As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:128-69-8
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inquiryItems Standard Result Appearance Bright red uniform powder Bright red uniform powder Purity (Acid anhydride va
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryProduct description: Product name 3,4,9,10-Perylenetetracarboxylic dianhydride CAS number 128-69-8 Assay ≥99% Appearance Red powder Capacity 500mt/year Application Pigment in
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inquiry3,4,9,10-Perylenetetracarboxylic dianhydride Cas 128-69-8 with fast delivery Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Fo
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inquiryT he company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality service Appearance:White
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiry1.Established manufacturer. 2.Current ISO certified; REACH registered. 3.Track record of quality, Lot to lot consistency. 4.Zero defect, Return policy. 5.Sufficient inventory. 6.Wide product portfolio, A great choice of shades. 7.Joint product develo
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:128-69-8
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:128-69-8
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryPigment Red 224 CAS NO: 128-69-8 Molecular formula: C24H8O6 Appearance: uniform bright red powder Moisture: ≤0.5% Color light: approximate (compared with standard product) Tinting strength: 100±3% (compared with standard product) Use: used
Appearance:Brown-red powder Storage:R.T Package:25kg/drum Application:Dye Intermediate Transportation:Express/Sea/Air Port:Any port in China
Cas:128-69-8
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
Cas:128-69-8
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inquiryProduct Name: 3,4,9,10-Perylenetetracarboxylic dianhydride CAS: 128-69-8 MF: C24H8O6 MW: 392.32 EINECS: 204-905-3 Mol File: 128-69-8.mol 3,4,9,10-Perylenetetracarboxylic dianhydride Structure 3,4,9,10-Perylenetetracarboxylic dianh
Cas:128-69-8
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inquiry3,4,9,10-Perylenetetracarboxylic dianhydride CAS:128-69-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in hig
Cas:128-69-8
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:128-69-8
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:128-69-8
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inquiryProduct name: 3,4,9,10-Perylenetetracarboxylic Dianhydride CAS No.:128-69-8 Molecule Formula:C24H8O6 Molecule Weight:392.31 Purity: 99% Package: 25kg/drum Description:Red powder Manufacture Standards:Enterprise Standard TESTING I
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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inquiryN-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
A
N-(1-hexylheptyl)-perylene-3,4,9,10-tetracarboxylic-3,4-carboximide-9,10-anhydride
B
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
Conditions | Yield |
---|---|
With potassium hydroxide In tert-butyl alcohol for 0.166667h; Heating; | A 63% B n/a |
With potassium hydroxide In tert-butyl alcohol Heating; | A 40% B n/a |
N,N'-bis(1-octylnonyl)-perylene-3,4,9,10-tetracarboxylic diimide
A
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
B
N-(1-octylnonyl)-perylene-3,4:9,10-tetracarboxylic acid-3,4-anhydride-9,10-carboximide
Conditions | Yield |
---|---|
With potassium hydroxide In tert-butyl alcohol Heating; | A n/a B 58% |
1,1'-binaphthyl-4,4',5,5',8,8'-hexacarboxylic acid dianhydride sodium salt
A
1,1'-binaphthyl-4,4',5,5',8,8'-hexacarboxylic acid dianhydride disodium salt
B
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
Conditions | Yield |
---|---|
Product distribution; Mechanism; electrolysis at -1.0 V; | A n/a B 55% |
N,N’-bis-(10-nonadecyl)perylene-3,4,9,10-tetracarboxylic acid diimide
A
9-(1-nonyldecyl)-1H-isochromeno[6',5',4':10,5,6]anthra[2,1,9-def]isoquinoline-1,3,8,10(9H)-tetraone
