We are manufacturer of this product. If you are looking for the material's manufacturer or supplier in China, Ality Group is your best choice. Specifications of our 3-Bromopropyne CAS 106-96-7: Items Spec
Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Propargyl bromide Boiling point: 80~90℃ Flash point: 10°C Relative Density: 1.335 Refractive Index: 1.4940 Assay: ≥99%
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inquiryTIANFUCHEM--106-96-7--High purity 3-Bromopropyne factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business
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inquiryProduct name 3-Bromopropyne CAS NO 106-96-7 Appearance Light Yellow liquid Purity 99% MF C3H3Br EINECS 203
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. A
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inquiryAppearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryProduct name: Propargyl Bromide CAS No.:106-96-7 Molecule Formula:C3H3Br Molecule Weight:118.96 Purity: 99.0% Package: 200kg/drum Description:Colorless to light yellow liquid Manufacture Standards:Enterprise Standard
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inquiryBest service,high quality and cheap price. Storage:Keep away from heat,sparks and flames. Package:25kg/50kg/200kg drum or Customer demand Application:Used as pharmaceutical intermediates Transportation:BY sea/air or by courier
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Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
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3-BromopropyneAppearance:detailed see specifications Storage:Store in dry, dark and ventilated place Package:according to the clients requirement Application:Organic Building Blocks;Terminal;Electronic Chemicals;Materials Science;Aryl Fluorinated Bui
Conditions | Yield |
---|---|
With carbon tetrabromide; sodium bromide In N,N-dimethyl-formamide for 3h; Catalytic behavior; Irradiation; | 88% |
With tetradecafluorohexane; phosphorus tribromide In diethyl ether at 20℃; for 12h; | 80% |
With phosphorus tribromide 1.) 50 deg C - 60 deg C, 2.) reflux, 1 h; | 59% |
propargyl alcohol
A
bromoallene
B
propargyl bromide
C
1,3-dibromopropene
D
2-bromoallyl bromide
Conditions | Yield |
---|---|
With phosphorus tribromide In toluene at 0 - 50℃; for 3.25h; Product distribution / selectivity; | A 1.38% B 78.81% C 3.17% D 14.78% |
With phosphorus tribromide In isopar C at 6 - 50℃; for 3.71667 - 33.5833h; Product distribution / selectivity; | A 1.22% B 62.1% C 2.88% D 10.14% |
Conditions | Yield |
---|---|
at 400℃; flash vacuum pyrolysis; | A 65% B 15% |
propargyl alcohol
A
propargyl bromide
B
1,3-dibromopropene
C
2-bromoallyl bromide
Conditions | Yield |
---|---|
With phosphorus tribromide In isopar C at 6 - 50℃; for 3.71667h; Product distribution / selectivity; | A 64.37% B 2.54% C 10.26% |
diethoxyphosphoryl-acetic acid ethyl ester
A
ethyl 2-(diethoxyphosphoryl)-2-(2-propynyl)pent-4-ynoate
B
propargyl bromide
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide at 60℃; for 120h; Yields of byproduct given; | A 58% B n/a |
Conditions | Yield |
---|---|
With water; potassium bromide |
3-bromo-2-chloroprop-1-ene
A
bromoallene
B
chloroallene
C
2-propynyl chloride
D
propargyl bromide
Conditions | Yield |
---|---|
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; phenol Yield given; |
Conditions | Yield |
---|---|
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; phenol at 120 - 122℃; Yield given; | |
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; phenol Product distribution; various concentrations of phenol; |
2-bromo-3-chloro-propene
A
bromoallene
B
chloroallene
C
2-propynyl chloride
D
propargyl bromide
Conditions | Yield |
---|---|
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; phenol Yield given; |
