As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:104-88-1
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inquiryTalent Advantages: The Company features strong technical strength, possesses an efficient and cohesive management team, and enthusiastic and creative talents. The whole team has excellent execution ability, faces the market competition with firm be
Items Standard Result Appearance White crystals White crystals Assay 99%min
Cas:104-88-1
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:104-88-1
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inquiryProduct description: Product name 4-Chlorobenzaldehyde CAS number 104-88-1 Assay ≥99% Appearance White solid Capacity 200mt/year Application Pharmaceutical/pesticide/dye inte
Cas:104-88-1
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inquiryISO Certification Technology: Technology innovation is our eternal pursuit,or we will be left behind.Our technology experts,all from famous universities and institutes,has rich experience and high achievements in chemical research.This makes sure
4-C hloro benzaldehyde Molecular Formula: C7H5ClO Structure: Molecular Weight: 140.57 Color: White to Light Yellow Density: 1.196
Cas:104-88-1
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:104-88-1
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
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Chemwill Asia co.,Ltd is one of the leading manufacturer in CHINA. Product quality, process, price and service 4-Chlorobenzaldehyde CAS 104-88-1 PCAD IN Stock p-Chlorobenzenecarboxaldehyde 104-88-1 104-88-1 CAS 104-88-1 highly quality and
Cas:104-88-1
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inquiryProduct Name: 4-Chlorobenzaldehyde Synonyms: Chloromezanone Impurity;4-Chlorobenzoic aldehyde;4-CHLOROBENZALDEHYDE;AMMONIA WATER;AMMONIA SOLUTION, STRONG;AMMONIA NO 1;AMMONIA NO 2;AMMONIA 1 ION CHROMATOGRAPHY STANDARD CAS: 104-88-1 MF: C7H5ClO
Cas:104-88-1
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:104-88-1
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inquiryName: 4-Chloro Benzaldehyde CAS:104-88-1 MF: C7H5ClO Appearance:White Powder Storage:Store in cool and dry place, away from sun light. Package:25KG Application:Syntheses Material Intermediates Transportation:By sea or by air Port:Qingdao Port
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Cas:104-88-1
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inquiryAppearance:White to pale yellow liquid Storage:Store below +30°C. Package:200kg/Drum Application:4-Chlorobenzaldehyde is used as an intermediate for the manufacture of dyestuffs, optical brighteners, pharmaceuticals, agricultural chemicals and met
Cas:104-88-1
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Cas:104-88-1
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the
Cas:104-88-1
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inquiryWuhan hanweishi Pharmchem Co., Ltd(Hanways chempharm) is a specialized company concentrating on the R&D, production, marketing and technical service of APIs and pharmaceutical intermediates. The leading products range are APIs, Hormones, Peptides
Cas:104-88-1
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Cas:104-88-1
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inquiry4-Chlorobenzaldehyde CAS:104-88-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter
