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Cas:13568-40-6
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Cas:13568-40-6
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inquiryProduct Name: Lithium molybdate(VI) Synonyms: (beta-4)-molybdate(moo42-dilithium;Molybdate (MoO42-), dilithium, (T-4)-;Molybdate (MoO42-), dilithium, (T-4)-;LITHIUM METAMOLYBDATE;LITHIUM MOLYBDATE;LITHIUM MOLYBDATE(VI);LITHIUM
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Name Lithium molybdate CAS No 13568-40-6 Appearance White shiny crystalline powder.Soluble in water, ammonia and alkali solution. Usage 1. Used as
About Product Details Lithium molybdate Basic information Product Name: Lithium molybdate Synonyms: Molybdic acid dilithium salt;LITHIUM METAMOLYBDATE;LITHIUM MOLYBDATE;LITHIUM MO
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inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:13568-40-6
Min.Order:10 Gram
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inquiryLithium molybdate CAS : 13568-40-6.Molecular Formula: Li2MoO4Appearance: White crystalLi2MoO4: 99.5% min.H2O: 0.4% max.Li2CO3: 0.01% max. SO4: 0.05% max Cl: 0.01% max Fe2O3: 0.005% max NH3: 0.0002% max Ca: 0.0005% max Application:Used in Synthesis, P
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Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryConditions | Yield |
---|---|
In water pH 7-7.5; 2 h boiling on water bath; filtering, drying; | 94% |
In water pH 7-7.5; 2 h boiling on water bath; filtering, drying; | 94% |
In neat (no solvent, solid phase) for 5 mo; not isolated, detected by XRD; | |
Heating; |
Conditions | Yield |
---|---|
In water H2MoO4*H2O (1 mmol) added to aq. soln. of LiOH*H2O (2 mmol), stirred for20 min; filtered, allowed to stant (air) at room temp. for 1 week; | 87% |
Conditions | Yield |
---|---|
MoO3:Li2CO3 (1:1); reaction begins at 300°C; | |
heating (823 K); |
Conditions | Yield |
---|---|
byproducts: Li; above 1150 °C, Li2O a Mo crucible; | |
at 1320°C, in Mo vessel; | |
at 1320°C, in Mo vessel; |
Conditions | Yield |
---|---|
In neat (no solvent) mixing, firing in air (740K) in a silica crucible fo 48 h with one intermediate grinding; | |
In neat (no solvent) mixing of powdered and dried stoichiometric amounts of starting materials, firing in air at around 740 K for 48 h; |
Conditions | Yield |
---|---|
at 350°C, Li2O:MoO3 mol ratio beetween 1:1 and 2:1; | |
at 350°C, Li2O:MoO3 mol ratio beetween 1:1 and 2:1; |
Conditions | Yield |
---|---|
In water standing (some d); recrystn. (H2O); | |
In neat (no solvent) byproducts: H2O; ground under ambient conditions in air for 1 min, allowed to dry at roomtemp. for ca 1 h; |
Conditions | Yield |
---|---|
With ammonium molybdate In water | |
With ammonium molybdate In water |
Conditions | Yield |
---|---|
above 1150°C; | |
above 1150°C; |
Conditions | Yield |
---|---|
In not given byproducts: CaSO4; equilibrium react. at 25°C;; | |
In not given byproducts: CaSO4; equilibrium react. at 25°C;; |
Conditions | Yield |
---|---|
In neat (no solvent) reaction at 705°C;; | |
In neat (no solvent) reaction at 705°C;; |
Conditions | Yield |
---|---|
In neat (no solvent) accelerated reaction above 705°C;; |
A
lithium molybdate
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; 149°C; no isolation, monitoring by DTA; |
Conditions | Yield |
---|---|
In neat (no solvent) decomposition at 735°C;; |
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) MoO3, Bi2O3 and Li2CO3, milled for 4.5 h, dried, calcined at 500-550°C for 4 h, remilled for 5 h with H2O, pressed into pellets at 200 MPa with polyvinyl alcohol, sintered at 660°C for 2 h in ambient atm.; monitored by XRD; |
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) stoich. mixt. was initially calcined at 350°C, then annealed for 80-100 h; XRD; |
lithium carbonate
A
lithium molybdate
Conditions | Yield |
---|---|
In melt |
Conditions | Yield |
---|---|
In ethanol at 20℃; |
Conditions | Yield |
---|---|
at 500℃; for 5h; |
Conditions | Yield |
---|---|
at 400℃; for 4h; Temperature; |
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) Li2MoO4, ZnO, MoO2 and Mo powder in stoich. ratio were sealed in an evacuated tube and held at 1100°C for 5 days; ppt. was washed with HCl and deionized water, solid was then dried under vac. at 110°C; elem.anal.; | 90% |
lithium molybdate
iminodiacetic acid
Conditions | Yield |
---|---|
In water aq. soln. of Li2MoO4 (1 mmol) added to aq. soln. of iminodiacetic acid (1 mmol), refluxed for 6 h; filtered, allowed to stand (air) at room temp. for 4 weeks; elem. anal.; | 82% |
lithium molybdate
Methylenediphosphonic acid
water
lithium hydroxide
Conditions | Yield |
---|---|
With N2H4*H2O In water Mo compd. dissolved in HCl soln., N2H4*H2O added, stirred at 60°C, allowed to cool to room temp., Mo compd. and CH2(PO3H2)2 added, LiOH soln. added dropwise until pH 6.0; crystd. at room temp. for 5 d; elem. anal.; | 53% |
lithium molybdate
Methylenediphosphonic acid
water
lithium hydroxide
Conditions | Yield |
---|---|
With N2H4*H2O In water Mo compd. dissolved in HCl soln., N2H4*H2O added, stirred at 60°C, allowed to cool to room temp., LiOH soln. added dropwise until pH 1.5,CH2(PO3H2)2 added, LiOH soln. added dropwise until pH 3.5; crystd. for 5 d; elem. anal.; | 50% |