2-bromo-3-chloro-propene
A
bromoallene
B
chloroallene
C
propargyl bromide
Conditions | Yield |
---|---|
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; phenol Yield given; |
prop-2-yn-1-ol methanesulfonate
propargyl bromide
Conditions | Yield |
---|---|
With magnesium bromide In diethyl ether at 15℃; for 1h; |
propynyl radical
propargyl bromide
Conditions | Yield |
---|---|
With bromine at 22.9 - 258.9℃; Kinetics; Irradiation; carrier gas, He, the role of resonance stabilization; |
Conditions | Yield |
---|---|
With pyridine; tributyltin bromide at 50℃; Thermodynamic data; Equilibrium constant; Δ G; |
Conditions | Yield |
---|---|
With pyridine; tributyltin bromide at 50℃; Thermodynamic data; Equilibrium constant; Δ G; |
Conditions | Yield |
---|---|
With phosphorus tribromide |
bromocyane
N-methyl-N-propargylaniline
A
methyl(phenyl)cyanamide
B
propargyl bromide
Conditions | Yield |
---|---|
auf dem Wasserbad; |
2-[N-propargyl-N-(2',6'-dibromo-phenyl)-amino]-2-imidazoline
A
propargyl bromide
B
NC 6
2-[N-propargyl-N-(2',6'-dichloro-4'-bromo-phenyl)-amino]-2-imidazoline
A
propargyl bromide
B
St 871
2-[N-propargyl-N-(2'-chloro-3'-methyl-phenyl)-amino]-2-imidazoline
A
propargyl bromide
B
(2-chloro-3-methyl-phenyl)-(4,5-dihydro-1H-imidazol-2-yl)-amine
2-[N-propargyl-N-(2',6'-diethyl-phenyl)-amino]-2-imidazoline
A
propargyl bromide
B
NC 5
2-[N-propargyl-N-(3'-methoxyphenyl)-amino]-2-imidazoline
A
2-[N-(3'-methoxy-phenyl)-amino]-2-imidazoline
B
propargyl bromide
(2-chloro-4-methyl-phenyl)-(4,5-dihydro-1H-imidazol-2-yl)-prop-2-ynyl-amine
A
propargyl bromide
B
Tolonidine
(2-chloro-6-methyl-phenyl)-(4,5-dihydro-1H-imidazol-2-yl)-prop-2-ynyl-amine
A
propargyl bromide
B
(2-chloro-6-methyl-phenyl)-(4,5-dihydro-1H-imidazol-2-yl)-amine
2-[N-propargyl-N-(2',5'-dichloro-phenyl)-amino]-2-imidazoline
A
propargyl bromide
B
(2,5-dichloro-phenyl)-(4,5-dihydro-1H-imidazol-2-yl)-amine
(2,4-dichloro-phenyl)-(4,5-dihydro-1H-imidazol-2-yl)-prop-2-ynyl-amine
A
propargyl bromide
B
NC 8
Conditions | Yield |
---|---|
With zinc In tetrahydrofuran for 0.5h; | 100% |
Stage #1: propargyl bromide With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In diethyl ether; hexane at -78℃; for 0.333333h; Stage #2: benzophenone In diethyl ether at -78 - 20℃; for 2h; Stage #3: With hydrogen cation In diethyl ether | 96% |
Stage #1: benzophenone; propargyl bromide With dysprosium; sodium iodide; mercury dichloride In tetrahydrofuran at -14 - 20℃; Propargylation; Stage #2: With hydrogenchloride In water Hydrolysis; | 92% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; | 100% |
Stage #1: aniline With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Stage #2: propargyl bromide In N,N-dimethyl-formamide at 20℃; | 100% |
With potassium carbonate In acetonitrile at 20℃; Sealed tube; Inert atmosphere; | 99% |
propargyl bromide
diethyl malonate
diethyl 2,2-di(prop-2-yn-1-yl)malonate
Conditions | Yield |
---|---|
Stage #1: diethyl malonate With sodium hydride In tetrahydrofuran; mineral oil for 2h; Inert atmosphere; Cooling with ice; Stage #2: propargyl bromide In tetrahydrofuran; mineral oil at 0℃; Inert atmosphere; | 100% |
With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide In water at 20℃; for 15h; | 94% |
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride for 16h; | 90% |
propargyl bromide
2-acetylaminomalonic acid diethyl ester
diethyl α-acetamido-α-propargylmalonate
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile at 20℃; for 18h; | 100% |
With caesium carbonate In acetonitrile at 20℃; for 18h; | 99% |
With sodium hydride In N,N-dimethyl-formamide at 60℃; for 3h; | 95% |
Conditions | Yield |
---|---|
With sodium hydroxide; tetrabutyl ammonium fluoride In benzene a) 0 deg C, 30 min, b) r.t., 2h; | 100% |
