Product Name: triethyliodosilane Synonyms: triethyliodosilane CAS: 1112-49-8 398- Appearance:white powder Storage:room tempurature Package:as required Application:Organic Chemicals Transportation:by sea or air Port:Sha
Cas:1112-49-8
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high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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High purity Application:Pharmaceutical intermediates, Material synthesis and analyzing the expectant ingredients
triethylsilyl phenylselenide
A
triethylsilyl iodide
B
diphenyl diselenide
Conditions | Yield |
---|---|
With iodine | A 89% B 96% |
Conditions | Yield |
---|---|
With butyryl iodide; bis(acetylacetonate)nickel(II) at 20℃; for 2h; | A 90% B 81% |
Conditions | Yield |
---|---|
With triethylsilane; bis(acetylacetonate)nickel(II) at 20℃; for 2h; | A 90% B 81% |
Conditions | Yield |
---|---|
With I2 In tetrachloromethane | 86% |
With I2 In tetrachloromethane | 86% |
Conditions | Yield |
---|---|
With methyl iodide; palladium dichloride at 20℃; for 1.5h; | 85% |
With I2 | 85% |
With acetyl iodide In toluene at 100℃; for 6h; | 58% |
triethylsilane
nitromethane
trimethylsilyl iodide
A
triethylsilyl iodide
B
Hexamethyldisiloxane
C
1,1,1-triethyl-3,3,3-trimethyl-disiloxane
D
hexaethyl disiloxane
E
methylamine hydroiodide
Conditions | Yield |
---|---|
Product distribution; Mechanism; 2 h at -5 deg C, then 5 h at 30 deg C; | A n/a B n/a C n/a D n/a E 80% |
Conditions | Yield |
---|---|
80% |
Conditions | Yield |
---|---|
With I2; Al | 75% |
With I2; AlI3 | 59% |
With aluminium(III) iodide | |
With iodine; aluminium |
Conditions | Yield |
---|---|
With lithium iodide at 50℃; for 4h; | 65% |
Multi-step reaction with 2 steps 1: 1.) Na / 1.) THF, 3 h, reflux, 2.) 16 h, reflux 2: 89 percent / I2 View Scheme | |
With sodium iodide In DMF (N,N-dimethyl-formamide); acetonitrile at 20℃; for 1h; Product distribution / selectivity; |
H2SiEt2
ethyl iodide
A
triethylsilyl iodide
B
diethyldiiodosilane
Conditions | Yield |
---|---|
palladium dichloride at 60℃; for 12h; | A 36% B 31% |
Conditions | Yield |
---|---|
With iodine; aluminium | |
With aluminium(III) iodide; iodine | |
With I2; AlI3 | 65-77 |
With I2; Al | 65-77 |
Conditions | Yield |
---|---|
With iodine |
Conditions | Yield |
---|---|
With aluminium trichloride |
Conditions | Yield |
---|---|
Conditions | Yield |
---|---|
Conditions | Yield |
---|---|
Conditions | Yield |
---|---|
With methyl iodide; palladium dichloride In toluene at 80 - 90℃; for 17h; | A 1.65 g B 2.12 g |
acetyl iodide
hexaethyl disiloxane
A
triethylsilyl iodide
B
triethylsilyl acetate
Conditions | Yield |
---|---|
at 90℃; for 6h; | A 40 % Spectr. B 50 % Spectr. |
Conditions | Yield |
---|---|
[HIr(III)(1,3-(t-Bu2PO)2C6H3)*Me2CO](1+)*B(C6F5)4(1-) In various solvent(s) at 23℃; Kinetics; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 44 percent / acetyl iodide / 50 °C 2: 40 percent Spectr. / 6 h / 90 °C View Scheme | |
Multi-step reaction with 2 steps 1: Na / not given 2: I2 / chloroform View Scheme |
Conditions | Yield |
---|---|
In diethyl ether |
Conditions | Yield |
---|---|
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Na / neat (no solvent) 2: I2 / tetrachloromethane View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: C6H5NH2 View Scheme | |
Multi-step reaction with 3 steps 1: HCl / hydrogenchloride 2: C6H5NH2 / tetrachloromethane View Scheme |
1,1-dimethoxyethylene
triethylsilyl iodide
methyl (triethylsilyl)acetate
Conditions | Yield |
---|---|
98% |
triethylsilyl iodide
silver trifluoroacetate
triethylsilyl trifluoroacetate
Conditions | Yield |
---|---|
93% | |
triethylsilyl iodide
silver(1+) propionate
triethylsilyloxy propionate
Conditions | Yield |
---|---|
86% |
Conditions | Yield |
---|---|
In various solvent(s) electrolysis; | 80% |
With [{Ir(μ-Cl)(CO)2}2]; N-ethyl-N,N-diisopropylamine In toluene at 80℃; for 24h; Schlenk technique; Inert atmosphere; | 70 %Chromat. |
triethylsilyl iodide
diethyldiiodosilane
Conditions | Yield |
---|---|
With I2; AlI3 | 75% |
With aluminium(III) iodide; iodine | |
With iodine; aluminium |
triethylsilyl iodide
bis(triethylsilyl)-sulfide
Conditions | Yield |
---|---|
With Ag2S boiling of (C2H5)3SiI and Ag2S;; | 46% |
With silver sulfide | |
With mercury sulfide |
Conditions | Yield |
---|---|
With (DrewPhos)2PdI2; triethylamine In 1,4-dioxane at 20℃; for 4h; Negishi Coupling; Inert atmosphere; Schlenk technique; | 30% |
Conditions | Yield |
---|---|
With sodium |
Conditions | Yield |
---|---|
With silver carbonate | |
With silver nitrate | |
With HgO (C2H5)3SiI and HgO in coldness;; | |
With HgO (C2H5)3SiI and HgO in coldness;; |
Conditions | Yield |
---|---|
In benzene |
triethylsilyl iodide
Triethylstannylessigsaeure-triethylsilylester
Bis-O-triaethyl-silyl-ketenacetal
Conditions | Yield |
---|---|
triethylsilyl iodide
Methylester der γ-Iodmercuriacetessigsaeure
<1-Triaethylsiloxy-vinyl>-essigsaeure-methylester
Conditions | Yield |
---|---|
In Petroleum ether |
triethylsilyl iodide
-essigsaeure-methylester
<1-Methoxy-vinyloxy>-triaethyl-silan
Conditions | Yield |
---|---|
triethylsilyl iodide
diethyl mercuribis(diazoacetate)
(Diazo-ethoxycarbonylmethyl)-triethylsilane
Conditions | Yield |
---|---|
In diethyl ether |
Conditions | Yield |
---|---|
In pentane Heating; |
Conditions | Yield |
---|---|
In pentane Heating; |
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