As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for
Cas:106-86-5
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inquiry4-Vinyl-1-Cyclohexene 1,2-Epoxide reactive through its vinyl or epoxide functionalities, is useful as chemical intermediate. It also serves as reactive diluent where high crosslink density is not critical. Appearance:Transparent Liquid Application:
Cas:106-86-5
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inquiryItems Standard Result Appearance Colorless, transparent liquid Colorless, transparent liquid Assay,GC
Cas:106-86-5
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:106-86-5
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Type:Manufacturers
inquiryOur advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be sent
Cas:106-86-5
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inquiryName: 4-Vinyl-1-Cyclohexene 1,2-Epoxide CAS:106-86-5 Appearance:colorless liquid Appearance:colorless liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg Application: UV/EB Monomer Transportation:By sea P
Cas:106-86-5
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:106-86-5
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:106-86-5
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inquiryAppearance:Colorless to Almost colorless clear liquid Storage:room temperature Package:200kg/Drum Application:Chemicals Transportation:Express/Sea/Air Port:Any port in China
Cas:106-86-5
Min.Order:1 Kilogram
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:106-86-5
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:106-86-5
Min.Order:10 Kilogram
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inquiryBeluga chemical professional supply 1,2-Epoxy-4-vinylcyclohexane (mixture of isomers) CAS106-86-5 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities.
Cas:106-86-5
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:106-86-5
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inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Cas:106-86-5
Min.Order:10 Gram
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Type:Trading Company
inquiry1, 2-Epoxy-4-Vinylcyclohexane CAS:106-86-5 Specification Product name 1,2-Epoxy-4-vinylcyclohexane Cas number 106-86-5 Molecular formula C8H12O Appearance Colorless to Almost
Cas:106-86-5
Min.Order:1 Kilogram
Negotiable
Type:Other
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:106-86-5
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inquiryProduct quality: Our company have high quality product , and also the product we have good manufacture . First of all, this product is of fine quality. Every finish should be checked by quality inspection system.And every one should be also tried
Cas:106-86-5
Min.Order:1 Metric Ton
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Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:106-86-5
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inquiryOur Advantages Production: Advanced chemical equipment with years of experience Staffs for producing various extract products. Quality Control:A complete set of Testing Professional and Analysis Equipment ensures the Quality Requirements and Specif
Cas:106-86-5
Min.Order:1 Kilogram
FOB Price: $75.0 / 150.0
Type:Trading Company
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:106-86-5
Min.Order:1 Gram
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:106-86-5
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:106-86-5
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:106-86-5
