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inquiryProduct Name: Lithium hydroxide Synonyms: Lithium Hydroxide Anhydrous [for General Organic Chemistry];"Lithium hydroxide, anhydrous/ 99%";Lithium hydroxide ,99% [anhydrous];LithiuM hydroxide, anhydrous, pure, 98% 500GR;LITHIU
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inquiryCAS No.: 1310-65-2 MW: 23.95 MF: LiOH MELTING POINT:462 °C BOLING POINT: 925°C PH: 12-14 (50g/l, H2O, 50℃) Properties: White crystals;Soluble in water and slightly soluble in ethanol Water solubility(100
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inquiryLithium hydroxide Basic information Product Name: Lithium hydroxide Synonyms: LiOH;Lithium hydroxide (Li(OH));lithiumhydroxide(li(oh));lithiumhydroxideanhydrous;Lit
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[CeCl3(H2O)]
methyllithium
A
methane
B
cerium chloride
C
lithium hydroxide
Conditions | Yield |
---|---|
In tetrahydrofuran (vac.); | A 40% B n/a C n/a |
Conditions | Yield |
---|---|
In gaseous matrix Kinetics; byproducts: H; react. of Li atoms and water vapour (excess), N2 bath gas, T = 850, 900, 925, 950, 973, 1000K; monitoring by time-resolved laser induced fluorescence (670.7 nm); | |
In neat (no solvent) on moist air, fast reaction;; | |
In tetrahydrofuran reactn. of excess of lithium with H2*O; (17)O/(18)O-enrichment: about 10% (17)O, about 40% (18)O; |
Conditions | Yield |
---|---|
In water formation of a lot of Li2O and a few LiOH;; determination with electron diffraction;; |
water
water-d2
lithium
A
LiOD
B
lithium hydroxide
Conditions | Yield |
---|---|
In water dissolving Li in mixt. of H2O and (2)H2O under Ar atmosphere; H/(2)H ratio in electrolyte 0.22+/-0.01; |
Conditions | Yield |
---|---|
byproducts: NH3; |
Conditions | Yield |
---|---|
In tetrahydrofuran; hexane (N2); using Schlenk techniques; addn. of soln. of n-BuLi in hexane to cooled soln. of water in THF; |
Conditions | Yield |
---|---|
In not given byproducts: HD; formation from LiD and water besides HD;; |
Conditions | Yield |
---|---|
In neat (no solvent) Kinetics; analysis of the equilibrium of the reaction, determination of partial pressure of CO2 depending on temp.;; | |
In neat (no solvent) Kinetics; analysis of the equilibrium of the reaction, determination of partial pressure of CO2 depending on temp.;; |
Conditions | Yield |
---|---|
Li2O is heated at 673 K in Ar saturated atmosphere with water vapour (parial pressure 1.5 kPa).; | |
In water vaporization of aq. Li2O soln., strong heating of residue;; | |
In neat (no solvent) formation with Li2O and the moisture of the air;; | |
In water vaporization of aq. Li2O soln., strong heating of residue;; | |
In neat (no solvent) formation with Li2O and the moisture of the air;; |
Conditions | Yield |
---|---|
With barium sulfate In water pptn. from Li2SO4 soln. with baryte, filtration, vaporization;; melting in platinum crucible;; | |
With barium sulfate In water pptn. from Li2SO4 soln. with baryte, boiling very diluted soln. in platinum or silver crucible, melting at 445°C;; pouring on silver plate, crushing; LiOH contains water;; | |
With baryte In water pptn. from Li2SO4 soln. with baryte, boiling very diluted soln. in platinum or silver crucible, melting at 445°C;; pouring on silver plate, crushing; LiOH contains water;; | |
With baryte In water pptn. from Li2SO4 soln. with baryte, filtration, vaporization;; melting in platinum crucible;; |
Conditions | Yield |
