DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:873-76-7
Min.Order:1 Kilogram
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inquiryItems Standard Result Assay 98%min -----------------------------------------------------------------------------------------------
Cas:873-76-7
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Manufacturers
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Min.Order:5 Kiloliter
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Type:Manufacturers
inquiryOur advantage:Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scient
Cas:873-76-7
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:873-76-7
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Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Min.Order:1 Kilogram
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:873-76-7
Min.Order:10 Kilogram
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inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
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Type:Trading Company
inquiryWe are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED interme
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Min.Order:1 Kilogram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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Min.Order:0 Metric Ton
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Cas:873-76-7
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inquirylower price 873-76-7 4-Chlorobenzyl alcohol manufacturerAppearance:off-white powder Storage:dry place Package:according to customers' requirements Application:pharma intermediate Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB
Cas:873-76-7
Min.Order:1 Gram
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Type:Other
inquiryProduct name: 4-Chlorobenzyl Alcohol CAS No.:873-76-7 Molecule Formula:C7H7ClO Molecule Weight:142.58 Purity: 99% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:873-76-7
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Name: 4-Chlorobenzyl alcohol CAS: 873-76-7 MF: C7H7ClO MW: 142.58 EINECS: 212-852-2 Mol File: 873-76-7.mol 4-Chlorobenzyl alcohol Structure 4-Chlorobenzyl alcohol Chemical Properties Melting point 68-71 °C(lit.) Bo
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Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:873-76-7
Min.Order:1 Gram
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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Min.Order:1 Metric Ton
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Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Superior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:873-76-7
Min.Order:1 Metric Ton
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Type:Trading Company
inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermediat
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:873-76-7
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Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Conditions | Yield |
---|---|
With magnesium(II) perchlorate; polymer-bound NADH (2a) In acetonitrile; benzene at 80℃; for 120h; Further byproducts given; | 100% |
With diisopropoxytitanium(III) tetrahydroborate In dichloromethane at -20℃; for 0.133333h; | 100% |
With zirconium dioxide hydrate; isopropyl alcohol at 60℃; for 0.133333h; Meerwein-Ponndorf-Verley Reduction; | 100% |
Conditions | Yield |
---|---|
With C25H42N6Rh(1+)*CF3O3S(1-); phenylsilane In tetrahydrofuran at 30℃; for 20h; Inert atmosphere; | 100% |
With samarium diiodide; benzaldehyde; samarium(III) trifluoromethanesulfonate In tetrahydrofuran; methanol; water at 20℃; for 0.0166667h; Reduction; | 99% |
With samarium diiodide; phosphoric acid In tetrahydrofuran for 0.000833333h; Ambient temperature; | 94% |
Conditions | Yield |
---|---|
With C39H39N6ORu(1+)*Br(1-); potassium methanolate; hydrogen In tetrahydrofuran at 70℃; under 37503.8 Torr; for 4h; Reagent/catalyst; | 100% |