lithium molybdate
Conditions | Yield |
---|---|
With SnCl2*2H2O In hydrogenchloride addn. of aq. HCl to Li2MoO4 in H2O, addn. of SnCl2*2H2O; storage (20°C, 6 weeks), mechanical sepn. of crystals, washing (filtrated mother-liquor), drying in air on filter paper; | 4% |
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 7.5-20 mol % Na2MoO4 + 15.5-3 mol % Li2MoO4, Pt-electrodes, 0.02 to < 1 A cm**-2, 30-100°C over m. p. of electrolyte,6-8 h; washing of product deposited on cathode (hot water); |
lithium molybdate
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 3 mol % Na2MoO4 + 20 mol % Li2MoO4, Pt-electrodes, 1A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product mixt. deposited on cathode (hot water); powder X-ray diffraction; |
lithium molybdate
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 15.5 mol % Na2MoO4 + 7.5 mol % Li2MoO4, Pt-electrodes, 1 A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product mixt. deposited on cathode (hot water); powder X-ray diffraction; |
lithium molybdate
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 13 mol % Na2MoO4 + 10 mol % Li2MoO4, Pt-electrodes, 1 A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product mixt. deposited on cathode (hot water); powder X-ray diffraction; |
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 3 mol % Na2MoO4 + 20 mol % Li2MoO4, Pt-electrodes, 0.02 to < 1 A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product deposited on cathode (hot water); |
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 15.5 mol % Na2MoO4 + 7.5 mol % Li2MoO4, Pt-electrodes, 0.02 to < 1 A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product deposited on cathode (hot water); |
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 13 mol % Na2MoO4 + 10 mol % Li2MoO4, Pt-electrodes,0.02 to < 1 A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product deposited on cathode (hot water); |
Conditions | Yield |
---|---|
In melt Electrolysis; outgassed sample electrolysis (molar ratio MoO3:Li2MoO4=50.5:49.5, crucible, nitrogen flow, 560°C, 6.8 mA, start voltage 1.7 V, 6 d, end voltage 0.6 V); crystals sepn. (crucible soaking into hot dilute HCl); single crystal and powder X-ray diffraction, atomic absorption spectroscopy; | |
In neat (no solvent) Electrolysis; in MoO3 melt contg. 23 mol % Li2MoO4, Pt-electrodes, 0.02 to < 1 A cm**-2, 30-100°C over m. p. of electrolyte, 6-8 h; washing of product deposited on cathode (hot water); |
lithium molybdate
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 23 mol % Li2MoO4, Pt-electrodes, 1 A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product mixt. deposited on cathode (hot water); powder X-ray diffraction; |
Conditions | Yield |
---|---|
In melt Electrochem. Process; electrolytic redn. of a melt of Li2MoO4; | |
Electrolysis; electrolysis (0.03 A/cm**2, 4-5 h, 20-25 mol% Li2MoO4); detd. by gravimetry, X-ray photoelectron spectroscopy, laser emission spectroscopy, flame photometry, potentiometric titration; elem. anal.; | |
In neat (no solvent) Electrolysis; in MoO3 melt contg. 23 mol % Li2MoO4, Pt-electrodes, 0.02 to < 1 A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product deposited on cathode (hot water); |
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 18-13 mol % K2MoO4 + 5-10 mol % Li2MoO4, Pt-electrodes, 0.02 to < 1 A cm**-2, 30-100°C over m. p. of electrolyte, 6-8h; washing of product deposited on cathode (hot water); |
lithium molybdate
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 18 mol % K2MoO4 + 5 mol % Li2MoO4, Pt-electrodes, 1 A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product mixt. deposited on cathode (hot water); powder X-ray diffraction; |
lithium molybdate
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 13 mol % K2MoO4 + 10 mol % Li2MoO4, Pt-electrodes, 1A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product mixt. deposited on cathode (hot water); powder X-ray diffraction; |
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 18 mol % K2MoO4 + 5 mol % Li2MoO4, Pt-electrodes, 0.02 to < 1 A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product deposited on cathode (hot water); |
Conditions | Yield |
---|---|
In neat (no solvent) Electrolysis; in MoO3 melt contg. 13 mol % K2MoO4 + 10 mol % Li2MoO4, Pt-electrodes, 0.02 to < 1 A cm**-2, 10-15°C over m. p. of electrolyte, 6-8 h; washing of product deposited on cathode (hot water); |
lithium molybdate
molybdenum
Conditions | Yield |
---|---|
In melt Electrolysis; electrolysis of 77.5mol%KF-7.5mol%Li2B4O7-15.0%Li2MoO4 bath, anode: Mo or graphite, cathode: Ni, Cu, Mo, steel or graphite, varying bath temp. and current density; detn. by X-ray; |
Conditions | Yield |
---|---|
In water aq. soln. of 1 mol Li2MoO4 and 5 mol NH4Cl;; crystn.;; |
lithium molybdate
bismuth(III) oxide
Conditions | Yield |
---|---|
In neat (no solvent) melting; |
Conditions | Yield |
---|---|
In melt crystallization from melt;; separation from excess Li2MoO4 with boiling H2O;; |
Conditions | Yield |
---|---|
at 550°C; | |
at 550°C; |
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