---|---|
With water In melt hydrolytic decompn.; | |
With H2O In melt hydrolytic decompn.; |
lithium hydroxide
Conditions | Yield |
---|---|
With air In neat (no solvent) formation by reaction of LiCl with dry air;; | |
With air; H2O In melt byproducts: Li2CO3, HCl; decompn. on melting on air;; | |
With air |
Conditions | Yield |
---|---|
With water In water equilibrium; depending on temp. (25.0-99.5°C); | |
With H2O In water |
Conditions | Yield |
---|---|
With air In neat (no solvent) formation on reaction with air at normal temp.;; identification by electron diffraction;; | |
With air In neat (no solvent) formation on reaction with air at normal temp.;; identification by electron diffraction;; |
lithium
A
copper
B
lithium hydroxide
Conditions | Yield |
---|---|
With hydrogen In neat (no solvent) in the presence of H2, formation of LiOH and Li2O;; | |
With H2 In neat (no solvent) in the presence of H2, formation of LiOH and Li2O;; |
lithium hydroxide
Conditions | Yield |
---|---|
With lime milk | |
With calcium hydroxide In not given on heating spodumene to 1100-1150°C and then treating with lime milk at 100-205°C under pressure;; |
Conditions | Yield |
---|---|
In not given |
Conditions | Yield |
---|---|
In not given byproducts: NaF, Si(OH)4; reaction of Li2SiF6 with NaOH, formation of LiOH, NaF and Si(OH)4;; |
Conditions | Yield |
---|---|
In not given byproducts: Na2SO4; on cooling reaction of Li2SO4 with NaOH until Na2SO4 is crystallized, then crystallizing of pure LiOH;; |
lithium hydroxide
Conditions | Yield |
---|---|
With calcium oxide In not given byproducts: Ca(OH)2, CaO*Al2O3; mixture is cooled with air and crushed wet, soluble LiOH is formed;; |
Conditions | Yield |
---|---|
With Mg-amalgam In water byproducts: Mg(OH)2, NH2OH; exotherm reaction; drying over H2SO4; | |
With Mg-amalgam In water byproducts: Mg(OH)2, NH2OH; exotherm reaction; drying over H2SO4; |
Conditions | Yield |
---|---|
In water byproducts: CO2; equil.;; | |
In water determination of equil. in boiling soln.;; | |
In water determination of equil. in boiling soln.;; | |
In water byproducts: CO2; equil.;; |
Conditions | Yield |
---|---|
In not given reaction of Li2SiO3 with Ca(OH)2;; | |
In water 5-6 h boiling of mixt. of Li2CO3, Ca(OH)2 and H2O with stirring, filtration, vaporization of filtrate;; melting in silver crucible;; | |
In water 5-6 h boiling of mixt. of Li2CO3, Ca(OH)2 and H2O with stirring, filtration, vaporization of filtrate;; melting in silver crucible;; | |
In not given reaction of Li2SiO3 with Ca(OH)2;; |
lithium hydroxide
Conditions | Yield |
---|---|
With methyllithium In water aq. soln. of Li2SO4 reacts with lime to LiOH;; | |
With lime In water |
Conditions | Yield |
---|---|
In water mixing hot satd. soln. of Ba(OH)2 with small excess of hot satd. Li2SO4 soln., decantation of clear soln. after storage for few days;; carbonate free aq. soln. of LiOH;; | |
In not given formation of pure LiOH;; | |
In water mixing hot satd. soln. of Ba(OH)2 with small excess of hot satd. Li2SO4 soln., decantation of clear soln. after storage for few days;; carbonate free aq. soln. of LiOH;; |
Conditions | Yield |
---|---|
Kinetics; other Radiation; Irradiation with a CW CO2 laser at an output power of P=25 W.; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; heating in stream of dry H2 at various temp.;; | |
below 140°C in dry H2 stream; | |
byproducts: H2O; 140°C; X-ray diffraction, atomic absorption; |
C