Min.Order:10 Gram
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:106-86-5
Min.Order:100 Gram
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inquirySuperior quality, moderate price & quick delivery. Appearance:Colorless transparent liquid Storage:Store in a cool and ventilated place, away from fire and heat Package:as per your request Application:Can be widely used in the organosilicon
Cas:106-86-5
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Name: 1,2-Epoxy-4-vinylcyclohexane Synonyms: 1,2-EPOXY-4-VINYLCYCLOHEXANE;3-VINYL-7-OXABICYCLO[4.1.0] HEPTANE;3-ETHENYL-7-OXABICYCLO[4.1.0]HEPTANE;4-VINYL-1-CYCLOHEXENE 1,2-EPOXIDE;Vinyl cyclohexane monoxide;VINYL(4-)-1-CYCLOHE
Cas:106-86-5
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:106-86-5
Min.Order:1 Metric Ton
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Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With [(C18H37)2(CH3)2N]3[SiO4H(WO5)3]; dihydrogen peroxide In ethyl acetate at 59.84℃; for 2h; Green chemistry; | 99% |
With tert.-butylhydroperoxide at 79.84℃; Reagent/catalyst; Temperature; Green chemistry; | 95% |
With 3-chloro-benzenecarboperoxoic acid In benzene at 20℃; for 0.5h; | 94% |
1,1,3,3-tetrachloropropanone
4-ethenylcyclohexene
A
4-vinylcyclohexene dioxide
B
1,2-Epoxy-4-vinylcyclohexane
C
7,8-Epoxy-1-Cyclohexene
D
tetrachloroacetone hydrate
Conditions | Yield |
---|---|
With disodium hydrogenphosphate; dihydrogen peroxide In chloroform for 24h; Ambient temperature; | A 2% B 60% C 2.5% D n/a |
With disodium hydrogenphosphate; dihydrogen peroxide In chloroform for 24h; Ambient temperature; | A 2% B 60% C 1.5% D n/a |
4-ethenylcyclohexene
A
1,2-Epoxy-4-vinylcyclohexane
B
3,4-dihydroxy-1-vinylcyclohexane
Conditions | Yield |
---|---|
With dihydrogen peroxide; magnesium sulfate; methyltrioxorhenium(VII) In tert-butyl alcohol at 15℃; for 2h; | A 50% B 40% |
With dihydrogen peroxide; magnesium sulfate; methyltrioxorhenium(VII) In tert-butyl alcohol at 15℃; for 2h; | A 40% B 50% |
With dihydrogen peroxide; acetic acid In water at 70℃; for 4h; Temperature; |
4-ethenylcyclohexene
A
4-vinylcyclohexene dioxide
B
1,2-Epoxy-4-vinylcyclohexane
C
7,8-Epoxy-1-Cyclohexene
Conditions | Yield |
---|---|
With dimethylammonium tetrakis(diperoxotungsto)phosphate; dihydrogen peroxide In benzene at 60℃; for 1h; | A 3 % Chromat. B 83 % Chromat. C 2 % Chromat. |
With dihydrogen peroxide; cetylpyridinium bromide; H3PMo10W2O40 In acetonitrile at 60℃; for 3h; Product distribution; Further Variations:; Catalysts; Solvents; Temperatures; |
4-ethenylcyclohexene
A
1,2-Epoxy-4-vinylcyclohexane
B
7,8-Epoxy-1-Cyclohexene
C
3,4-dihydroxy-1-vinylcyclohexane
Conditions | Yield |
---|---|
With [π-C5H5N(+)(CH2)15CH3]3(PMo12O40)(3-); dihydrogen peroxide; magnesium sulfate In chloroform at 60℃; for 24h; Yield given. Yields of byproduct given; |
4-ethenylcyclohexene
A
1,2-Epoxy-4-vinylcyclohexane
B
4-Vinylcyclohex-1-en-4-ol
trans-4-Vinylcyclohex-1-en-3-ol
trans-4-Vinylcyclohex-1-en-6-ol
cis-4-Vinylcyclohex-1-en-6-ol
cis-3-Vinylcyclohex-1-en-6-ol
Conditions | Yield |
---|---|
With oxygen; sodium sulfite Product distribution; multistep reaction: 1) 80 deg C, 15 h, 101.3 kPa; | A 0.6 % Chromat. B 15.2 % Chromat. C 15.1 % Chromat. D 22.6 % Chromat. E 45.0 % Chromat. F n/a |
4-ethenylcyclohexene
A
1,2-Epoxy-4-vinylcyclohexane
trans-3-Hydroperoxy-4-vinylcyclohex-1-en
cis-6-Hydroperoxy-3-vinylcyclohex-1-en
D
4-Hydroperoxy-4-vinylcyclohex-1-en
trans-6-Hydroperoxy-4-vinylcyclohex-1-en