Cas:104-88-1
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:104-88-1
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inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:104-88-1
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryHebei Mojin Biotechnology Co., Ltd,Our business covers more than 30 countries, most of the big customers come from Europe, America and other countries in the world, we can guarantee the quality and price. In recent decades, with the efforts of all em
Cas:104-88-1
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inquiryp-Chlorobenzaldehyde CAS: 104-88-1 Specification product name 4-chlorobenzaldehyde chemical structure cas 104-88-1 mf c7h5clo e
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:As customer request Port:Qingda
Cas:104-88-1
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inquiryConditions | Yield |
---|---|
With oxygen; perruthenate modified mesoporous silicate MCM-41 In toluene at 80℃; for 1h; Oxidation; | 100% |
With n-butyltriphenylphosphonium permanganate In acetonitrile at 20℃; for 0.25h; | 100% |
With butyltriphenylphosphonium chlorochromate In acetonitrile for 0.75h; Heating; | 100% |
2-(4-chlorophenyl)-1,3-benzodithiole
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With tetrafluoroboric acid; mercury(II) oxide In tetrahydrofuran for 0.25h; Ambient temperature; | 100% |
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride for 0.0416667h; Product distribution; Ambient temperature; pH = 4-6, regeneration of aldehyde; | 100% |
(acetyloxy)(4-chlorophenyl)methyl acetate
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With [NO(1+)*18-crown-6*H(NO3)2(1-)]; silica gel In dichloromethane at 20℃; for 0.0833333h; | 100% |
With poly(4-vinylpyridine)-supported sulfuric acid In acetonitrile at 50℃; for 0.75h; Green chemistry; | 100% |
With bismuth(III) chloride In chloroform for 0.416667h; deprotection; Heating; | 99% |
4-chlorobenzyltrimethylsilyl ether
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With nitrogen dioxide at 20℃; for 0.0833333h; | 100% |
With trichloroisocyanuric acid In acetonitrile for 0.166667h; Reflux; | 100% |
With NTPPPODS In acetonitrile for 0.0666667h; Reflux; | 99% |
2-(4-chlorobenzyloxy)tetrahydro-2H-pyran
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With aluminium trichloride; benzyltriphenylphosphonium chlorate In acetonitrile at 20℃; for 1h; | 100% |
With allyltriphenylphopsphonium peroxodisulfate In acetonitrile for 0.333333h; Heating; | 99% |
With N-Bromosuccinimide; β‐cyclodextrin In acetone at 20℃; for 0.5h; | 95% |
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With caro's acid; silica gel In dichloromethane for 0.133333h; Heating; | 100% |
Conditions | Yield |
---|---|
Stage #1: ethyl 4-chlorobenzoate With morpholine; diisobutylaluminium hydride In tetrahydrofuran; hexane at 0℃; for 3.16667h; Inert atmosphere; Stage #2: With diisobutylaluminium hydride In tetrahydrofuran; hexane at 0℃; for 0.166667h; Inert atmosphere; | 99% |
With phenylsilane; cobalt(II) diacetate tetrahydrate; sodium triethylborohydride In 1,2-dimethoxyethane; toluene at 25℃; for 15h; Inert atmosphere; Schlenk technique; | 84% |
With n-butyllithium; diisobutylaluminium hydride; tert-butyl alcohol In tetrahydrofuran; hexane at 0℃; | 83% |
