Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:112-35-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:112-35-6
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inquiryProduct description: Product name Triethylene glycol monomethyl ether CAS number 112-35-6 Assay ≥99% Appearance Colorless transparent liquid Capacity 1000mt/year Application
Cas:112-35-6
Min.Order:1 Kilogram
FOB Price: $12.0
Type:Lab/Research institutions
inquiryFactory supply Triethylene glycol MonoMethyl ether CAS 112-35-6 with fast delivery Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediat
Cas:112-35-6
Min.Order:10 Kilogram
FOB Price: $10.0
Type:Trading Company
inquiryhigh purity Appearance:Colorless transparent liquid Storage:Sealed, dry, microtherm , avoid light and smell. Package:meet customer's demand Application:organic synthesis Transportation:by sea or by air Port:shanghai
Cas:112-35-6
Min.Order:1 Kilogram
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Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:112-35-6
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:112-35-6
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:112-35-6
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:112-35-6
Min.Order:1 Kilogram
FOB Price: $3.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:112-35-6
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:112-35-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Name: TRIETHYLENE GLYCOL MONOMETHYL ETHER CAS: 112-35-6 MF: C7H16O4 MW: 164.2 EINECS: 203-962-1 Mol File: 112-35-6.mol TRIETHYLENE GLYCOL MONOMETHYL ETHER Structure TRIETHYLENE GLYCOL MONOMETHYL ETHER Chemical Properties M
Cas:112-35-6
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryTRIETHYLENE GLYCOL MONOMETHYL ETHER CAS:112-35-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality
Cas:112-35-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:112-35-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:112-35-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:112-35-6
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:112-35-6
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Type:Lab/Research institutions
inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:112-35-6
Min.Order:4 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHigh purity 112-35-6 Methoxy Triglycol in bulk supply Best price Molecular Formula C7H16O4 Molar Mass 164.2 Density 1.026g/mLat 25°C(lit.) Melting Point -45°C(lit.) Boling Point 12
Cas:112-35-6
Min.Order:1 Gram
Negotiable
Type:Other
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:112-35-6
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirysupplier in China Appearance:Colorless odorless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as a brake fluid and chemical raw
Cas:112-35-6
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:112-35-6
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryProduct name: Tri-Ethylene Glycol Monomethyl Ether CAS No.:112-35-6 Molecule Formula:C7H16O4 Molecule Weight:164.20 Purity: 98.0% Package: 200kg/drum Description:Colorless and clear liquid Manufacture Standards:Enterprise Standard
Cas:112-35-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:112-35-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:112-35-6
Min.Order:0
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Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re
Cas:112-35-6
Min.Order:0
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Type:Other
inquiry3-Hydroxybenzyl alcohol
A
triethylene glucol monomethyl ether
B
3-Phenoxybenzyl alcohol
Conditions | Yield |
---|---|
A n/a B 87% |
dimethyl sulfate