With C56H70Cl3N10Ru2(1+)*F6P(1-); potassium tert-butylate; hydrogen In tetrahydrofuran; dodecane at 70℃; under 37503.8 Torr; for 16h; Inert atmosphere; Glovebox; Autoclave; | 100% |
With C13H34BFeNOP2; hydrogen In tetrahydrofuran at 60℃; under 22502.3 Torr; for 18h; Autoclave; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With N-methylpyrrolidine zinc borohydride In tetrahydrofuran at 20℃; for 1.16667h; | 100% |
With Zr(BH4)2Cl2(dabco)2 In tetrahydrofuran for 1.7h; Heating; | 98% |
With sodium tetrahydroborate; lithium perchlorate In acetonitrile for 0.666667h; | 95% |
4-chlorobenzoic anhydride
A
para-Chlorobenzyl alcohol
B
para-chlorobenzoic acid
Conditions | Yield |
---|---|
With methanol; sodium tetrahydroborate In tetrahydrofuran for 1h; Ambient temperature; | A 94% B 100% |
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With water | 100% |
2-(4-chlorobenzyloxy)tetrahydro-2H-pyran
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
silica-supported prop-1-ylsulfonic acid In methanol | 99.4% |
With sulfuric acid; silica gel In methanol at 20℃; for 0.5h; | 98% |
With lithium borohydride In methanol at 20℃; for 0.416667h; | 96% |
Conditions | Yield |
---|---|
With samarium diiodide; water In tetrahydrofuran for 0.00277778h; Ambient temperature; | 99% |
With C24H20ClN2OPRu; potassium tert-butylate; hydrogen In tetrahydrofuran at 110℃; under 10640.7 Torr; for 36h; Inert atmosphere; Schlenk technique; | 85% |
With [fac-8-(2-diphenylphosphinoethyl)aminotrihydroquinoline]RuH(η1-BH4)(CO); hydrogen In isopropyl alcohol at 140℃; under 37503.8 Torr; for 24h; Autoclave; | 62 %Chromat. |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; hafnium tetrachloride In tetrahydrofuran at 20℃; for 5.6h; Inert atmosphere; Cooling with ice; | 98% |
With phenylsilane; potassium tert-butylate; water; sodium triethylborohydride; cobalt(II) chloride In 1,4-dioxane; toluene at 60℃; for 15h; Inert atmosphere; Glovebox; Schlenk technique; | 98% |
With C30H34Cl2N2P2Ru; potassium methanolate; hydrogen In tetrahydrofuran at 100℃; under 38002.6 - 76005.1 Torr; for 15h; Glovebox; Autoclave; | 96% |
Conditions | Yield |
---|---|
With methanol; potassium permanganate at 25℃; chemoselective reaction; | 98% |
With methanol; [Dy2((2-hydroxy-3-methoxyphenyl)methylene benzohydrazide)2(triflate)2(H2O)4] for 40h; Reflux; Inert atmosphere; chemoselective reaction; | 81% |
With water In acetonitrile for 0.166667h; Quantum yield; Irradiation; |
4-chlorobenzyltrimethylsilyl ether
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With poly (ethylene glycol)-sulfonated sodium montmorillonite nanocomposite In methanol at 20℃; for 0.0333333h; | 98% |
With methanol; 1,3-disulfonic acid imidazolium hydrogen sulfate at 20℃; for 0.0666667h; Green chemistry; | 96% |
With rice husk ash supported on anatase-phase titania nanoparticles nanocomposite In methanol at 20℃; for 0.05h; | 96% |
4-chlorobenzaldehyde
benzyl-methyl-amine
A
(4'-chlorobenzyl) 4-chlorobenzoate
B
N-benzyl-4-chloro-N-methylbenzamide
C
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
tris(bis(trimethylsilyl)amido)lanthanum(III) In benzene-d6 at 25℃; for 24h; | A n/a B 98% C n/a |
Conditions | Yield |
---|---|
With 1-methylimidazole hydrogen sulfate at 120℃; for 0.0166667h; Microwave irradiation; chemoselective reaction; | 97% |
phosphotungstic acid In ethanol for 4.5h; Heating; | 87% |
4-chlorobenzaldehyde
aniline
A
4-chlorobenzanilide
B
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
Stage #1: aniline With n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere; Stage #2: 4-chlorobenzaldehyde With yttrium(III) chloride In toluene at 20℃; for 48h; Cannizzaro reaction; Inert atmosphere; Stage #3: With hydrogenchloride In water; toluene at 20℃; Inert atmosphere; | A 97% B n/a |
4-chlorobenzaldehyde
isopropyl alcohol
A
acetone
B