lithium hydroxide
Conditions | Yield |
---|---|
In water byproducts: H2O; hydrolysis, in nickel autoclave, above 200°C; |
Conditions | Yield |
---|---|
With water In water with water and exclusion of air, decomposition in PH3, LiOH and NH3; sinilary reaction with dild. acids;; | |
With H2O In water with water and exclusion of air, decomposition in PH3, LiOH and NH3; sinilary reaction with dild. acids;; |
Conditions | Yield |
---|---|
In water with water decomposition in PH3 and LiOH;; | |
In water with water decomposition in PH3 and LiOH;; |
methyl 3-(4-(tert-butoxycarbonylamino)-1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidine-4-carboxamido)-3-(4-chlorophenyl)propanoate
lithium hydroxide
methyl 3-(4-(tert-butoxycarbonylamino)-1-(7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidine-4-carboxamido)-3-(4-chlorophenyl)propanoate
Conditions | Yield |
---|---|
In tetrahydrofuran; water at 20℃; | 100% |
Conditions | Yield |
---|---|
In ethylene glycol at 215℃; for 36h; Time; Solvent; Autoclave; High pressure; | 100% |
lithium hydroxide
Conditions | Yield |
---|---|
In water (Et3NH)2(B12H12) was added to 2 equiv. aq. soln. LiOH and heated until soln. became clear; soln. was evapd. to dryness and dried in vacuo at 150-200°C; | 99% |
In water byproducts: Et3N, H2O; purging of soln. with N2 (80°C, 2 h); filtration., evapn. of soln. (vac., 80°C), drying (vac. 140°C); | 91% |
lithium hydroxide
Conditions | Yield |
---|---|
In water neutralized; | 99% |
Conditions | Yield |
---|---|
In water; isopropyl alcohol by dissolving mixt. of educts (in 1:3 molar ratio) in small amt. of H2O on steam bath; addn. of i-propanol to hot soln., cooling to room temp.; filtering under N2; washing with i-propanol and anhydrous ether; purified by dissolving in ether and pptn. with i-propanol; | 98% |
In water; isopropyl alcohol |
tris(2,6-dimethoxyphenyl)borane
lithium hydroxide
Conditions | Yield |
---|---|
In methanol; water | 98% |
lithium hydroxide
Conditions | Yield |
---|---|
In methanol; water for 3h; Reflux; | 98% |
9-ethyl-9-borabicyclo[3.3.1]nonane
lithium hydroxide
lithium 1,5-cyclooctanediylethylhydroxoborate
Conditions | Yield |
---|---|
In tetrahydrofuran Ar atmosphere; addn. of B-compd. in THF to LiOH in THF (25 min), stirring (room temp.); partial evapn. (12 Torr), drying (20°C, 0.001 Torr), not pure, elem. anal.; | 97% |
piperazinium oxalate monohydrate
lithium hydroxide
Conditions | Yield |
---|---|
In water High Pressure; Ni(OH)2, (C4H12N2)(C2O4)*H2O, LiOH and H2O heated in autoclave to 180°C for 72 h, cooled; elem. anal.; | 97% |
lithium hydroxide
Conditions | Yield |
---|---|
In methanol; water 20°C; 48 h;; elem. anal.;; | 96% |
Conditions | Yield |
---|---|
In water H2O, an aq. soln. of H2O2, LiOH soln., and U salt combined and stirred; MeOH or EtOH or i-PrOH added rapidly, filtered; | 96% |
2,3-dichloro-pyridine
2-(prop-2-yloxycarbonyl)-5-trfluoromethylphenylboronic acid
lithium hydroxide
2-(3-chloro-pyridin-2-yl)-4-trifluoromethyl-benzoic acid
Conditions | Yield |
---|---|
Stage #1: 2,3-dichloro-pyridine; 2-(prop-2-yloxycarbonyl)-5-trfluoromethylphenylboronic acid With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,4-dioxane; water at 30 - 110℃; for 20h; Inert atmosphere; Stage #2: lithium hydroxide In 1,4-dioxane; water at 70℃; | 96% |
lithium hydroxide
Conditions | Yield |
---|---|
In ethanol; water in H2O/EtOH at room temp.; | 95% |
lithium hydroxide
Conditions | Yield |
---|---|
