Henan Allgreen Chemical Co.,Ltd
The company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dry, m
Cas:111-66-0
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryAlity Chemical Corporation
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Dayang Chem (Hangzhou) Co.,Ltd.
DayangChem exported this product to many countries and regions at best price in China. If you are looking for the product’s supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product specifica
Chemwill Asia Co., Ltd.
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Henan Tianfu Chemical Co., Ltd.
Product Name: 1-OCTENE Synonyms: 1-OCTENE, 98%1-OCTENE, 98%1-OCTENE, 98%1-OCTENE, 98%;1-Octene [Standard Material for GC];Oct-1-ene Caprylene;1-Octene, 99+% 2.5LT;Dialen 8;Gulftene 8;Linealene 8;NSC 8457 CAS: 111-66-0 MF: C8H16 MW: 112.21 EINE
Cas:111-66-0
Min.Order:1 Kilogram
FOB Price: $240.0
Type:Lab/Research institutions
inquiryHebei yanxi chemical co.,LTD.
Hebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
Changchun Artel lmport and Export trade company
Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Hangzhou Keyingchem Co.,Ltd
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
SHANGHAI T&W PHARMACEUTICAL CO., LTD.
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Hangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:111-66-0
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHANGZHOU YUNUO CHEMICAL CO.,LTD
Superior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat
Zibo Dorne chemical technology co. LTD
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Kono Chem Co.,Ltd
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Wuhan Fortuna Chemical Co.,Ltd
Best service,high quality and cheap price. Storage:Keep away from heat,sparks and flames. Package:25kg/50kg/200kg drum or Customer demand Application:Used as pharmaceutical intermediates Transportation:BY sea/air or by courier
Zhuozhou Wenxi import and Export Co., Ltd
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:111-66-0
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAntimex Chemical Limied
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Xiamen AmoyChem Co.,Ltd
Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
Hunan Longxianng Runhui Trading Co.,Ltd
1-OCTENE,111-66-0Appearance:white powder Storage:Room temperature. Package:normal packing Application:Pharmaceutical Intermediates, OLED Intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport t
Chemsigma International Co.,Ltd.
bulk?production Application:Pharmaceutical intermediates
HWRK Chem
in storeAppearance:Colorless, flammable liquid Package:1L Application:Organic Chemicals
HENAN SUNLAKE ENTERPRISE CORPORATION
Henan Sunlake Enterprise Corporation Our Advantages 1, Any inquiry about ch
Zhengzhou Kingorgchem Chemical Technology Co., Ltd.
1. Subsidiary of Institute of Chemistry, Henan Academy of Sciences, national research platform;2. About 30 years’ experience in this field since 1983;3. An experienced R&D team consisting of Doctors and Masters;4. Various types of analytical instrume
Cas:111-66-0
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHebei Ruishun Trade Co.,Ltd
Profile HeBei Ruishun Trade Co.LTD, registered capital one million,have a production of pharmaceutical raw materials, pharmaceutical raw materials factory reagent r&d center,Seek development by credit
Xiamen BaiFuchem Co.,Ltd
BaiFuChem is a Professional chemical raw material supplier in China, our main products include Biochemical , Pharma Intermediate and Organic chemical etc. BaiFuChem have wealth of products,experience , expertise and state-of-the-art
Nanjing Chemlin Chemical Co., Ltd.
Compound sourcing ServicesAgency of testing serviceFactory audit serviceFounded in Dec. 1999, Nanjing Chemlin Chemical Industrial Co.,Ltd(CHEMLIN) has been covering the business scope from trading of chemicals to custom-synthesis & Manufacturing. Co
SuZhou LaiTeou
[Chinese] 1 - octene "English name" 1 - OCTENE 1 - OCTYLENE CAPRYLENE OCT 1 - ENE 1-0 ctene 1 - C8H16 1 - caprylene Alpha - Octene Alpha - Octylene N - 1 - Octene Neodene 8 Octen OCTENE-1 Octylene Caprylene~
Yinghao Pharm Co.,Ltd.