Conditions | Yield |
---|---|
With samarium diiodide; phosphoric acid In tetrahydrofuran for 0.000833333h; Ambient temperature; | 99% |
Conditions | Yield |
---|---|
With sodium periodate; C53H44As2N2O3Ru In water; ethyl acetate; acetonitrile at 25℃; for 0.5h; | 99% |
With sodium periodate; C22H23ClIN2Os(1+)*F6P(1-) In water; tert-butyl alcohol at 60℃; for 1h; Schlenk technique; Inert atmosphere; | 99% |
With sodium periodate; C18H15ClFN2Ru(1+)*Cl(1-) In water; tert-butyl alcohol at 60℃; for 1h; Catalytic behavior; Schlenk technique; Inert atmosphere; | 99% |
N,N-dimethyl-4-chlorobenzamide
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With lithium diisobutylmorpholinoaluminum hydride In tetrahydrofuran; hexane at 0℃; for 0.5h; | 99% |
With sodium hydride; sodium iodide In tetrahydrofuran at 40℃; chemoselective reaction; | 71% |
With bis-(1,2-dimethylpropyl)borane In tetrahydrofuran; dodecane at 25℃; | 70 % Chromat. |
With C11H25AlNO4(1-)*Na(1+) In tetrahydrofuran; toluene at 0 - 20℃; for 0.5h; | > 99 %Chromat. |
copper(I) chloride
1,10-Phenanthroline
para-Chlorobenzyl alcohol
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
In diethyl ether; toluene | 99% |
di(p-tolyl) sulfoxide
para-Chlorobenzyl alcohol
A
di-(p-tolyl)sulfane
B
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With per-rhenic acid In toluene for 17h; Reflux; | A 99% B 70% |
Conditions | Yield |
---|---|
With methanol; potassium permanganate In ethyl acetate at 25℃; for 24h; | 99% |
With lithium perchlorate In methanol at 0℃; Inert atmosphere; Sealed tube; Electrochemical reaction; Cooling with ice; | 68% |
Conditions | Yield |
---|---|
With benzyltriphenylphosphonium dichromate In acetonitrile for 0.25h; Oxidation; Heating; | 98% |
With benzyltriphenylphosphonium dichromate; silica gel for 0.0833333h; | 98% |
With tribromo-isocyanuric acid In acetonitrile at 20℃; for 1h; | 98% |
2-(4-chlorophenyl)-1,3-dithiane
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With aluminium trichloride; 1-benzyl-1-aza-4-azoniabicyclo<2.2.2>octane periodate at 20℃; for 0.166667h; | 98% |
With bromine; dimethyl sulfoxide In chloroform at 20℃; for 0.25h; | 97% |
With bromine; silica gel In dichloromethane at 20℃; for 0.166667h; | 97% |
α-(3-oxobutyl)-4,4'-dichlorobenzoin
A
1-(p-chlorophenyl)-1,4-pentanedione
B
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With potassium cyanide In N,N-dimethyl-formamide for 0.5h; Ambient temperature; | A 98% B n/a |
α-(2-ethoxycarbonylethyl)-4,4'-dichlorobenzoin
A
ethyl 4-(4-chlorophenyl)-4-oxobutanoate
B
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With potassium cyanide In N,N-dimethyl-formamide at 80℃; for 0.25h; | A 98% B n/a |
Conditions | Yield |
---|---|
With cerium triflate In nitromethane; water at 20℃; for 2h; | 98% |
With aluminium trichloride; 1-benzyl-4-aza-1-azoniabicyclo[2.2.2]octane dichromate for 0.0111111h; | 97% |
With erbium(III) triflate In nitromethane at 20℃; for 8h; | 97% |
Conditions | Yield |
---|---|
With quinolinium dichromate(VI) In acetonitrile for 1h; Heating; | 98% |
With water; silica gel; bis(trimethylsilyl)chromate In chloroform for 0.166667h; Heating; | 98% |
With benzyltriphenylphosphonium peroxodisulfate In acetonitrile for 0.1h; Heating; | 96% |
Conditions | Yield |
---|---|