cis-6-Hydroperoxy-4-vinylcyclohex-1-en
Conditions | Yield |
---|---|
With oxygen at 80℃; under 759.8 Torr; for 15h; Product distribution; autoxidation; | A 4 % Chromat. B 13 % Chromat. C 6 % Chromat. D 13 % Chromat. E 18 % Chromat. F 45 % Chromat. |
4-ethenylcyclohexene
acetic acid
A
1,2-Epoxy-4-vinylcyclohexane
B
3,4-dihydroxy-1-vinylcyclohexane
Conditions | Yield |
---|---|
With MoOBr3; dihydrogen peroxide at 70℃; for 6h; Product distribution; other cyclohexene derivatives; other molybdenum complexes; |
4-ethenylcyclohexene
A
4-vinylcyclohexene dioxide
B
1,2-Epoxy-4-vinylcyclohexane
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; silica gel; molybdenum trioxide In decane at 50℃; for 12h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With air; bis(hexafluoroacetylacetonato)cobalt; isobutyraldehyde In 1,2-dichloro-ethane at 20℃; under 7600 Torr; for 24h; Product distribution; Further Variations:; Reagents; Pressures; | A 20 % Chromat. B 80 % Chromat. |
With air; bis(hexafluoroacetylacetonato)cobalt; isobutyraldehyde In 1,2-dichloro-ethane at 20℃; under 7600 Torr; for 24h; | A 20 % Chromat. B 80 % Chromat. |
With [Mn(CF3SO3)2(H,MePyTACN)]; dihydrogen peroxide; acetic acid In acetonitrile at 0℃; for 1.5h; chemoselective reaction; |
1,2-Epoxy-4-vinylcyclohexane
Conditions | Yield |
---|---|
With Perbenzoic acid; chloroform |
4-ethenylcyclohexene
A
1,2-Epoxy-4-vinylcyclohexane
B
7,8-Epoxy-1-Cyclohexene
Conditions | Yield |
---|---|
With dihydrogen peroxide; TBA-[γ-SiW10O34(H2O)2]4- In acetonitrile at 31.85℃; for 4h; Product distribution; Further Variations:; Catalysts; Reagents; | A 94 % Chromat. B 4 % Chromat. |
With peracetic acid; Mn3(2-pyridinal-1-phenylethylimine)2(OAc)6 In acetonitrile at 25℃; for 0.3h; Title compound not separated from byproducts; | |
With dihydrogen peroxide; teterabutylammonium In acetonitrile at 31.85℃; for 4h; | |
With iodosylbenzene; iron(III) tetraphenylporphyrin In dichloromethane at 25℃; for 0.5h; Product distribution; Further Variations:; Catalysts; |
methanol
4-ethenylcyclohexene
A
4-vinylcyclohexene dioxide
B
1,2-Epoxy-4-vinylcyclohexane
C
7,8-Epoxy-1-Cyclohexene
D
cyclohex-3-enyl acetaldehyde
E
3-cyclohexenyl-2-ethanone
G
C9H16O2
Conditions | Yield |
---|---|
With dihydrogen peroxide In water at 64.84℃; for 2h; regioselective reaction; |
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; 2BF4(1-)*C30H32N8O3Ru(2+) In dichloromethane at 20℃; for 24h; Inert atmosphere; Darkness; regioselective reaction; |
methanol
4-ethenylcyclohexene
A
4-vinylcyclohexene dioxide
B
1,2-Epoxy-4-vinylcyclohexane
C
7,8-Epoxy-1-Cyclohexene
E
C9H16O2
F
3-Cyclohexene-1-carboxaldehyde
Conditions | Yield |
---|---|
With dihydrogen peroxide In water at 65℃; for 1.5h; |
1,2-Epoxy-4-vinylcyclohexane
1,1,3,3-tetramethyl-1-(2-trimethylsilanylethyl)disiloxane
3-{2-[1,1,3,3-tetramethyl-3-(2-trimethylsilanylethyl)disiloxanyl]ethyl}-7-oxabicyclo[4.1.0]heptane
Conditions | Yield |
---|---|
With buffer; Karstedt's catalyst In toluene at 80 - 90℃; | 100% |
With dihydrogen hexachloroplatinate at 75 - 85℃; for 2h; |
1,2-Epoxy-4-vinylcyclohexane
Triethoxysilane
(2-(7-oxabicyclo[4.1.0]heptan-3-yl)ethyl)triethoxysilane
Conditions | Yield |
---|---|
With platinum-containing olefin organic polymer catalyst at 25℃; for 3h; | 99% |
With (TFAPDI)Co(2-ethylhexanoate)2 In neat (no solvent) at 23℃; for 1h; | 96% |
With (1-mesityl-3-methylimidazol-2-ylidene)Co(N(SiMe3)2)2 In neat (no solvent) at 20℃; for 8h; Inert atmosphere; Glovebox; chemoselective reaction; | 94% |