2,2'-[1,2-ethanediylbis(oxy)]bisethanol
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
With sodium hydroxide at 120℃; for 4h; | 59% |
With sodium hydroxide at 120℃; |
triethylene glycol benzyl methyl ether
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
With hydrogen; palladium | 97% |
2-[2-(2-methoxyethoxy)etoxy]acetic acid
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
Stage #1: 2-[2-(2-methoxyethoxy)etoxy]acetic acid With chloroformic acid ethyl ester; triethylamine In tetrahydrofuran at 22℃; for 0.333333h; Stage #2: With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 1h; Stage #3: With potassium hydrogensulfate In tetrahydrofuran; ethyl acetate at 22℃; for 24h; | 17% |
A
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
With RG7 In toluene at 25℃; Equilibrium constant; |
dimethyl sulfate
2,2'-[1,2-ethanediylbis(oxy)]bisethanol
A
triethylene glucol monomethyl ether
B
Triethylene glycol dimethyl ether
Conditions | Yield |
---|---|
Stage #1: 2,2'-[1,2-ethanediylbis(oxy)]bisethanol With sodium hydroxide at 55 - 60℃; for 0.166667h; Stage #2: dimethyl sulfate at 55 - 60℃; for 6h; | A 33% B n/a |
Conditions | Yield |
---|---|
With solid alkali In 1,4-dioxane; water | 15% |
Conditions | Yield |
---|---|
With phosphoric acid at 60 - 70℃; | |
With sodium methylate at 60 - 140℃; |
triethylene glycol monobenzyl ether
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. NaOH 2: 97 percent / H2 / Pd View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aq. NaOH 2: aq. NaOH 3: 97 percent / H2 / Pd View Scheme |
methyl iodide
2,2'-[1,2-ethanediylbis(oxy)]bisethanol
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran for 2h; |
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane; water at 30℃; Rate constant; Kinetics; Thermodynamic data; ΔH(excit.), ΔS(excit.), var. temp.; |
2,5-dihydroxy-4-nitrobenzoic acid methyl ester
A
triethylene glucol monomethyl ether
B
methyl 2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)-4-nitrobenzoate
Conditions | Yield |
---|---|
With potassium carbonate In acetone Inert atmosphere; Reflux; |
Conditions | Yield |
---|---|
With sodium methylate |
bicyclo[2.2.1]hept-5-ene-2-carboxylic acid 2-(2-[2-methoxyethoxy]ethoxy)ethyl ester
A
triethylene glucol monomethyl ether
B
bicyclo[2.2.1]hept-2-ene-5-carbonyl chloride
Conditions | Yield |
---|---|
With Citric acid buffer; phosphoric acid at 80℃; pH=3.1; Kinetics; Further Variations:; pH-values; Temperatures; |
triethylene glucol monomethyl ether
3,6,9-trioxadecyl iodide
Conditions | Yield |
---|---|
Stage #1: triethylene glucol monomethyl ether With 1H-imidazole; triphenylphosphine In tetrahydrofuran at 20℃; for 0.05h; Inert atmosphere; Stage #2: With iodine In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; | 77% |
With 1H-imidazole; iodine; triphenylphosphine In toluene for 4h; Heating; | 53% |
Multi-step reaction with 2 steps 1: pyridine / CH2Cl2 2: NaI / acetone / 5 h / Heating View Scheme |
triethylene glucol monomethyl ether
1-chloro-3,6,9-trioxadecane
Conditions | Yield |
---|---|
With pyridine; thionyl chloride In chloroform for 3h; Heating; | 94% |
With pyridine; thionyl chloride In toluene at 60 - 80℃; for 3h; Cooling with ice; | 92% |
With pyridine; thionyl chloride In tetrahydrofuran | 90% |
triethylene glucol monomethyl ether
4-Nitrophthalonitrile
4-phthalonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 24h; | 82% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 24h; | 81% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 24h; | 75% |
triethylene glucol monomethyl ether
methanesulfonyl chloride
8-methoxy-1-(methylsulfonyl)oxy-3,6-dioxaoctane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 1.5h; | 100% |