Stage #1: 1-Chloro-4-iodobenzene With iodine; triethylamine; triphenylphosphine In dichloromethane; toluene at 20℃; for 0.0833333h; Sealed tube; Green chemistry; Stage #2: formic acid In dichloromethane; toluene at 70℃; for 1.5h; Catalytic behavior; Solvent; Reagent/catalyst; Temperature; Time; Sealed tube; Green chemistry; | 98% |
Stage #1: formic acid; 1-Chloro-4-iodobenzene With palladium diacetate; acetic anhydride; tricyclohexylphosphine In N,N-dimethyl-formamide at 30℃; for 1h; Inert atmosphere; Green chemistry; Stage #2: With triethylamine In N,N-dimethyl-formamide at 80℃; for 6h; Inert atmosphere; Green chemistry; | 95% |
With iodine; triethylamine; triphenylphosphine In toluene at 80℃; for 2h; Sealed tube; | 92% |
α-(2-cyano-1-methylethyl)-4,4'-dichlorobenzoin
A
4-(4-chlorophenyl)-3-methyl-4-oxobutyronitrile
B
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With potassium cyanide In N,N-dimethyl-formamide for 0.5h; Ambient temperature; | A 97% B n/a |
2-(4-chlorophenyl)-1,3-oxathiolane
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 2-(4-chlorophenyl)-1,3-oxathiolane In ethanol at 20℃; Stage #2: With water In ethanol at 20℃; | 97% |
With Iron(III) nitrate nonahydrate at 90℃; for 0.1h; | 92% |
With N-Bromosuccinimide; water In acetone at 20℃; for 0.25h; Hydrolysis; | 91% |
Conditions | Yield |
---|---|
With iron(III) p-toluenesulfonate hexahydrate In water for 1h; Reflux; | 97% |
With N-Bromosuccinimide In water; acetone at 20℃; for 18h; Ring cleavage; | 21 % Chromat. |
N-(4-chlorobenzylidene)-4-chlorobenzylamine
A
4-chlorobenzaldehyde
B
4-chlorobenzamide
Conditions | Yield |
---|---|
With manganese(IV) oxide In dichloromethane at 40℃; under 760.051 Torr; for 24h; Molecular sieve; | A 97% B 95% |
Conditions | Yield |
---|---|
With dihydrogen peroxide In water; acetonitrile at 25℃; for 10h; UV-irradiation; | 96% |
With 1H-imidazole; sodium periodate In water; acetonitrile at 20℃; for 30h; | 94% |
With potassium 12-tungstocobaltate(III) In water; acetonitrile for 0.233333h; Microwave irradiation; | 94% |
Conditions | Yield |
---|---|
indium(III) chloride In methanol; water for 1.08333h; Heating; | 96% |
With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile for 1h; Ambient temperature; | 92% |
With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile for 1h; Product distribution; Ambient temperature; other protected acetals; var. solvents and reaction times; | 92% |
4-chlorobenzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In isopropyl alcohol for 1.5h; Ambient temperature; stirred; | 96% |
(4-Chloro-phenyl)-phenylamino-methanesulfonic acid; compound with methylamine
A
4-chlorobenzaldehyde
B
(4-Chloro-phenyl)-phenylamino-methanesulfonic acid; compound with phenylamine
Conditions | Yield |
---|---|
With hydrogenchloride for 24h; | A n/a B 96% |
Conditions | Yield |
---|---|
With sodium tris(diethylamino)aluminum hydride In tetrahydrofuran; dodecane at -78℃; for 12h; | 96% |
With lithium-tris(diethylamino)hydridoaluminate In tetrahydrofuran at -78℃; for 3h; Reduction; | 90% |
Multi-step reaction with 2 steps 1: chlorobis(cyclooctene)-iridium(I) dimer / dichloromethane / 1 h / 50 °C / Inert atmosphere 2: hydrogenchloride / diethyl ether; water / 0.5 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere 2: pyridinium chlorochromate / dichloromethane View Scheme |