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With titanium(IV) oxide at 24.84℃; Meerwein-Ponndorf-Verley Reduction; Sealed tube; UV-irradiation; Inert atmosphere; Green chemistry; chemoselective reaction; | A 96% B 87% |
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With sodium hydroxide In water Schlenk technique; Inert atmosphere; | 96% |
With water; sodium hydroxide In benzene-d6 at 20℃; Glovebox; Inert atmosphere; | |
With sodium hydroxide In methanol for 2h; | |
With sodium hydroxide In water |
4-chlorobenzaldehyde
A
para-Chlorobenzyl alcohol
B
para-chlorobenzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-chlorobenzaldehyde With potassium hydroxide for 0.0833333h; Cannizzaro Reaction; Milling; Inert atmosphere; Sealed tube; Green chemistry; Stage #2: With hydrogenchloride In water Green chemistry; | A 95% B 95% |
With sodium hydroxide In water at 20℃; for 3.5h; Cannizzaro Reaction; | A n/a B 89% |
With TEA; magnesium bromide In dichloromethane at 20℃; for 48h; Cannizzaro reaction; | A 88% B n/a |
Conditions | Yield |
---|---|
With 1-methylimidazole hydrogen sulfate at 120℃; for 0.0166667h; Microwave irradiation; chemoselective reaction; | 95% |
phosphotungstic acid In ethanol for 4.5h; Heating; | 87% |
benzyloxy-trimethylsilane
4-chloro-1-[(ethoxymethoxy)methyl]benzene
A
para-Chlorobenzyl alcohol
B
benzyl alcohol
Conditions | Yield |
---|---|
With 1-methylimidazole hydrogen sulfate at 120℃; for 0.0166667h; Microwave irradiation; chemoselective reaction; | A 95% B 10% |
Benzyl acetate
4-chloro-1-[(ethoxymethoxy)methyl]benzene
A
para-Chlorobenzyl alcohol
B
benzyl alcohol
Conditions | Yield |
---|---|
With 1-methylimidazole hydrogen sulfate at 120℃; for 0.0166667h; Microwave irradiation; chemoselective reaction; | A 95% B 20% |
4-chlorobenzaldehyde p-toluenesulfonylhydrazone
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With water; potassium carbonate at 130℃; for 0.166667h; Microwave irradiation; | 95% |
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With sodium hydroxide In water Inert atmosphere; | 95% |
2-((4-chlorobenzyl)oxy)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With silica gel at 25℃; Inert atmosphere; Glovebox; | 95% |
With silica gel In methanol for 4h; Reflux; | 94% |
With silica gel In hexane; ethyl acetate | 92% |
4-[(chlorophenyl)methoxy](1,1-dimethylethyl)dimethylsilane
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With hafnium tetrakis(trifluoromethanesulfonate) In methanol at 20℃; for 7h; | 95% |
With hafnium tetrakis(trifluoromethanesulfonate) In methanol at 20℃; for 7h; | 95% |
With methanol at 20℃; for 2.33333h; | 95% |
4-chlorobenzoyl azide
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With zinc(II) tetrahydroborate In 1,2-dimethoxyethane for 5.5h; Ambient temperature; | 94% |
With Ca(BH2S3)2 In tetrahydrofuran for 2h; Heating; | 87% |
p-hydroxymethylphenylboronic acid
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With N-chloro-succinimide; copper(l) chloride In acetonitrile at 80℃; for 12h; | 94% |
With N-chloro-succinimide In acetonitrile at 80℃; for 16h; | 93% |
4-chlorobenzaldehyde
4-n-methylphenylacetylene
B
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With triethylamine; zinc(II) iodide In toluene at 80℃; for 12h; Schlenk technique; Inert atmosphere; | A 94% B n/a |
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With carbon tetrabromide In isopropyl alcohol for 2h; Heating; | 93% |
4-chlorobenzaldehyde
A
1,2-bis(4-chlorophenyl)-1,2-ethandiol
B
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
With vanadium(II) chloride In ethanol; water at 16 - 22℃; for 0.416667h; sonication; | A 92% B 2% |
With ammonium chloride; magnesium Ambient temperature; | A 90% B 7% |
With zinc(II) chloride; zinc In tetrahydrofuran; water for 3h; Ambient temperature; | A 16% B 82% |
acetophenone
para-Chlorobenzyl alcohol
3-(4-chlorophenyl)-1-phenylpropan-1-one
Conditions | Yield |
---|---|
With titanium(IV) oxide; potassium hydroxide In toluene at 100℃; for 10h; Sealed tube; Irradiation; | 100% |