Yinghao Pharm products include: leader molecule, heterocyclic compounds,chiral compounds, photoelectric materials, biochemical reagents etc. For example:benzene, pyrimidine, boricacid,pyridine, pyrazole, imidazole, pyrrole, fluorine and other derivat
Synthetic route
| Conditions | Yield |
|---|---|
| With zirconocene dichloride; tert-butylmagnesium chloride; water Product distribution; multistep reaction; other hydrozirconation agents; other substrates; | 100% |
| With hydrogen In ethanol at 20℃; under 760.051 Torr; for 2.5h; | 95% |
| With 2,6-bis[1-(2,6-diisopropylphenylimino)ethyl]pyridine cobalt(II) dichloride; diethoxymethylane; sodium triethylborohydride In neat (no solvent) at -78 - 40℃; for 1h; | 95% |
-
-
191331-78-9
(S)-2-octyl chloroformate
-
A
-
13389-42-9
trans-2-Octene
-
B
-
111-66-0
oct-1-ene
-
C
-
18651-57-5
(R)-2-chlorooctane
| Conditions | Yield |
|---|---|
| With hexabutylguanidinium chloride In neat (no solvent) for 10h; | A n/a B n/a C 100% |
| Conditions | Yield |
|---|---|
| With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate at 0℃; for 3h; | 97% |
| With aluminum oxide at 350℃; | |
| With fired clay fragments at 450 - 500℃; |
| Conditions | Yield |
|---|---|
| With potassium hydroxide; triisopropylsilanol In N,N-dimethyl-formamide Ambient temperature; | 97% |
| With 3-(tert-Butylamino)-1,1,1,5,5,5-hexakis(dimethylamino)-3-<amino>-1λ5,3λ5,5λ5-1,4-triphosphazadiene In tetrahydrofuran; xylene for 6h; Ambient temperature; | 96% |
| With lithium diisopropylamide at 0℃; Kinetics; | 87% |
| Conditions | Yield |
|---|---|
| With hydrogen In hexane at 40℃; under 760.051 Torr; for 6h; | A 3% B 97% |
| With triisobutylaluminum; zirconocene dichloride In benzene for 0.333333h; | A 44% B 51% |
| With hydrogen In cyclohexane at 150℃; under 75007.5 Torr; for 48h; Autoclave; Glovebox; | A 43% B 47% |
| Conditions | Yield |
|---|---|
| With hexabutylguanidinium chloride at 100℃; for 5h; Yields of byproduct given; | A n/a B n/a C 97% |
| Conditions | Yield |
|---|---|
| With nickel(II) iodide; 1,1,3,3-Tetramethyldisiloxane; copper(II) bis(trifluoromethanesulfonate); triphenylphosphine In neat (no solvent) at 190℃; for 16h; Reagent/catalyst; Sealed tube; Schlenk technique; Inert atmosphere; | 94% |
| With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)nickel (0); 2,2-dimethylpropanoic anhydride; potassium iodide at 180 - 190℃; for 2h; Inert atmosphere; Glovebox; | 78% |
| With sodium persulfate; sulfuric acid; silver nitrate; copper(II) sulfate 1.) water, reflux, 2.) 5 min, reflux; Yield given. Multistep reaction; |
| Conditions | Yield |
|---|---|
| cobalt(II) naphthenate In nonane Product distribution / selectivity; | 93.1% |
| Conditions | Yield |
|---|---|
| With potassium hydroxide; Aliquat 336 at 20℃; for 20h; | A 92% B 7% |
-
-
111-83-1
1-bromo-octane
-
-
917-58-8
potassium ethoxide
-
A
-
929-61-3
ethyl octyl ether
-
B
-
111-66-0
oct-1-ene
| Conditions | Yield |
|---|---|
| With Aliquat 336 at 20℃; for 20h; | A 92% B 5% |