3-Methyl-2-thioxo-thiazolidin-4-on
4-chlorobenzaldehyde
5-(4-chlorophenylmethylene)-3-methyl-4-oxo-2-thioxothiazolidine
Conditions | Yield |
---|---|
With sodium acetate In methanol for 0.416667h; Heating; | 100% |
With acetic acid; triethylamine In ethyl acetate at 85℃; for 3h; | 96% |
With aluminum oxide; potassium fluoride In solid for 0.0666667h; microwaves (350 W); | 94% |
Conditions | Yield |
---|---|
With ammonium acetate at 110℃; for 96h; | 100% |
With ammonium acetate Henry reaction; Reflux; | 92% |
With (2-hydroxyethyl)ammonium formate at 20℃; for 2.1h; Knoevenagel condensation; Ionic liquid; | 90% |
Conditions | Yield |
---|---|
With copper(II) ferrite In dimethyl sulfoxide at 120℃; for 0.0333333h; Microwave irradiation; | 100% |
With bridged diamino-functionalized periodic mesoporous organosilicas with high nitrogen contents at 90℃; for 5h; Henry Nitro Aldol Condensation; | 99% |
With acetic acid; benzylamine at 78 - 80℃; for 3.5h; Product distribution / selectivity; | 97.1% |
Conditions | Yield |
---|---|
With polymer supported 4-DMAP at 20℃; for 0.416667h; Reagent/catalyst; Henry Nitro Aldol Condensation; | 100% |
With triethylamine at 80℃; for 0.0166667h; Henry reaction; microwave irradiation; | 99% |
With Musca acuminata (banana) peel ash In neat (no solvent) at 20℃; for 0.333333h; Henry Nitro Aldol Condensation; Green chemistry; | 98% |
4-chlorobenzaldehyde
4-methoxy-aniline
N-(4-chlorobenzylidene)-4-methoxyaniline
Conditions | Yield |
---|---|
for 6h; Ambient temperature; | 100% |
In ethanol for 1h; Sonication; | 100% |
at 20℃; for 14h; Molecular sieve; | 99% |
Conditions | Yield |
---|---|
With acetic acid In 1,2-dichloro-ethane at 20℃; for 24h; Inert atmosphere; | 100% |
With formic acid In ethanol; water at 20℃; for 0.0166667h; Green chemistry; | 99% |
at 20℃; for 14h; Molecular sieve; | 98% |
Conditions | Yield |
---|---|
With sodium hydrogensulfite In N,N-dimethyl acetamide at 100℃; for 2h; | 100% |
With copper(II) particles immobilized on nanosilica thiolated dendritic polymer In ethyl acetate at 50℃; for 0.25h; Catalytic behavior; Solvent; Temperature; Time; Reagent/catalyst; | 100% |
With sodium metabisulfite In N,N-dimethyl-formamide at 80℃; for 0.1h; Microwave irradiation; | 99% |
4-chlorobenzaldehyde
benzylamine
N-(4-chlorobenzylidene)benzylamine
Conditions | Yield |
---|---|
for 6h; Molecular sieve; Reflux; | 100% |
In ethanol at 20℃; | 94% |
In dichloromethane at 20℃; for 16h; Molecular sieve; | 92% |
4-chlorobenzaldehyde
2-hydroxyethanethiol
2-(4-chlorophenyl)-1,3-oxathiolane
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In diethyl ether for 3h; Heating; | 100% |
With zirconium(IV) chloride In dichloromethane at 20℃; for 0.333333h; Cyclization; Condensation; Monothioacetalization; | 97% |
TiCl4 on montmorillonite In dichloromethane for 0.5h; Heating; | 97% |
Conditions | Yield |
---|---|
at 150℃; for 1h; Knoevenagel condensation; | 100% |
hydrotalcite structure integrating fluoride ions In DMF (N,N-dimethyl-formamide) at 25℃; for 0.25h; Conversion of starting material; Knoevenagel Condensation; | 100% |
With 1-butyl-1,4-diazabicyclo[2.2.2]octanylium hydrotetrafluoroborate In water at 20℃; for 0.0333333h; Knoevenagel condensation; | 100% |
4-chlorobenzaldehyde
diethyl malonate
diethyl 4-chlorobenzylidenemalonate