With C27H24Cl3F6IrN2; potassium hydroxide In toluene at 130℃; for 2h; | 94% |
With C16H14IrN2O3; caesium carbonate In tert-Amyl alcohol for 6h; Reflux; | 91% |
Conditions | Yield |
---|---|
With oxygen; perruthenate modified mesoporous silicate MCM-41 In toluene at 80℃; for 1h; Oxidation; | 100% |
With n-butyltriphenylphosphonium permanganate In acetonitrile at 20℃; for 0.25h; | 100% |
With butyltriphenylphosphonium chlorochromate In acetonitrile for 0.75h; Heating; | 100% |
Conditions | Yield |
---|---|
With tetrachloromethane; cross-linked polymer (containing 2.50 mmol of phosphine/g) for 3h; Heating; | 100% |
With ziconium(IV) oxychloride octahydrate; lithium chloride In ethanol; water at 90℃; for 1.5h; | 95% |
With 1,3,5-trichloro-2,4,6-triazine; dimethyl sulfoxide at 20℃; for 0.25h; chemoselective reaction; | 94% |
1,1,1,3,3,3-hexamethyl-disilazane
para-Chlorobenzyl alcohol
4-chlorobenzyltrimethylsilyl ether
Conditions | Yield |
---|---|
With aluminum potassium sulfate dodecahydrate In acetonitrile at 20℃; for 0.333333h; | 100% |
With 1,3-disulfonic acid imidazolium hydrogen sulfate In neat (no solvent) at 20℃; for 0.0166667h; Green chemistry; | 100% |
With asymmetric salen type di-Schiff base-based zinc complex supported on Fe3O4 nanoparticles at 20℃; for 0.2h; | 100% |
Conditions | Yield |
---|---|
(NH4)8[CeW10O36]*20H2O for 0.0833333h; Heating; | 100% |
With SBA-15-Ph-Pr-SO3H at 20℃; for 0.333333h; | 100% |
With tin(IV) tetraphenylporphyrin perchlorate at 20℃; for 0.0833333h; | 99% |
Conditions | Yield |
---|---|
With bromine; oxygen In acetonitrile for 10h; Irradiation; | 100% |
With periodic acid; tripropylammonium fluorochromate (VI) In acetonitrile at 0℃; | 99% |
With silica-supported Jones reagent In dichloromethane for 0.035h; | 99.4% |
Dimethoxymethane
para-Chlorobenzyl alcohol
1-chloro-4-[(methoxymethoxy)methyl]benzene
Conditions | Yield |
---|---|
With N,N,N’,N’-tetrabromobenzene-1,3-disulfonamide at 20℃; for 1.2h; | 100% |
With zirconyl triflate at 20℃; for 0.166667h; neat (no solvent); chemoselective reaction; | 100% |
With 12-tungstophosphoric acid immobilized on [bmim][FeCl4] at 75 - 82℃; for 0.00555556h; Microwave irradiation; | 98% |
Conditions | Yield |
---|---|
With ammonium hydroxide; oxygen In tert-Amyl alcohol at 130℃; under 3750.38 Torr; for 24h; | 100% |
Stage #1: para-Chlorobenzyl alcohol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine In dichloromethane at 20℃; for 1h; Inert atmosphere; Stage #2: With ammonia; iodine In dichloromethane; water at 20℃; for 2h; Inert atmosphere; | 99% |
With ammonia; oxygen In tert-Amyl alcohol; water at 100℃; under 3750.38 Torr; for 5h; Autoclave; High pressure; | 99% |
1-hydroxy-pyrrolidine-2,5-dione
para-Chlorobenzyl alcohol
4-chlorobenzoic acid N-hydroxysuccinimide ester
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; benzoic acid In ethyl acetate for 0.5h; cooling; | 100% |
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide In decane; acetonitrile at 80℃; for 18h; Solvent; | 92% |
With tert.-butylhydroperoxide; oxygen In acetonitrile for 24h; Irradiation; Sealed tube; | 52% |
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate) at 100℃; for 0.0833333h; Microwave irradiation; | 100% |
para-Chlorobenzyl alcohol
1,1'-carbonyldiimidazole
4-chlorobenzyl 4-[3-oxo-3-(2-oxo-2,3-dihydrobenzoxazol-6-yl)propyl]piperazine-1-carboxylate
Conditions | Yield |
---|---|
Stage #1: para-Chlorobenzyl alcohol; 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide at 20℃; for 3h; Stage #2: C14H17N3O3*ClH In N,N-dimethyl-formamide at 20℃; for 18h; | 100% |
1-Phenylethanol
para-Chlorobenzyl alcohol
3-(4-chlorophenyl)-1-phenylpropan-1-one
Conditions | Yield |
---|---|
With Cu-Ag supported on hydrotalcite In o-xylene at 150℃; for 8h; Inert atmosphere; | 100% |
With C44H35ClO4P2Ru; potassium hydroxide In para-xylene at 130℃; for 24h; Reagent/catalyst; Inert atmosphere; Schlenk technique; Molecular sieve; | 95% |