B
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
Conditions | Yield |
---|---|
With potassium hydroxide In tert-butyl alcohol Heating; | A 50.1% B n/a |
1,1'-binaphthyl-4,4',5,5'-tetracarboxylic acid dianhydride
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
Conditions | Yield |
---|---|
Product distribution; Mechanism; electrolysis at -1.3 V; | 3% |
perylene-3,4,9,10-tetracarboxylic acid
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
Conditions | Yield |
---|---|
With acetic anhydride | |
With sodium hydroxide | |
With sulfuric acid at 20℃; for 12h; |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: acetic acid; potassium dichromate / 6 h / 80 °C 2.1: ammonium hydroxide / 1.67 h / 20 - 70 °C 3.1: barium(II) hydroxide; sodium acetate / 6 h / 200 - 300 °C / Inert atmosphere 3.2: 1 h / 75 °C 3.3: 1.5 h / 80 - 100 °C 4.1: sulfuric acid / 2 h / 220 °C 4.2: 1 h / 90 °C / Darkness; Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1: acetic acid / 6 h / 20 - 80 °C 2: ammonium hydroxide / 1.67 h / 20 - 70 °C 3: potassium hydroxide; sodium acetate / dimethyl sulfoxide / 6 h / 100 °C / Microwave irradiation; Inert atmosphere 4: sulfuric acid / 2 h / 220 °C View Scheme |
1,8-Naphthalic anhydride
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: ammonium hydroxide / 1.67 h / 20 - 70 °C 2.1: barium(II) hydroxide; sodium acetate / 6 h / 200 - 300 °C / Inert atmosphere 2.2: 1 h / 75 °C 2.3: 1.5 h / 80 - 100 °C 3.1: sulfuric acid / 2 h / 220 °C 3.2: 1 h / 90 °C / Darkness; Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: ammonium hydroxide / 1.67 h / 20 - 70 °C 2: barium(II) hydroxide; sodium acetate / 6 h / 200 - 300 °C / Inert atmosphere 3: sulfuric acid / 2 h / 20 - 220 °C View Scheme | |
Multi-step reaction with 3 steps 1: ammonium hydroxide / 1.67 h / 20 - 70 °C 2: potassium hydroxide; sodium acetate / dimethyl sulfoxide / 6 h / 100 °C / Microwave irradiation; Inert atmosphere 3: sulfuric acid / 2 h / 220 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: barium(II) hydroxide; sodium acetate / 6 h / 200 - 300 °C / Inert atmosphere 1.2: 1 h / 75 °C 1.3: 1.5 h / 80 - 100 °C 2.1: sulfuric acid / 2 h / 220 °C 2.2: 1 h / 90 °C / Darkness; Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: barium(II) hydroxide; sodium acetate / 6 h / 200 - 300 °C / Inert atmosphere 2: sulfuric acid / 2 h / 20 - 220 °C View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide; sodium acetate / dimethyl sulfoxide / 6 h / 100 °C / Microwave irradiation; Inert atmosphere 2: sulfuric acid / 2 h / 220 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: acetic acid; potassium dichromate / 6 h / 20 - 80 °C 2: ammonium hydroxide / 1.67 h / 20 - 70 °C 3: barium(II) hydroxide; sodium acetate / 6 h / 200 - 300 °C / Inert atmosphere 4: sulfuric acid / 2 h / 20 - 220 °C View Scheme |
1-hexylheptylamine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
N-(1-hexylheptyl)perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-imide
Conditions | Yield |
---|---|
With 1H-imidazole at 180℃; for 5h; | 100% |
With 1H-imidazole In dichloromethane at 150℃; for 5h; | 100% |
With 1H-imidazole; zinc diacetate at 155℃; for 4h; | 99% |
1-pentanamine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
N,N’-bis(pentyl)-3,4:9,10-perylenebis(dicarboximide)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 4h; Reflux; | 100% |
With 1H-imidazole for 1h; | 96% |
In 1H-imidazole at 160℃; for 1h; Autoclave; | |
With zinc acetate hydrate In quinoline Reflux; | |
Stage #1: n-Pentylamine; perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride In water at 20℃; for 0.333333h; Green chemistry; Stage #2: In water at 200℃; for 24h; Autoclave; High pressure; Green chemistry; |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
1-aminooctadecane
N,N’-bis(octadecyl)-3,4:9,10-perylenebis(dicarboximide)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 8h; Reflux; | 100% |
With 1H-imidazole at 140℃; for 3h; | 89% |