With triethylamine In dichloromethane | 100% |
With triethylamine In dichloromethane at 0 - 20℃; for 2h; | 97% |
triethylene glucol monomethyl ether
carbonochloridic acid, chloromethyl ester
chloromethyl (2-(2-(2-methoxyethoxy)ethoxy)ethyl) carbonate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; for 22h; Inert atmosphere; | 99% |
With pyridine In dichloromethane at 0 - 20℃; | 99% |
With pyridine In dichloromethane | |
With pyridine In dichloromethane at 20℃; | |
With pyridine In dichloromethane at -78℃; for 3h; |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene at 110℃; for 4h; Dean-Stark; Inert atmosphere; | 90% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 25℃; for 2h; | 86% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 6h; | 86% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0 - 20℃; for 5h; | 99% |
With triethylamine In tetrahydrofuran at 0 - 20℃; for 5h; | 99% |
In dichloromethane at 0 - 20℃; for 16.5h; | 67% |
triethylene glucol monomethyl ether
propargyl bromide
3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)prop-1-yne
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran at 0 - 20℃; for 168h; Inert atmosphere; | 99% |
Stage #1: triethylene glucol monomethyl ether With sodium hydride In tetrahydrofuran; mineral oil at 0℃; Inert atmosphere; Stage #2: propargyl bromide With tetra-(n-butyl)ammonium iodide In tetrahydrofuran; mineral oil at 0 - 20℃; Inert atmosphere; | 91% |
With sodium hydride; sodium iodide In tetrahydrofuran; toluene; mineral oil at 20℃; for 16h; Inert atmosphere; | 85% |
triethylene glucol monomethyl ether
epichlorohydrin
2-((2-(2-(2-methoxyethoxy)ethoxy)ethoxy)methyl)oxirane
Conditions | Yield |
---|---|
Stage #1: triethylene glucol monomethyl ether With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 2h; Stage #2: epichlorohydrin In tetrahydrofuran; mineral oil at 20℃; for 20h; Reflux; | 91% |
With sodium hydride In tetrahydrofuran 1.) 2h, 2.) RT, 16h; 4h, reflux; | 86.6% |
With tetra(n-butyl)ammonium hydroxide; sodium hydroxide In water at 0 - 20℃; for 16h; Cooling with ice; | 79% |
triethylene glucol monomethyl ether
bromoacetic acid tert-butyl ester
tert-butyl (monomethoxy)triethylene glycol acetate
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 12h; | 98% |
Stage #1: triethylene glucol monomethyl ether With potassium tert-butylate In tert-butyl alcohol at 20℃; for 2h; Stage #2: bromoacetic acid tert-butyl ester In tert-butyl alcohol at 20℃; for 12h; | 75% |
With sodium hydride In tetrahydrofuran at 20 - 25℃; Cooling with ice; | 59.6% |
Stage #1: triethylene glucol monomethyl ether With sodium hydride In tetrahydrofuran; hexane at 0℃; for 0.5h; Inert atmosphere; Stage #2: bromoacetic acid tert-butyl ester In tetrahydrofuran; hexane at 0 - 20℃; for 15h; Inert atmosphere; | 50% |
With sodium hydride In tetrahydrofuran |
triethylene glucol monomethyl ether
2-Bromoacetyl bromide
2-bromoacetic acid-2-[2-(2-methoxyethoxy)ethoxy]ethyl ester
Conditions | Yield |
---|---|
With triethylamine In diethyl ether at 0 - 20℃; for 0.683333h; Inert atmosphere; | 73% |
With triethylamine In dichloromethane at -78℃; Inert atmosphere; | 58% |
With triethylamine In dichloromethane at -78 - -20℃; Inert atmosphere; | |
With sodium hydrogencarbonate In acetonitrile at 0℃; for 0.166667h; Inert atmosphere; |
triethylene glucol monomethyl ether
3,6,9-trioxadecyl bromide
Conditions | Yield |
---|---|
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0℃; for 5h; Inert atmosphere; | 84% |
With phosphorus tribromide In methanol; diethyl ether 1.) 0 deg C, 10 min, 2.) RT, 30 min; | 75% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0 - 50℃; for 12h; Inert atmosphere; | 70% |