-
-
84363-56-4
2-(phenylsulfonyl)-1-(trimethylsilyl)octane
-
-
111-66-0
oct-1-ene
| Conditions | Yield |
|---|---|
| With tetrabutyl ammonium fluoride In tetrahydrofuran for 0.666667h; Heating; | 92% |
| Conditions | Yield |
|---|---|
| With trifluoroacetic anhydride | 91% |
| Conditions | Yield |
|---|---|
| With CrCl2(tetrahydrofuran)2; N,N'-bis(diphenylphosphino)-N,N'-dimethylpropane-1,3-diamine In methyl cyclohexane at 80℃; under 30003 Torr; for 0.5h; Inert atmosphere; | A 9% B 91% |
| bis(2-(decylthio)ethyl)amine; chromium chloride In toluene at 90℃; under 33753.4 Torr; for 0.502778 - 0.527778h; Product distribution / selectivity; | A 90.85% B 0.5% |
| chromium(III)2-ethylhexanoate; trimethylaluminum; N-[bis(2-methoxyphenyl)phosphino]-P,P-bis(2-methoxyphenyl)-N-methylphosphinous amide In methyl cyclohexane; toluene at 60℃; under 36003.6 - 37503.8 Torr; for 0.175h; Product distribution / selectivity; | A 89.7% B 8.5% |
| Conditions | Yield |
|---|---|
| With formic acid at 20 - 240℃; Inert atmosphere; | 91% |
| With methyltrioxorhenium(VII); sodium sulfite at 150℃; for 20h; sealed tube; | 60 %Chromat. |
| With 15-crown-5; tetrabutylammonium perrhenate; sodium sulfite In benzene at 150 - 160℃; for 100h; regiospecific reaction; | 68 %Chromat. |
| Conditions | Yield |
|---|---|
| at 375℃; under 760.051 Torr; for 0.7h; Reagent/catalyst; | A 5.9% B 90.1% |
| With copper(II) sulfate In neat (no solvent) at 180℃; under 660 Torr; for 5h; Yield given; |
| Conditions | Yield |
|---|---|
| With lithium diisopropylamide In tetrahydrofuran; hexane at -78℃; | 89% |
| Multi-step reaction with 2 steps 1: 1.) sodium hydride / 1.) DMF, 20 deg C, 1 h, 2.) 80 deg C, 18 h 2: 1.) NaH / 1.) DMF, 1 h, 2.) 70 deg C, 6 h View Scheme | |
| Multi-step reaction with 2 steps 1: sodium hydride, trifluoroacetamide / dimethylformamide / 18 h / 80 °C 2: 1.) NaH / 1.) DMF, 1 h, 2.) 70 deg C, 6 h View Scheme | |
| Multi-step reaction with 2 steps 1: potassium iodide / methanol / Irradiation 2: methanol / Irradiation View Scheme |
| Conditions | Yield |
|---|---|
| In diethyl ether for 15h; from 0 degC to 20 degC; | 88% |
| Conditions | Yield |
|---|---|
| With tetrabutylammomium bromide; cesium fluoride for 1h; Heating; | A 88% B 9.4 % Chromat. |
| With C12H35N7P2*FH In tetramethylurea; 1,3,5-trimethyl-benzene at 120℃; for 0.416667h; Inert atmosphere; | A 72% B 14% |
| With 1,1,1-trifluoro-2-(2,2,2-trifluoroethoxy)ethane; 2,2-Dimethylpropyltrimethylammonium fluoride at 25℃; | A 71% B 29% |
| Conditions | Yield |
|---|---|
| With lithium diisopropylamide In tetrahydrofuran; hexane at -78℃; | 88% |
| With sodium hydride In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 14h; | 87% |
| With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride at 0 - 20℃; Inert atmosphere; | 87% |
| Conditions | Yield |
|---|---|
| With sodium hydride In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 13h; | 88% |
| With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride at 0 - 20℃; Inert atmosphere; | 88% |