With graphene nanoplates-supported platinum nanoparticles In neat (no solvent) at 80℃; for 2h; Catalytic behavior; | 92% |
Conditions | Yield |
---|---|
With graphene nanoplates-supported platinum nanoparticles In neat (no solvent) at 80℃; for 2h; Catalytic behavior; | 98% |
With dihydrogen hexachloroplatinate at 75 - 85℃; for 2h; | 96% |
With dihydrogen hexachloroplatinate at 75 - 85℃; | 96% |
1,2-Epoxy-4-vinylcyclohexane
Conditions | Yield |
---|---|
With platinum In benzene at 20℃; for 34h; | 98% |
Conditions | Yield |
---|---|
With chloro(1,5-cyclooctadiene)rhodium(I) dimer In neat (no solvent) at 50℃; for 2h; | 98% |
1,2-Epoxy-4-vinylcyclohexane
1,1,3,3-Tetramethyldisiloxane
1,3-bis(2(3,4-epoxycyclohexyl)ethyl)-1,1,3,3-tetramethyldisiloxane
Conditions | Yield |
---|---|
In ethanol; toluene at 65℃; for 0.333333h; Temperature; Solvent; Reagent/catalyst; Inert atmosphere; Molecular sieve; Microwave irradiation; | 97.8% |
In tetrahydrofuran; ethanol at 75℃; for 4h; Reagent/catalyst; Temperature; Solvent; Molecular sieve; Inert atmosphere; | 96.9% |
2C8H18S*3Cl(1-)*Rh(3+) In ethanol; hexane at 82℃; for 3h; Heating / reflux; |
1,2-Epoxy-4-vinylcyclohexane
1,1,3,3,5,5,7,7-octamethyltetrasiloxane
(1,7-bis(1,2-epoxycyclohexyl-4-ethyl))-1,1,3,3,5,5,7,7-octamethyltetrasiloxane
Conditions | Yield |
---|---|
polymer-bound Wilkinson's catalyst In toluene at 100 - 115℃; for 48h; Heating / reflux; | 96% |
1,2-Epoxy-4-vinylcyclohexane
3,4-dihydroxy-1-vinylcyclohexane
Conditions | Yield |
---|---|
With water at 20℃; for 5h; Conversion of starting material; | 95% |
With water; Amberlyst 15 resin at 20℃; for 24h; Conversion of starting material; | 95% |
With sulfuric acid In water at 20℃; | 85% |
1,2-Epoxy-4-vinylcyclohexane
1-dimethylsiloxy-3,5,7,9,11,13,15-heptakis(trimethylsiloxy)pentacyclo[9.5.1.1(3,9).1(5,15).1(7,13)]-octasiloxane
Conditions | Yield |
---|---|
1,3-di(η2-vinyl)-1.1.3.3-tetramethyldisiloxane platinum(0) In toluene at 20℃; for 2h; | 95% |
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex In toluene at 40℃; for 12h; Schlenk technique; | 95% |
1,2-Epoxy-4-vinylcyclohexane
Conditions | Yield |
---|---|
With 2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine cobalt(II) dichloride; diethoxymethylane; sodium triethylborohydride In toluene at -78 - 20℃; for 5h; | 95% |
1,2-Epoxy-4-vinylcyclohexane
dimethylmethoxysilane
Conditions | Yield |
---|---|
With C24H30ClN3NiO2; sodium t-butanolate In tetrahydrofuran at 20℃; for 6h; Inert atmosphere; Glovebox; | 93% |
1,2-Epoxy-4-vinylcyclohexane
Conditions | Yield |
---|---|
With aluminum oxide; thiourea In water at 25℃; for 2h; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With potassium hydroxide In toluene at 20 - 105℃; for 18h; Reagent/catalyst; Temperature; Solvent; | 93% |
1,2-Epoxy-4-vinylcyclohexane
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex In 5,5-dimethyl-1,3-cyclohexadiene; toluene at 90℃; for 3h; | 92% |
Conditions | Yield |
---|---|
With C77H70N2OPtSi2 In toluene at 80℃; for 24h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Sealed tube; regioselective reaction; | 91% |
1,2-Epoxy-4-vinylcyclohexane
trimethoxysilane
trimethoxy[2-(7-oxabicyclo[4.1.0]-hept-3-yl)ethyl]silane
Conditions | Yield |
---|---|
chloroplatinic acid | 90% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In neat (no solvent) at 100℃; for 18h; chemoselective reaction; | 90% |
In neat (no solvent) at 90℃; under 3750.38 Torr; for 24h; Autoclave; | 83% |