With C44H35ClO4P2Ru; sodium sulfate; potassium hydroxide In toluene at 150℃; for 24h; Inert atmosphere; Schlenk technique; chemoselective reaction; | 95% |
Conditions | Yield |
---|---|
In water; toluene for 24h; Reflux; Dean-Stark; | 100% |
3,4-dihydro-2H-pyran
para-Chlorobenzyl alcohol
2-(4-chlorobenzyloxy)tetrahydro-2H-pyran
Conditions | Yield |
---|---|
silica-supported prop-1-ylsulfonic acid In acetonitrile for 0.166667h; | 99.9% |
With chloromethylated polystyrene supported tetrakis(p-aminophenyl)porphyrinatotin(IV) trifluoromethanesulfonate In tetrahydrofuran at 20℃; for 0.1h; | 99% |
With mesoporous p-hydroxybenzenesulphonic acid-formaldehyde polymer resin In neat (no solvent) at 20℃; for 1.15h; chemoselective reaction; | 97% |
Conditions | Yield |
---|---|
In toluene for 5h; Heating; | 99.5% |
4-chloro-aniline
para-Chlorobenzyl alcohol
4-chloro-N-(4-chlorobenzyl)aniline
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In toluene at 110℃; for 48h; Inert atmosphere; | 99% |
Stage #1: 4-chloro-aniline; para-Chlorobenzyl alcohol With (1,3-bis(2,6-di-iso-propylphenyl)-4,5-dihydroimidazol-2-ylidene) copper chloride; potassium tert-butylate; oxygen In tetrahydrofuran at 20℃; for 6h; Molecular sieve; Stage #2: With (1,3-bis(2,6-di-iso-propylphenyl)-4,5-dihydroimidazol-2-ylidene) copper chloride In tetrahydrofuran at 20℃; for 8h; Molecular sieve; | 94% |
With C51H40Cl2N2O3P2Ru; potassium hydroxide In toluene at 120℃; for 14h; | 84% |
Conditions | Yield |
---|---|
With hydrazine hydrate; C23H40MnNO2P2; potassium tert-butylate In tert-butyl alcohol at 115℃; for 48h; Wolff-Kishner Reduction; Green chemistry; | 99% |
With carbon monoxide; hydrogen; benzene at 190℃; under 176522 Torr; Reagens 4: Octacarbonyldikobalt, Reagens 5: Kobaltcarbonat; | |
With 2,4,6-trimethyl-pyridine; 4,4'-dimethoxyphenyl disulfide; iridium(lll) bis[2-(2,4-difluorophenyl)-5-methylpyridine-N,C20]-4,40-di-tert-butyl-2,20-bipyridine hexafluorophosphate; triphenylphosphine In toluene for 24h; Irradiation; | 74 %Chromat. |
Conditions | Yield |
---|---|
Stage #1: para-Chlorobenzyl alcohol With 1,2,3-Benzotriazole; thionyl chloride In dichloromethane Stage #2: With potassium bromide In dichloromethane; N,N-dimethyl-formamide for 0.266667h; | 99% |
With N-Bromosuccinimide; triphenylphosphine for 0.00277778h; microwave irradiation; | 98% |
With bromine; triphenylphosphine In dichloromethane at -78 - 20℃; for 18h; Inert atmosphere; | 97% |
para-Chlorobenzyl alcohol
1-chloro-4-(iodomethyl)benzene
Conditions | Yield |
---|---|
Stage #1: para-Chlorobenzyl alcohol With 1,2,3-Benzotriazole; thionyl chloride In dichloromethane Stage #2: With potassium iodide In dichloromethane; N,N-dimethyl-formamide for 0.0833333h; | 99% |
With bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; hydrogen; iodine; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,2-dichloro-ethane at 20℃; under 22502.3 Torr; Autoclave; Schlenk technique; | 99% |
With bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; Ru(OCOCH3)2{(S)-2,2'-bis(diphenylphosphino)-1,1'-dinaphthyl)}; hydrogen; iodine In toluene at 20℃; under 22502.3 Torr; for 5.5h; | 99% |
para-Chlorobenzyl alcohol
C20H21N3O6S
1-benzyloxycarbonyl-2-tert-butyloxycarbonyl-1-(4-chlorobenzyl)-2-(4-cyanobenzenesulfonyl)-hydrazine
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran | 99% |
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran Mitsunobu reaction; | 99% |
Conditions | Yield |
---|---|
With bismuth(lll) trifluoromethanesulfonate at 20℃; for 0.583333h; | 99% |
With potassium fluoride at 80℃; for 3h; | 97% |
With 50wtpercent Cs2.5H0.5PW12O40 supported on MCM-41 In acetonitrile at 50℃; for 0.5h; | 97% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
2-Nitrobenzenesulfonyl chloride
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
Multistep reaction; | 99% |
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