| Conditions | Yield |
|---|---|
| aluminum oxide; tetramethylstannane; rhenium(VII) oxide In chlorobenzene at 25℃; for 3h; Yields of byproduct given; | A n/a B 87.8% |
| Conditions | Yield |
|---|---|
| With Aliquat 336 at 20℃; for 20h; | A 87% B 13% |
-
-
111-83-1
1-bromo-octane
-
-
141-52-6
sodium ethanolate
-
A
-
929-61-3
ethyl octyl ether
-
B
-
111-66-0
oct-1-ene
| Conditions | Yield |
|---|---|
| With potassium hydroxide; Aliquat 336 at 20℃; for 20h; | A 86% B 10% |
-
-
107465-90-7
di-2-octyl phenylphosphonate
-
A
-
111-67-1
2-octene
-
B
-
111-66-0
oct-1-ene
-
C
-
1571-33-1
phenylphosphonate
| Conditions | Yield |
|---|---|
| With Amberlite 200C In dichloromethane at 40℃; for 72h; Product distribution; | A n/a B n/a C 85% |
-
-
28540-81-0
(E) 2-iodo-1-chloroethylene
-
-
629-05-0
n-octyne
-
A
-
111-66-0
oct-1-ene
-
B
-
96251-47-7
(1E,3E)-1-chloro-1,3-decadiene
| Conditions | Yield |
|---|---|
| Stage #1: n-octyne With diisobutylaluminium hydride In n-heptane at 50℃; for 4h; Stage #2: With indium(III) chloride In tetrahydrofuran; n-heptane at 0℃; for 0.5h; Stage #3: (E) 2-iodo-1-chloroethylene With trifuran-2-yl-phosphane; Cl2Pd[bis(2-diphenylphosphinophenyl)ether]; diisobutylaluminium hydride In tetrahydrofuran; hexane; n-heptane at 0℃; for 4h; | A 4 % Spectr. B 85% |
| Conditions | Yield |
|---|---|
| With tetra(n-butyl)ammonium hydrogensulfate; triphenyltinfluoride In acetonitrile at 85℃; for 10h; | A 83% B 12% |
| Conditions | Yield |
|---|---|
| With 2C24BF20(1-)*C21H16N3P(2+) In dichloromethane at 55℃; for 24h; Reagent/catalyst; Inert atmosphere; | 83% |
-
-
51003-20-4
(R)-2-octanol trimethylsilyl ether
-
A
-
7642-04-8
cis-2-octene
-
B
-
13389-42-9
trans-2-Octene
-
C
-
111-66-0
oct-1-ene
| Conditions | Yield |
|---|---|
| With diethylamino-sulfur trifluoride In dichloromethane at -78 - -20℃; for 10h; | A n/a B n/a C n/a D 82% |
-
-
56798-08-4
(E)-1-bromo-2-iodoethylene
-
-
629-05-0
n-octyne
-
A
-
111-66-0
oct-1-ene
-
B
-
71686-99-2
(7E,9E)-hexadeca-7,9-diene
-
C
-
174365-91-4
(1E,3E)-1-bromo-1,3-decadiene
| Conditions | Yield |
|---|---|
| Stage #1: n-octyne With diisobutylaluminium hydride In n-heptane at 50℃; for 4h; Stage #2: With indium(III) chloride In tetrahydrofuran; n-heptane at 0℃; for 0.5h; Stage #3: (E)-1-bromo-2-iodoethylene With trifuran-2-yl-phosphane; Cl2Pd[bis(2-diphenylphosphinophenyl)ether]; diisobutylaluminium hydride In tetrahydrofuran; hexane; n-heptane at 0℃; for 4h; | A 7% B 2% C 82% |
| Conditions | Yield |
|---|---|
| at 80-100 °C;; | 100% |
| at 80-100 °C;; | 100% |
| In neat (no solvent) other Radiation; under Ar; (60)Co-irradiation; 1.5:1 molar ratio (olefine:Sn-compound) ;25°C; GLC; | 74% |
| Conditions | Yield |
|---|---|
| With hydrogen; In dichloromethane at 65℃; for 15h; same yield with a similar catalyst; Pressure (range begins): 120 ; | 100% |
| With {(η6-C6H6)Ru(NCCH3)3}{BF4}2; water; hydrogen In benzene at 90℃; under 30400 Torr; for 4h; | 100% |