With C37H41FeN6O2(1+)*I(1-); bis(triphenylphosphine)iminium chloride In neat (no solvent) at 80℃; under 3750.38 Torr; for 24h; Autoclave; | 76% |
Conditions | Yield |
---|---|
With C20H13FeN2O5; tetrabutylammomium bromide at 100℃; under 3750.38 - 7500.75 Torr; for 18h; Sealed tube; | 90% |
Conditions | Yield |
---|---|
Stage #1: 4-allylguaiacol; octakis(dimethylsiloxy)octasilsesquioxane With bis(1,5-cyclooctadiene)diiridium(I) dichloride; Karstedt's catalyst In toluene at 90℃; Stage #2: 1,2-Epoxy-4-vinylcyclohexane In toluene at 90℃; | 89% |
Conditions | Yield |
---|---|
With [(N(C6H4N(CH3)2)2)Ni(OCH3)] In tetrahydrofuran at 20℃; for 6h; Inert atmosphere; Glovebox; Sealed tube; chemoselective reaction; | 88% |
Stage #1: 1,2-Epoxy-4-vinylcyclohexane; diphenylsilane With bis(acetylacetonate)nickel(II) In tetrahydrofuran at 20℃; for 0.0166667h; Inert atmosphere; Stage #2: With sodium triethylborohydride In tetrahydrofuran at 20℃; for 4h; Inert atmosphere; | 83% |
With sodium methylate In tetrahydrofuran Heating; | 76% |
Conditions | Yield |
---|---|
Stage #1: 1,2-Epoxy-4-vinylcyclohexane; octakis(dimethylsiloxy)octasilsesquioxane With bis(1,5-cyclooctadiene)diiridium(I) dichloride; Karstedt's catalyst In toluene at 90℃; Stage #2: Triethoxyvinylsilane In toluene at 90℃; | 88% |
Conditions | Yield |
---|---|
Stage #1: Methyl 10-undecenoate; octakis(dimethylsiloxy)octasilsesquioxane With bis(1,5-cyclooctadiene)diiridium(I) dichloride; Karstedt's catalyst In toluene at 90℃; Stage #2: 1,2-Epoxy-4-vinylcyclohexane In toluene at 90℃; | 87% |
Conditions | Yield |
---|---|
With nickel(II) chloride hexahydrate; potassium tert-butylate In tetrahydrofuran at -30℃; for 1h; Schlenk technique; Inert atmosphere; Sealed tube; | 87% |
Conditions | Yield |
---|---|
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tetramethylammonium formiate; triphenylphosphine In water; N,N-dimethyl-formamide at 80℃; for 4h; Heck Reaction; regioselective reaction; | 86% |
Conditions | Yield |
---|---|
With C21H12Cl6NO4V; tetrabutylammomium bromide In neat (no solvent) at 85℃; under 7500.75 Torr; for 18h; | 82% |
With calcium iodide In neat (no solvent) at 70℃; under 15001.5 Torr; for 24h; diastereoselective reaction; | 77% |
With C68H70Co3N16O8; tetrabutyl-ammonium chloride In neat (no solvent) at 80℃; under 15514.9 Torr; for 4h; Inert atmosphere; Autoclave; |
Conditions | Yield |
---|---|
Stage #1: 3,7-dimethylocta-1,6-dien-3-ol; octakis(dimethylsiloxy)octasilsesquioxane With bis(1,5-cyclooctadiene)diiridium(I) dichloride; Karstedt's catalyst In toluene at 90℃; Stage #2: 1,2-Epoxy-4-vinylcyclohexane In toluene at 90℃; | 82% |
1,2-Epoxy-4-vinylcyclohexane
Conditions | Yield |
---|---|
With oxygen; copper(II) bis(trifluoromethanesulfonate); dimethyl sulfoxide; bismuth at 100℃; for 1.3h; | 77% |
1,2-Epoxy-4-vinylcyclohexane
Dimethylphenylsilane
<2-(3,4-Epoxy-cyclohexyl)-aethyl>-dimethyl-phenyl-silan
Conditions | Yield |
---|---|
With (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; N-ethyl-N,N-diisopropylamine; triisopropylsilanethiol In 1,4-dioxane at 20℃; Schlenk technique; Sealed tube; Inert atmosphere; Irradiation; | 77% |
Stage #1: 1,2-Epoxy-4-vinylcyclohexane; Dimethylphenylsilane With C11H13Cl2CoN5 In toluene at 80℃; for 0.5h; Schlenk technique; Stage #2: With sodium triethylborohydride In toluene at 80℃; for 24h; Schlenk technique; | |
With C77H70N2OPtSi2 In toluene at 80℃; for 8h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; Schlenk technique; regioselective reaction; | 99 %Chromat. |
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