Conditions | Yield |
---|---|
With C16H14MnN2O2(1+)*[(Si3Mg5.5Li0.3)O20(OH)4](1-) In toluene at 120℃; for 72h; Knoevenagel Condensation; Inert atmosphere; | 100% |
With 3-hydroxyethylammonium-n-propanesulfonate In water at 70℃; for 0.25h; Knoevenagel condensation; | 92% |
With piperidine; acetic acid In ethanol at 110℃; for 48h; Knoevenagel Condensation; | 92% |
4-chlorobenzaldehyde
1,2-bis(4-chlorophenyl)-1,2-ethandiol
Conditions | Yield |
---|---|
With aluminium; potassium hydroxide In methanol at 0℃; for 1h; Inert atmosphere; | 100% |
With tris(2,2’-bipyridine)ruthenium(II); sodium dodecyl-sulfate; ascorbate In water for 3h; pH=12.7; Irradiation; | 100% |
With ZnIn2S4; triethylamine In water; acetonitrile for 0.5h; Sealed tube; Sonication; Irradiation; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With potassium hydroxide; tris-(dibenzylideneacetone)dipalladium(0); tert-butyl XPhos In 1,4-dioxane; water at 80℃; for 18h; | 100% |
With [(2-di-tert-butylphosphino-3-methoxy-6-methyl-2,4,6-triisopropyl-1,1-biphenyl)-2-(2-aminobiphenyl)]palladium(II) methanesulfonate; caesium carbonate; Benzaldoxime In N,N-dimethyl-formamide at 80℃; for 18h; Inert atmosphere; Glovebox; Sealed tube; | 99% |
With trans-di(μ-acetato)bis[o-(di-o-tolyl-phosphino)benzyl]dipalladium(II); C29H45Pt; potassium carbonate In water; N,N-dimethyl-formamide at 115℃; for 0.5h; Inert atmosphere; Microwave irradiation; | 93% |
Conditions | Yield |
---|---|
With magnesium(II) perchlorate; polymer-bound NADH (2a) In acetonitrile; benzene at 80℃; for 120h; Further byproducts given; | 100% |
With diisopropoxytitanium(III) tetrahydroborate In dichloromethane at -20℃; for 0.133333h; | 100% |
With zirconium dioxide hydrate; isopropyl alcohol at 60℃; for 0.133333h; Meerwein-Ponndorf-Verley Reduction; | 100% |
Conditions | Yield |
---|---|
With sodium perborate In acetic acid for 1.5h; steam bath; | 100% |
With hydrogen bromide; oxygen In acetonitrile at 20℃; for 5h; UV-irradiation; | 100% |
With C4H11FeMo6NO24(3-)*3C16H36N(1+); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 8h; Green chemistry; | 99% |
4-amino-phenol
4-chlorobenzaldehyde
4-{[(4-chlorophenyl)methylidene]amino}phenol
Conditions | Yield |
---|---|
for 24h; Ambient temperature; | 100% |
With piperidine In ethanol Condensation; Heating; | 85% |
With dodecatungstosilic acid; phosphorus pentoxide In neat (no solvent, solid phase) at 20℃; | 82% |
Conditions | Yield |
---|---|
antimony(III) chloride; iron for 12h; Ambient temperature; | 100% |
Ce(3+)-mont at 25℃; for 12h; | 99% |
With 1-Benzyl-3,5-bis(methoxycarbonyl)pyridin-1-ium Bromide at 20℃; for 24h; Inert atmosphere; | 99% |
4-chlorobenzaldehyde
acrylonitrile
2-[(4-chlorophenyl)hydroxymethyl]acrylonitrile
Conditions | Yield |
---|---|
With octanol; 1,4-diaza-bicyclo[2.2.2]octane at 20℃; for 12h; Baylis-Hillman reaction; | 100% |
With 1,4-diaza-bicyclo[2.2.2]octane; 1-methyl-3-butyl-1,2,3-triazolium hexafluorophosphate at 20℃; Baylis-Hillman reaction; Inert atmosphere; Ionic liquid; | 99% |
With 1,4-diaza-bicyclo[2.2.2]octane at 20℃; for 1.2h; Baylis-Hillman reaction; neat (no solvent); | 99% |
4-chlorobenzaldehyde
Dimethyl phosphite
dimethyl 1-hydroxy-1-(4-chlorophenyl)methylphosphonate
Conditions | Yield |
---|---|
With triethylamine at 50℃; Pudovik Reaction; Inert atmosphere; Sealed tube; | 100% |