| With hydrogen; In dichloromethane at 65℃; for 15h; Product distribution; other catalyst, other substrates; Pressure (range begins): 120 ; | 100% |
| Conditions | Yield |
|---|---|
| With poly{[CuBa(pyridine-2,5-dicarboxylate)2(H2O)5]*H2O}; dihydrogen peroxide In acetonitrile at 60℃; for 6h; Catalytic behavior; Reagent/catalyst; | 100% |
| With dmap; osmium(VIII) oxide; 4-methylmorpholine N-oxide; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate In water; tert-butyl alcohol at 20℃; for 16h; | 99% |
| With 4-methylmorpholine N-oxide; dendritic osmium catalyst In hexane; acetonitrile; tert-butyl alcohol at 20℃; for 36h; | 98% |
-
-
111-66-0
oct-1-ene
-
-
21948-46-9, 72778-28-0
1,2-dichlorooctane
| Conditions | Yield |
|---|---|
| With tetraethylammonium trichloride In dichloromethane | 100% |
| With chlorine In chloroform at 20℃; for 1.5h; | 97% |
| With oxone||potassium monopersulfate triple salt; potassium chloride; N-(n-butyl)-2-methylbenzamide In dichloromethane; water at 20℃; for 0.25h; | 91% |
| Conditions | Yield |
|---|---|
| With 3-chloro-benzenecarboperoxoic acid; iron(III) perchlorate In acetonitrile at -10℃; for 0.0833333h; | 100% |
| With 3-chloro-benzenecarboperoxoic acid; (Cl8TPP)FeIII(ClO4) In acetonitrile at -10℃; for 0.0833333h; Product distribution; invetigation of the iron(III) perchlorate-catalyzed epoxidation of olefins and oxidative cleavage of diols by m-chloroperbenzoic acid and pentafluoroiodobenzene; | 100% |
| With oxygen; isobutyraldehyde In acetonitrile at 60℃; for 18h; | 99% |
| Conditions | Yield |
|---|---|
| at 90℃; for 5h; Inert atmosphere; | 100% |
| at 90℃; for 5h; Inert atmosphere; | 100% |
| With graphene nanoplates-supported platinum nanoparticles In neat (no solvent) at 80℃; for 2h; Catalytic behavior; | 99% |
| Conditions | Yield |
|---|---|
| With triethyl borane; oxygen In cyclohexane at 20℃; | 100% |
| at 30℃; for 17h; (γ-irradiation); |
| Conditions | Yield |
|---|---|
| With 2-pyridylpropylimine rhodium(I)chlorocarbonyl; hydrogen In toluene at 95℃; Catalytic behavior; Reagent/catalyst; Pressure; Temperature; Autoclave; chemoselective reaction; | 100% |
| With hydrogen In dichloromethane at 45℃; under 51716.2 Torr; for 16h; Autoclave; Inert atmosphere; Green chemistry; regioselective reaction; | 100% |
| With hydrogen In cyclohexane at 120℃; under 37503.8 Torr; for 4h; Autoclave; | 99% |
-
-
111-66-0
oct-1-ene
-
-
75067-06-0
thexylchloroborane * dimethylsulfide
-
A
-
111-87-5
octanol
-
B
-
4128-31-8
rac-octan-2-ol
-
C
-
594-60-5
2,3-dimethylbutan-2-ol
| Conditions | Yield |
|---|---|
| With methanol; dihydrogen peroxide Product distribution; different solvents; other olefins; | A 99.2% B 0.8% C 100% |
| Conditions | Yield |
|---|---|
| With dihydrogen peroxide; 6-molybdo-6-tungstophosphoric acid/Al/C In tert-butyl alcohol at 60℃; for 4h; | 100% |
| With [Me(n-Oct)3N]3{PO4[WO(O2)2]4}; dihydrogen peroxide In water; 1,2-dichloro-ethane at 95℃; for 5h; Catalytic behavior; Reagent/catalyst; Temperature; Concentration; Reflux; Green chemistry; | 97% |
