphenyl-1H-quinoxalin-2-one
Conditions | Yield |
---|---|
In benzene at 60℃; for 30h; | A 20% B 14% C 14% |
diisopropyl peroxydicarbonate
A
4-Methoxybenzophenone
B
4-methoxy-benzaldehyde
C
11-(4-methoxyphenyl)dibenz<1,4>oxazepine
Conditions | Yield |
---|---|
In benzene at 60℃; for 6h; imine:reagent=1:4; Yield given. Further byproducts given; | A 18% B n/a C 17% D n/a |
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