Stage #1: 4-chlorobenzaldehyde With phosphotungstic acid supported on silica-coated magnetic Fe3O4 nanoparticle In neat (no solvent) at 20℃; for 0.25h; Kabachnik-Fields Reaction; Green chemistry; Stage #2: Dimethyl phosphite In neat (no solvent) at 20℃; for 4h; Green chemistry; | 96% |
With potassium phosphate In neat (no solvent) at 20℃; for 0.0666667h; Green chemistry; | 93% |
morpholine
4-chlorobenzaldehyde
4,4'-((4-chlorophenyl)methylene)dimorpholine
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate) In water at 20℃; for 0.0333333h; | 100% |
With boron trioxide In benzene at 50℃; for 2h; | 90% |
With potassium carbonate In dichloromethane at 20℃; | 80% |
In benzene Reflux; | 50% |
In water; methyl cyclohexane |
4-hydroxy[1]benzopyran-2-one
4-chlorobenzaldehyde
3,3'-(4-chlorophenylmethylene)-bis-4-hydroxycoumarin
Conditions | Yield |
---|---|
With glycerol-based carbon sulfonic acid In ethanol; water at 80℃; for 0.333333h; Solvent; Temperature; Concentration; | 100% |
With silica-supported Preyssler acid nanoparticles In ethanol at 25℃; for 0.333333h; | 99% |
With cholin hydroxide In water at 50℃; for 2h; | 99% |
4-amino-2,3-dimethyl-1-phenylpyrazolin-5-one
4-chlorobenzaldehyde
4-(4-chlorobenzylideneamino)-1,2-dihydro-1,5-dimethyl-2-phenylpyrazol-3-one
Conditions | Yield |
---|---|
at 20℃; for 1h; | 100% |
In ethanol Reflux; | 94.66% |
In ethanol at 20℃; for 0.0111111h; | 92% |
acetic anhydride
4-chlorobenzaldehyde
(acetyloxy)(4-chlorophenyl)methyl acetate
Conditions | Yield |
---|---|
With poly(4-vinylpyridine)-supported sulfuric acid In dichloromethane at 20℃; for 0.0833333h; Green chemistry; chemoselective reaction; | 100% |
1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione at 20℃; for 0.7h; | 99% |
copper(II) sulfate at 20℃; for 0.5h; | 99% |
1.3-propanedithiol
4-chlorobenzaldehyde
2-(4-chlorophenyl)-1,3-dithiane
Conditions | Yield |
---|---|
With lithium tetrafluoroborate at 25℃; for 3h; | 100% |
With perchloric acid; silica gel at 25 - 30℃; for 0.0166667h; | 100% |
With Lewis acid | 100% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 35 - 40℃; for 2.5h; | 100% |
With sodium hydroxide In ethanol | |
With sodium hydroxide In ethanol; water for 0.5h; Heating; |
Conditions | Yield |
---|---|
With antimony In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide for 15h; Heating; | 100% |
With water; tin(ll) chloride at 50℃; for 12h; Barbier reaction; | 98% |
With stannous fluoride In various solvent(s) for 1h; Ambient temperature; | 96% |
n-pentyl methyl ketone
4-chlorobenzaldehyde
(E)-1-(4-chlorophenyl)oct-1-en-3-one
Conditions | Yield |
---|---|
Stage #1: n-pentyl methyl ketone With piperidine In ethanol at 20℃; for 2h; Stage #2: 4-chlorobenzaldehyde In ethanol for 72h; Reflux; | 100% |
barium dihydroxide In ethanol for 1h; Heating; | 93% |
diisopropyl hydrogenphosphonate
4-chlorobenzaldehyde
[(4-chloro-phenyl)-hydroxy-methyl]-phosphonic acid diisopropyl ester
Conditions | Yield |
---|---|
With triethylamine In neat (no solvent) at 20℃; for 24h; Pudovik Reaction; Inert atmosphere; | 100% |
With triethylamine at 50℃; Pudovik Reaction; Inert atmosphere; Sealed tube; | 100% |
With potassium phosphate In neat (no solvent) at 20℃; for 0.1h; Green chemistry; | 96% |
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