| With jones reagent; osmium(VIII) oxide In water; acetone for 20h; Ambient temperature; | 85% |
| Conditions | Yield |
|---|---|
| With zinc In diethyl ether at 15 - 20℃; for 1.5h; sonication; | 100% |
| With zinc/copper couple; trichlorophosphate In diethyl ether Reflux; | |
| With zinc-copper couple; trichlorophosphate In diethyl ether Reflux; Inert atmosphere; | |
| With zinc/copper couple; trichlorophosphate In diethyl ether at 0℃; Inert atmosphere; Reflux; |
-
-
111-66-0
oct-1-ene
-
-
1873-88-7
1,1,1,3,5,5,5-heptamethyltrisiloxan
-
-
17955-88-3
3-n-octyl-1,1,1,3,5,5,5-heptamethyltrisiloxane
| Conditions | Yield |
|---|---|
| With tetradecyl(tributyl)phosphonium bis(trifluoromethylsulfonyl)amide; C24H20Cl2P2Pt at 100℃; for 1h; Reagent/catalyst; | 100% |
| With tetradecyl(tributyl)phosphonium bis(trifluoromethylsulfonyl)amide; bis(cyclooctadiene (μ-silyloxytrimethyl) rhodium(I)) at 110℃; for 1h; Catalytic behavior; Reagent/catalyst; Time; | 100% |
| With nickel 2-ethylhexanoate; 1,4-bis(2,6-diisopropylphenyl)-2,3-dimethyl-1,4-diazabuta-1,3-diene In neat (no solvent) at 23℃; for 6h; regioselective reaction; | 99% |
-
-
111-66-0
oct-1-ene
-
-
25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
-
-
66217-56-9
4,4,5,5-tetramethyl-2-octyl-[1,3,2]dioxaborolane
| Conditions | Yield |
|---|---|
| With sodium triethylborohydride at 23℃; for 3h; Catalytic behavior; Reagent/catalyst; Inert atmosphere; | 100% |
| Wilkinson's catalyst In dichloromethane 25°C, 10 min; | 99% |
| With chlorocarbonylbis(triphenylphosphine)rhodium(I) In dichloromethane at 0 - 20℃; for 1.83333h; Inert atmosphere; | 99% |
| Conditions | Yield |
|---|---|
| With hypophosphorous acid; palladium; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In water; N,N-dimethyl-formamide at 110℃; for 24h; | 100% |
| With tris-(dibenzylideneacetone)dipalladium(0); hypophosphorous acid; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; oxygen In N,N-dimethyl-formamide at 110℃; for 20h; | |
| Multi-step reaction with 2 steps 1: tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tetrahydrofuran / 9 h / 70 °C 2: sodium hydroxide; potassium permanganate / water / 5 h / 15 °C / Cooling with ice View Scheme |
| Conditions | Yield |
|---|---|
| With diisobutylaluminium hydride 75-80°C;; | 100% |
| With (iso-C4H9)2AlH 75-80°C;; | 100% |
| With diisobutylaluminium hydride 75-80°C;; | 100% |
| Conditions | Yield |
|---|---|
| In dichloromethane at 20℃; for 4h; Inert atmosphere; | 100% |
-
-
111-66-0
oct-1-ene
-
-
2984-50-1, 50418-68-3, 77495-66-0, 77549-73-6
(2S)-2-hexyloxirane
| Conditions | Yield |
|---|---|
| With titanium(IV) isopropylate; Pentafluorobenzoic acid; C32H22F10N2O2; dihydrogen peroxide In water; 1,2-dichloro-ethane at 20℃; for 45h; Inert atmosphere; enantioselective reaction; | 100% |
| With titanium(IV) isopropylate; C46H40N2O2; dihydrogen peroxide In dichloromethane; water; 1,2-dichloro-ethane at 20℃; for 100h; Reagent/catalyst; Inert atmosphere; | 82% |