63% |
Conditions | Yield |
---|---|
With 1H-imidazole at 100℃; for 1h; Inert atmosphere; | 100% |
With 1H-imidazole at 120℃; for 0.5h; | 97% |
With 1H-imidazole at 120℃; | 95.4% |
Conditions | Yield |
---|---|
Stage #1: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride With potassium hydroxide In water Stage #2: 1-dodecylbromide With potassium iodide | 100% |
With Aliquat 336; potassium iodide; potassium hydroxide Inert atmosphere; | 96% |
With 1-dodecyl alcohol; 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 60℃; for 12h; | 86% |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
perylene-3,4,9,10-tetracarboxylic acid monoanhydride monopotassium carboxylate
Conditions | Yield |
---|---|
Stage #1: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride With potassium hydroxide In water for 2h; Stage #2: With acetic acid In water at 90℃; for 0.666667h; | 99% |
Stage #1: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride With potassium hydroxide at 90℃; for 1h; Stage #2: With phosphoric acid | 96% |
Stage #1: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride With water; potassium hydroxide at 90℃; for 2h; Stage #2: With acetic acid at 90℃; for 0.666667h; | 96% |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
1,7-dibromoperylene-3,4,9,10-tetracarboxylic dianhydride
Conditions | Yield |
---|---|
Stage #1: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride With sulfuric acid; iodine at 20 - 85℃; for 0.75h; Stage #2: With bromine at 95℃; | 99% |
With sulfuric acid; bromine at 40℃; for 12h; | 95% |
With sulfuric acid; iodine | 95% |
2-Ethylhexylamine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
2,9-bis(2-ethylhexyl)anthra[2,1,9-def:6,5,10-d',e',f']diisoquinoline-1,3,8,10(2H,9H)-tetraone
Conditions | Yield |
---|---|
With 1H-imidazole; zinc diacetate at 160℃; for 5h; Inert atmosphere; | 99% |
With 1H-imidazole | 98% |
In N,N-dimethyl-formamide for 8h; Inert atmosphere; Reflux; | 97% |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
1,6,7,12-tetrachloro-perylene-3,4,9,10-tetracarboxylic acid dianhydride
Conditions | Yield |
---|---|
With sulfuric acid; chlorine at 120℃; | 99% |
With chlorosulfonic acid; iodine at 65℃; for 20h; | 98% |
With chlorosulfonic acid; iodine at 65℃; for 20h; | 94% |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
perylene-3,4,9,10-tetracarboxylic acid
Conditions | Yield |
---|---|
With potassium hydroxide In water for 12h; Heating; | 99% |
Stage #1: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride With potassium hydroxide In water at 20℃; for 6h; Stage #2: With hydrogenchloride In water pH=Ca. 7; | 80% |
With sodium hydroxide |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
N,N-dimethylethylenediamine
2,9-bis(2-(dimethylamino)ethyl)anthra[2,1,9-def:6,5,10-d′e′f ′]-diisoquinoline-1,3,8,10(2H,9H)-tetraone
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 200℃; for 0.966667h; Microwave irradiation; | 99% |
In iso-butanol at 90℃; for 24h; Inert atmosphere; | 97% |
In N,N-dimethyl-formamide at 130℃; for 5h; | 92% |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
2-(2-Aminoethoxy)ethanol
2,9-bis(2-(2-hydroxyethoxy)ethyl)anthra[2,1,9-def:6,5,10-d'e'f']diisoquinoline-1,3,8,10(2H,9H)-tetraone
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 200℃; for 0.966667h; Microwave irradiation; | 99% |
at 130℃; for 3h; | 94% |
at 130℃; for 3h; Inert atmosphere; | |
With N,N-dimethyl acetamide; zinc diacetate at 160℃; for 8h; Inert atmosphere; |
2-n-hexyldecan-1-amine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
N,N'-di(2-n-hexyldecyl)-perylene-3,4:9,10-tetracarboxylic acid bisimide
Conditions | Yield |
---|---|
With 1H-imidazole; zinc diacetate at 160℃; Inert atmosphere; | 99% |
With 1H-imidazole at 180℃; for 4h; Inert atmosphere; | 86% |
With 1H-imidazole at 160℃; for 5h; Inert atmosphere; | 71% |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
N,N;-bis(2-butyloctyl)-3,4,9,10-perylene diimide