With triethylamine In diethyl ether at 20℃; for 2h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2h; | 96% |
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran | 100% |
With potassium carbonate In acetone Reflux; | 100% |
Stage #1: ortho-cresol With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 0.5h; Inert atmosphere; Stage #2: propargyl bromide In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide; toluene at 20℃; for 60h; | 100% |
With potassium carbonate In acetone Reflux; | 100% |
With potassium carbonate In N,N-dimethyl-formamide; toluene at 20℃; for 12h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone Reflux; | 100% |
Stage #1: p-cresol With potassium carbonate In N,N-dimethyl-formamide for 0.166667h; Schlenk technique; Inert atmosphere; Stage #2: propargyl bromide In N,N-dimethyl-formamide at 20℃; for 24h; Schlenk technique; Inert atmosphere; | 99% |
With caesium carbonate In acetonitrile | 93% |
Conditions | Yield |
---|---|
With sodium hydroxide In methanol at 0 - 20℃; for 1h; | 100% |
(i) Na, liq. NH3, (ii) /BRN= 605309/; Multistep reaction; | |
With sodium ethanolate In ethanol |
(2-furyl)methyl alcohol
propargyl bromide
2-((prop-2-yn-1-yloxy)methyl)furan
Conditions | Yield |
---|---|
Stage #1: (2-furyl)methyl alcohol With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1.5h; Stage #2: propargyl bromide In N,N-dimethyl-formamide at 20℃; Reagent/catalyst; | 100% |
With para-chlorotoluene; lithium In tetrahydrofuran at -35 - 20℃; for 10h; Heating / reflux; | 93% |
Stage #1: (2-furyl)methyl alcohol With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.166667h; Stage #2: propargyl bromide In N,N-dimethyl-formamide; toluene at 23℃; for 4h; | 86% |
1H-indol-2-ylcarboxaldehyde
propargyl bromide
1-(prop-2-yn-1-yl)-1H-indole-2-carbaldehyde
Conditions | Yield |
---|---|
Stage #1: 1H-indol-2-ylcarboxaldehyde With sodium hydride In N,N-dimethyl-formamide Inert atmosphere; Schlenk technique; Cooling with ice; Stage #2: propargyl bromide In N,N-dimethyl-formamide at 20℃; Inert atmosphere; Schlenk technique; Cooling with ice; | 100% |
Stage #1: 1H-indol-2-ylcarboxaldehyde With sodium hydride In N,N-dimethyl-d6-formamide Stage #2: propargyl bromide In N,N-dimethyl-formamide; toluene for 6.5h; | 97% |
With sodium hydride In N,N-dimethyl-formamide | 75% |
(+/-)-5-phenyl-2-pyrrolidinone
propargyl bromide
N-propargyl-5-phenyl-2-pyrrolidone
Conditions | Yield |
---|---|
With potassium hydroxide; tetrabutylammomium bromide In tetrahydrofuran at 0 - 20℃; for 6h; | 100% |
7-hydroxy-4-methyl-chromen-2-one
propargyl bromide
7-propargyloxy-4-methyl-2H-chromen-2-one
Conditions | Yield |
---|---|
With potassium carbonate In toluene; acetonitrile at 60℃; Inert atmosphere; | 100% |
With potassium carbonate In acetone for 4h; Heating; | 97% |
With potassium carbonate In toluene; acetonitrile at 60℃; for 12h; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
Stage #1: indole-2,3-dione With potassium carbonate In N,N-dimethyl-formamide for 0.333333h; Cooling with ice; Stage #2: propargyl bromide In N,N-dimethyl-formamide at 20℃; for 3h; | 100% |
With KF-Celite In 2-methyltetrahydrofuran for 3h; Reflux; chemoselective reaction; | 95% |
With potassium carbonate In N,N-dimethyl-formamide | 95% |
tetramethylene glutarimide
propargyl bromide
8-Propargyl-8-azaspiro<4.5>decane-7,9-dione
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 10h; Heating; | 100% |
With potassium carbonate In acetone Heating; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 4h; Reflux; | 100% |
With potassium carbonate In acetone Reflux; | 100% |
With potassium carbonate for 6h; Reflux; | 100% |
Conditions | Yield |
---|---|
With aluminum oxide In diethyl ether at 20℃; for 96h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 5h; | 85% |