di(succinimido) carbonate
triethylene glucol monomethyl ether
2,5-dioxopyrrolidin-1-yl (2-(2-(2-methoxyethoxy)ethoxy)ethyl)carbonate
Conditions | Yield |
---|---|
Stage #1: triethylene glucol monomethyl ether With triethylamine In dichloromethane at 0℃; for 0.25h; Stage #2: di(succinimido) carbonate In dichloromethane at 20℃; for 18h; | 75% |
With triethylamine In acetonitrile at 20℃; for 16.1667h; | 55% |
With triethylamine In acetonitrile at 20℃; | 20% |
With triethylamine In acetonitrile |
triethylene glucol monomethyl ether
D-glucal triacetate
A
2-(2-(2-methoxyethoxy)ethoxy)ethanyl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside
B
2-(2-(2-methoxyethoxy)ethoxy)ethanyl 4,6-di-O-acetyl-2,3-dideoxy-β-D-erythro-hex-2-enopyranoside
Conditions | Yield |
---|---|
With tellurium tetrachloride In dichloromethane at 0 - 20℃; for 0.25h; Ferrier Carbohydrate Rearrangement; Inert atmosphere; diastereoselective reaction; | A 86% B n/a |
With toluene-4-sulfonic acid In acetonitrile at 25℃; for 0.333333h; Sonication; | A 82% B n/a |
With tellurium tetrachloride In dichloromethane at 20℃; for 0.25h; Inert atmosphere; Overall yield = 86%; Overall yield = 0.32g; | A n/a B n/a |
triethylene glucol monomethyl ether
3,5-dinitrobenoyl chloride
2‐[2‐(2‐methoxyethoxy)ethoxy]ethyl 3,5‐dinitrobenzoate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 1h; | 89.3% |
In N,N-dimethyl acetamide for 8h; cooling; | 69% |
With triethylamine In dichloromethane at 0 - 20℃; |
3-Bromothiophene
triethylene glucol monomethyl ether
3-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)thiophene
Conditions | Yield |
---|---|
Stage #1: triethylene glucol monomethyl ether With pyridine; copper(l) iodide; potassium tert-butylate In toluene at 20℃; for 0.5h; Stage #2: 3-Bromothiophene In toluene at 110℃; for 24h; | 68% |
Stage #1: triethylene glucol monomethyl ether With copper(l) iodide; potassium tert-butylate at 20℃; for 1h; Inert atmosphere; Stage #2: 3-Bromothiophene at 100℃; for 24h; Inert atmosphere; | 63% |
With sodium hydride; copper(I) bromide In N,N-dimethyl-formamide | 23% |
Stage #1: triethylene glucol monomethyl ether With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Inert atmosphere; Stage #2: 3-Bromothiophene With copper(I) bromide In N,N-dimethyl-formamide at 110℃; for 12h; Inert atmosphere; | 11.6 g |
Conditions | Yield |
---|---|
Stage #1: triethylene glucol monomethyl ether With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.5h; Inert atmosphere; Stage #2: 1,3,6,9,12-pentaoxa-2-thiacyclotetradecane 2,2-dioxide In tetrahydrofuran; mineral oil at 20℃; for 12h; Inert atmosphere; Stage #3: With sulfuric acid In tetrahydrofuran; water for 3h; Reflux; | 98% |
Stage #1: triethylene glucol monomethyl ether With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.5h; Inert atmosphere; Stage #2: 1,3,6,9,12-pentaoxa-2-thiacyclotetradecane 2,2-dioxide In tetrahydrofuran; mineral oil at 20℃; for 12h; Inert atmosphere; Stage #3: With sulfuric acid; water In tetrahydrofuran for 3h; Inert atmosphere; Reflux; | 89% |
Stage #1: triethylene glucol monomethyl ether With sodium hydride In tetrahydrofuran; mineral oil for 0.5h; Inert atmosphere; Stage #2: 1,3,6,9,12-pentaoxa-2-thiacyclotetradecane 2,2-dioxide With sulfuric acid In tetrahydrofuran; water; mineral oil at 20℃; pH=3; Inert atmosphere; | 84% |
triethylene glucol monomethyl ether
ethyl bromoacetate
methoxytriethyleneglycol carboxylic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: triethylene glucol monomethyl ether With tetrabutylammomium bromide; sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Stage #2: ethyl bromoacetate In tetrahydrofuran at 0 - 20℃; | 78.74% |