Conditions | Yield |
---|---|
With 1H-imidazole; zinc diacetate at 160℃; Inert atmosphere; | 99% |
3-(1H-imidazol-1-yl)propan-1-amine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 200℃; for 0.966667h; Microwave irradiation; | 99% |
In N,N-dimethyl-formamide at 140℃; for 72h; | 95% |
In N,N-dimethyl-formamide at 140℃; | 92.3% |
In 2-methyl-propan-1-ol at 90℃; |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
2-methoxyethylamine
2,9-bis(2-methoxyethyl)anthra[2,1,9-def:6,5,10-d'e'f']-diisoquinoline-1,3,8,10(2H,9H)-tetraone
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 200℃; for 0.966667h; Microwave irradiation; | 99% |
Conditions | Yield |
---|---|
With 1H-imidazole In water at 145 - 180℃; for 15h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride With water; potassium hydroxide at 70℃; for 1.5h; Stage #2: 1-bromo-butane With Aliquat 336 at 100℃; for 2h; pH=9; | 98.1% |
Stage #1: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride With potassium hydroxide In water at 75℃; for 1.5h; Stage #2: 1-bromo-butane In water at 100℃; for 2h; | 94.8% |
Stage #1: perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride With potassium hydroxide In water at 75℃; for 1.5h; Stage #2: 1-bromo-butane With tetrabutylammomium bromide at 100℃; for 2h; | 94.8% |
cyclohexylamine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
N,N'-bis(cyclohexyl)perylene-3,4,9,10-tetracarboxylic acid diimide
Conditions | Yield |
---|---|
at 135℃; for 24h; | 98% |
for 15h; Reflux; | 93% |
at 140℃; for 15h; | 93% |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
3-aminopentane
N,N'-bis(1-ethylpropyl)-3,4:9,10-perylenebis(dicarboximide)
Conditions | Yield |
---|---|
With 1H-imidazole at 110℃; for 24h; | 98% |
With 1H-imidazole at 140℃; for 5h; Inert atmosphere; | 96% |
With 1H-imidazole at 200℃; for 2h; | 92% |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
1-amino-2-propene
N,N'-diallylperylene-3,4:9,10-tetracarboxylic acid bisimide
Conditions | Yield |
---|---|
With zinc diacetate In quinoline at 120℃; for 5h; | 98% |
With 1H-imidazole at 160℃; for 4h; | 42% |
With zinc diacetate In quinoline at 120℃; for 5h; |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
methylamine
N,N'-Dimethylperylene-3,4,9,10-biscarboximide
Conditions | Yield |
---|---|
In water for 3h; Heating; | 98% |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
1,7-dinitro-3,4,9,10-perylenetetracarboxylic acid
Conditions | Yield |
---|---|
With nitric acid In chloroform at 25 - 30℃; for 2.5h; | 98% |
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
N,N-diethylethylenediamine
N,N'-bis(2-(N'',N''-diethylamino)ethyl)perylene-3,4:9,10-bis(dicarboximide)
Conditions | Yield |
---|---|
for 26h; Reflux; | 98% |
In N,N-dimethyl-formamide at 80℃; Inert atmosphere; | 85% |
at 100℃; for 15h; |
2-octyldodecylamine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
Conditions | Yield |
---|---|
With 1H-imidazole; zinc diacetate at 160℃; Inert atmosphere; | 98% |
With 1H-imidazole In o-xylene at 180℃; for 4h; Inert atmosphere; | 93.2% |
With 1H-imidazole In o-xylene at 180℃; for 4h; Inert atmosphere; | 93% |
1-bromo-butane
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
butan-1-ol
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile for 18h; Reflux; | 98% |
With tetra(n-butyl)ammonium hydroxide; potassium carbonate In water at 120℃; for 2h; Time; Inert atmosphere; | 97% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 100℃; for 2h; | 93% |
3-(3,5,7,9,11,13,15-heptaisobutylpentacyclo[9,5,1,1(3,9),1(7,13),1(5,15)]octasiloxane-1-yl)propylamine
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride
N,N'-propylheptakis(isobutyl) POSS-perylene tetracarboxylic acid bisimide
Conditions | Yield |
---|---|
With 1H-imidazole for 0.0833333h; Microwave irradiation; | 98% |
With 1H-imidazole at 120 - 140℃; for 4h; | 95% |
With 1H-imidazole at 140℃; for 4h; | 95% |
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