With potassium carbonate In N,N-dimethyl-formamide; toluene at 20℃; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran | 100% |
With potassium carbonate In N,N-dimethyl-formamide; toluene at 25℃; for 16h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 98% |
With potassium carbonate In acetonitrile for 6h; Reflux; | 97% |
methyl 4-hydroxylbenzoate
propargyl bromide
methyl 4-(2-propynoxy)benzoate
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium carbonate In acetone; toluene for 72h; Reflux; | 100% |
With potassium carbonate In acetone Inert atmosphere; | 99% |
With potassium carbonate In acetone at 65℃; for 18h; Inert atmosphere; | 98% |
isovanillin
propargyl bromide
4-methoxy-3-(prop-2-yn-1-yloxy)benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 3h; | 100% |
With potassium carbonate In acetone Reflux; | 97% |
With potassium carbonate In N,N-dimethyl-formamide for 4h; Ambient temperature; | 95% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone; toluene for 24h; Williamson Ether Synthesis; Reflux; | 100% |
Stage #1: 4-nitro-phenol With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere; Stage #2: propargyl bromide In N,N-dimethyl-formamide at 20℃; for 10h; Inert atmosphere; | 100% |
Stage #1: 4-nitro-phenol With potassium carbonate In acetonitrile at 20℃; for 0.166667h; Stage #2: propargyl bromide In acetonitrile Reflux; | 100% |
ethyl 1,4-dioxaspiro[4.5]decane-8-carboxylate
propargyl bromide
8-Ethoxycarbonyl-8-(prop-2-ynyl)-1,4-dioxaspiro[4.5]decane
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran 1.) -78 to 0 deg C, 2.) -78 deg C, 15 min; | 100% |
With lithium diisopropyl amide In tetrahydrofuran Yield given; | |
Stage #1: ethyl 1,4-dioxaspiro[4.5]decane-8-carboxylate With lithium diisopropyl amide In tetrahydrofuran at -70℃; for 1h; Inert atmosphere; Stage #2: propargyl bromide In tetrahydrofuran at -70 - 20℃; for 12h; Inert atmosphere; |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide; toluene at 60℃; for 2h; Inert atmosphere; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 60℃; Inert atmosphere; | 100% |
With potassium carbonate In acetone | 99% |
2-hydroxybromobenzene
propargyl bromide
1-bromo-2-(prop-2-yn-1-yloxy)benzene
Conditions | Yield |
---|---|
With potassium carbonate In toluene; acetonitrile at 60℃; for 16h; | 100% |
With potassium carbonate In N-methyl-acetamide; hexane; water; ethyl acetate | 99% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 14h; | 98% |
ethyl N-diphenylmethylene glycine
propargyl bromide
ethyl 2-[(diphenylmethylidene)amino]pent-4-ynoate
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 20h; Heating; | 100% |
With potassium carbonate In acetonitrile Alkylation; Heating; | 86% |
With potassium carbonate In acetonitrile Alkylation; | 86% |
(E)-3-trimethylsilyl-2-propenal
propargyl bromide
(E)-6-trimethylsilyl-hex-5-en-1-yn-4-ol
Conditions | Yield |
---|---|
With zinc; titanium tetrachloride In tetrahydrofuran for 0.5h; Ambient temperature; | 100% |
With zinc; titanium tetrachloride In tetrahydrofuran | |
With titanium tetrachloride; zinc In tetrahydrofuran at 0℃; Yield given; |
3-α-Naphthylpropargylpyrrolidine
propargyl bromide
1-(3-Naphthalen-1-yl-prop-2-ynyl)-1-prop-2-ynyl-pyrrolidinium; bromide
Conditions | Yield |
---|---|
In diethyl ether | 100% |
[3-(α-naphthyl)-2-propynyl]dipropylamine
propargyl bromide
Dipropylpropargyl<3-(α-naphthyl)propargyl>ammonium bromide
Conditions | Yield |
---|---|
In diethyl ether | 100% |
1-(3-(naphthalen-1-yl)prop-2-ynyl)piperidine
propargyl bromide
1-(3-Naphthalen-1-yl-prop-2-ynyl)-1-prop-2-ynyl-piperidinium; bromide
Conditions | Yield |
---|---|
In diethyl ether | 100% |
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