In ethanol; water in H2O/EtOH at room temp.; | 95% |
(S)-methyl 1-((6-(hydroxymethyl)pyridin-2-yl)methyl)pyrrolidine-2-carboxylate
lithium hydroxide
lithium (S)-1-((6-(hydroxymethyl)pyridin-2-yl)methyl)pyrrolidine-2-carboxylate
Conditions | Yield |
---|---|
In methanol; water for 3h; Reflux; | 95% |
Conditions | Yield |
---|---|
In water for 18h; Schlenk technique; Inert atmosphere; | 95% |
lithium hydroxide
Conditions | Yield |
---|---|
In ethanol at 70℃; | 95% |
Conditions | Yield |
---|---|
In water pH=7; | 95% |
Conditions | Yield |
---|---|
In water pH 7-7.5; 2 h boiling on water bath; filtering, drying; | 94% |
In water pH 7-7.5; 2 h boiling on water bath; filtering, drying; | 94% |
In neat (no solvent, solid phase) for 5 mo; not isolated, detected by XRD; | |
Heating; |
Conditions | Yield |
---|---|
With ethanol In ethanol byproducts: CH3CHO, H2O; High Pressure; equimolar amount of LiOH and V2O5 put into autoclave, filled with ethanol up to 80% of total volume, kept at 160°C under autogeneous pressure for 24 h, cooled to room temp. naturally; precipitate filtered, washed with ethanol, dried at 100°C for 2 h; | 94% |
water
titanium tetrachloride
citric acid monohydrate
lithium hydroxide
Conditions | Yield |
---|---|
In water TiCl4 added dropwise to a water on ice bath, acid added at room temp., pH adjusted to 2 (LiOH); stored for several d at room temp.; elem. anal.; | 93.7% |
Conditions | Yield |
---|---|
With citric acid In tetrahydrofuran; water Fe compd. and LiOH (1:2.5 molar ratio) stirred in THF/H2O (30/1, v/v) atroom temp. for 48 h; soln. poured in 10% citric acid, extd. (ethyl acetate), washed (H2O), dried (Na2SO4), filtered, evapd. (vac.), elem. anal.; | 93% |
lithium hydroxide
[HO(CH2)10C(C4HN(CH3)2)2BF2]
Conditions | Yield |
---|---|
With potassium acetate In not given | 92% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 24h; | 91.2% |
Conditions | Yield |
---|---|
Stage #1: C35H42N4O9; lithium hydroxide In tetrahydrofuran; methanol; water at 0 - 20℃; for 12h; Stage #2: With trifluoroacetic acid In tetrahydrofuran; methanol; water at 0 - 20℃; for 5h; | 91% |
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol at 0 - 28℃; for 48h; Inert atmosphere; Schlenk technique; | 91% |
P-trans-Cl{Rh(o-diphenylphosphinophenylamine)(CO)Cl}
lithium hydroxide
Conditions | Yield |
---|---|
In water; acetone LiOH in water added to Rh-complex in acetone under N2-atmosphere; stirred for 2 h;; water added with stirring, ppt. filtered off and washed with water, elem. anal;; | 90% |
[Pt(NHC(C6H5)N(C4H9)CH2CH2NH(C4H9))Cl(NC(C6H5))](1+)*Cl(1-)
lithium hydroxide
[Pt(NHC(C6H5)N(C4H9)CH2CH2NH(C4H9))Cl(NHC(O)C6H5)]*CH3OH
Conditions | Yield |
---|---|
With methanol In methanol to soln.of Pt complex in MeOH is added dropwise soln. of stoich. amt. of LiOH in MeOH; evapd. in vac., extd. with CH2Cl2, evapd., recrystd. from MeOH; elem. anal.; | 90% |
dichloro(benzene)ruthenium(II) dimer
lithium hydroxide
Conditions | Yield |
---|---|
In water-d2 5 equiv. of LiOH added to soln. of (C6H6RuCl2)2 and C4H10N2(CH2C5H2N(OH)2)2; not isolated, detected by NMR; | 90% |
lithium hydroxide
Conditions | Yield |
---|---|
With citric acid In tetrahydrofuran; water Fe compd. and LiOH (1:2.5 molar ratio) stirred in THF/H2O (30/1, v/v) atroom temp. for 48 h; soln. poured in 10% citric acid, extd. (ethyl acetate), washed (H2O), dried (Na2SO4), filtered, evapd. (vac.), elem. anal.; | 90% |
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