Stage #1: triethylene glucol monomethyl ether With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.5h; Williamson Ether Synthesis; Stage #2: ethyl bromoacetate In tetrahydrofuran; mineral oil at 0 - 20℃; for 2h; Williamson Ether Synthesis; | 56% |
With sodium hydride In 1,2-dimethoxyethane for 1h; | 42% |
C17H12O3
triethylene glucol monomethyl ether
2-[2-(2-methoxyethoxy)ethoxy]ethyl 3-(4-methylphenyl)-1-oxo-1H-indene-2-carboxylate
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap In dichloromethane at 20℃; | 67% |
2-chloromethyl-3-chloroprop-1-ene
triethylene glucol monomethyl ether
3-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}-2-({2-[2-(2-methoxyethoxy)ethoxy]ethoxy}methyl)propene
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20 - 65℃; for 12.25h; Inert atmosphere; | 81% |
With sodium hydride In tetrahydrofuran at 65℃; | 35% |
With sodium hydride In tetrahydrofuran at 65℃; for 24h; | |
Stage #1: triethylene glucol monomethyl ether With sodium hydride In tetrahydrofuran; mineral oil at 60℃; for 0.5h; Inert atmosphere; Stage #2: 2-chloromethyl-3-chloroprop-1-ene In tetrahydrofuran; mineral oil at 20 - 65℃; Inert atmosphere; | |
With sodium hydride In tetrahydrofuran at 65℃; for 12h; Inert atmosphere; |
triethylene glucol monomethyl ether
4,4'-(5,5-difluoro-1,9-diphenyl-5H-4l4,5l4-dipyrrolo[1,2-c:2',1'-f][1,3,5,2]triazaborinine-3,7-diyl)diphenol
2-(N-tert-butoxycarbonylamino)ethanol
C46H49BF2N4O7
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 16.33h; | 39% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 16h; | 39% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 16h; Mitsunobu reaction; | 33% |
triethylene glucol monomethyl ether
toluene-4-sulfonic acid
2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran; water at 0℃; for 3h; | 99% |
With triethylamine In tetrahydrofuran; dichloromethane at 20℃; for 24h; Inert atmosphere; | 81.6% |
triethylene glucol monomethyl ether
tert-Butyl acrylate
tert-butyl 2,5,8,11-tetraoxatetradecan-14-oate
Conditions | Yield |
---|---|
With sodium methylate at 20℃; | 75.3% |
Stage #1: triethylene glucol monomethyl ether With sodium In tetrahydrofuran at 20 - 50℃; Inert atmosphere; Stage #2: tert-Butyl acrylate In tetrahydrofuran at 20 - 40℃; | 65% |
With hydrogenchloride In tetrahydrofuran |
triethylene glucol monomethyl ether
phthalocyanine silicon(IV) dichloride
bis(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)silicon phthalocyanine
Conditions | Yield |
---|---|
With sodium hydride In toluene at 120℃; for 24h; Inert atmosphere; | 54% |
With sodium hydride In toluene Inert atmosphere; Reflux; | 32.91% |
With sodium hydride In toluene at 125℃; for 16h; | 25% |
With potassium carbonate In toluene for 14h; Inert atmosphere; Reflux; | 15.6% |
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 60℃; for 12h; | 70% |
With sodium hydride In N,N-dimethyl-formamide at 80℃; for 12h; | 70% |
Stage #1: triethylene glucol monomethyl ether With sodium hydride In N,N-dimethyl-formamide at 0℃; Stage #2: 2-chloro-4-(6-(piperidin-1-yl)naphthalen-2-yl)nicotinonitrile In N,N-dimethyl-formamide at 0 - 60℃; for 12h; | 70% |
triethylene glucol monomethyl ether
Conditions | Yield |
---|---|
With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; sodium hydride In tetrahydrofuran at 20℃; for 5.5h; Inert atmosphere; Cooling with ice; | 75% |
triethylene glucol monomethyl ether
10,12-docosadiynedioic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran at 20℃; for 18h; | 84% |
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