| With oxygen; isobutyraldehyde In acetonitrile at 25℃; for 8h; Catalytic behavior; Green chemistry; enantioselective reaction; | 70 %Chromat. |
| Conditions | Yield |
|---|---|
| In Petroleum ether at -10 - 0℃; for 1h; Inert atmosphere; | 100% |
| at 0 - 20℃; for 3h; Inert atmosphere; Further stages; | |
| In tetrahydrofuran at 20℃; for 1h; Cooling with ice; | |
| In diethyl ether Inert atmosphere; Reflux; |
| Conditions | Yield |
|---|---|
| With MesPDI; cobalt(II) stearate In tetrahydrofuran at 60℃; for 5h; Reagent/catalyst; | 100% |
| With C22H31Cl2CoN2P In neat (no solvent) at 60℃; for 24h; Reagent/catalyst; Temperature; Sealed tube; Inert atmosphere; regioselective reaction; | 92% |
| With 2,6-bis[1-(2,4,6-trimethylimino)ethyl]pyridine; C10H14CoO5 In toluene at 60℃; for 24h; Reagent/catalyst; Temperature; regioselective reaction; | 91% |
| With 2,6-bis[1-(2,4,6-trimethylimino)ethyl]pyridine; cobalt(II) tetrafluoroborate hexahydrate In tetrahydrofuran at 20℃; for 4h; Catalytic behavior; Reagent/catalyst; regioselective reaction; | 72 %Spectr. |
| Conditions | Yield |
|---|---|
| at 110℃; Inert atmosphere; Schlenk technique; | 100% |
-
-
111-66-0
oct-1-ene
| Conditions | Yield |
|---|---|
| With selenium dibromide In tetrachloromethane at -20 - 20℃; for 18h; regioselective reaction; | 100% |
| With selenium dibromide In chloroform at 20 - 25℃; for 18h; regioselective reaction; | 95% |
| Stage #1: oct-1-ene With selenium(IV) oxide; hydrogen bromide In diethyl ether; water at 0 - 25℃; for 0.5h; Stage #2: With sodium metabisulfite In benzene at 5 - 25℃; for 2h; | 84% |
-
-
111-66-0
oct-1-ene
| Conditions | Yield |
|---|---|
| With tellurium tetrachloride In chloroform at 20 - 25℃; for 20h; regioselective reaction; | 100% |
| Conditions | Yield |
|---|---|
| With tellurium tetrachloride In chloroform at 20 - 25℃; for 20h; regioselective reaction; | 100% |
| Conditions | Yield |
|---|---|
| With tellurium(IV) tetrabromide at 55 - 60℃; for 6h; regioselective reaction; | 100% |
-
-
111-66-0
oct-1-ene
| Conditions | Yield |
|---|---|
| With selenium(II) chloride In chloroform at -60 - 20℃; for 18h; regioselective reaction; | 100% |
| Stage #1: oct-1-ene With hydrogenchloride; selenium(IV) oxide In diethyl ether; water at 0 - 25℃; for 7h; Stage #2: With sodium metabisulfite In benzene at 5 - 25℃; for 2h; | 80% |
| Conditions | Yield |
|---|---|
| Stage #1: oct-1-ene With tellurium tetrachloride In chloroform at 0 - 20℃; for 14h; Stage #2: ethanol In chloroform for 5h; Reflux; | 100% |
| Conditions | Yield |
|---|---|
| for 2h; UV-irradiation; cooling; | 99.6% |
| Conditions | Yield |
|---|---|
| With Wilkinson's catalyst at 80℃; for 6h; Reagent/catalyst; | 99.3% |
| With graphite oxide-supported Karstedt catalyst at 60℃; for 1h; | |
| With rhodium(III) chloride trihydrate; diphenyl(3-triethylsilylphenyl)phosphine at 90℃; for 5h; Inert atmosphere; Schlenk technique; |
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