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inquiryGood quantity Titanium tetrachloride Basic information Product Name: Titanium tetrachloride Synonyms: (t-4)-titaniumchloride(ticl4;Tetrachlorure de titane;tetrachloruredetitane;tetrach
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titanium tetrachloride
Conditions | Yield |
---|---|
TiO2 contained with 2%MnO2; chlorination at 600°C; | 96.08% |
TiO2 contained with 2%MnO2; chlorination at 700°C; | 96.68% |
TiO2 contained with 2%MnO2; chlorination at 600°C; | 96.08% |
titanium tetrachloride
Conditions | Yield |
---|---|
chlorination at 740°C; | 95.58% |
chlorination at 640°C; | 79.52% |
chlorination at 520°C; | 68.51% |
titanium tetrachloride
Conditions | Yield |
---|---|
chlorination at 850°C; | 28% |
chlorination at 740°C; | 25.1% |
chlorination at 640°C; | 13.1% |
chloroform
A
hydrogenchloride
B
hexachlorobenzene
C
titanium tetrachloride
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: CO; TiO2/C mixt. (various ratio) heating in thermogravimetric analyzer at 2.7 K/min in Ar flow, Cl2 (p(Cl2)=33 kPa) introducing at 598 K, further heating up to 1000 K; TG; |
Conditions | Yield |
---|---|
In neat (no solvent) chlorination (molar ratio SCl4:TiO2 = 2:1); |
titanium tetrachloride
Conditions | Yield |
---|---|
chlorination; distilling, shaking with Na-amalgame for 48h in dry H2; | |
chlorination; distilling, shaking with Na-amalgame for 48h in dry H2; |
Conditions | Yield |
---|---|
In neat (no solvent) chlorination (fused silica reactor, 773, 973, 1173, and 1373 K, Cl2 velocity 1 cm/s); removal of Cl2 and TiCl4 on heat treatment (synthesis temp., vac., 1 h); | A n/a B >99 |
A
tetrachlorosilane
B
titanium tetrachloride
C
copper
Conditions | Yield |
---|---|
In neat (no solvent) Kinetics; CuCl and Si2Ti mixt. heated in evac. glass tube reactor (0.1 Pa) at 250-310°C, SiCl4 condn. in liquid nitrogen trap; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2, N2, TiCl3; transport reaction; small reaction rate at 1000°C, high reaction rate at 1500°C;; | |
byproducts: NH3; dry HCl is used;; | |
byproducts: NH3; dry HCl is used;; | |
In neat (no solvent) byproducts: H2, N2, TiCl3; transport reaction; small reaction rate at 1000°C, high reaction rate at 1500°C;; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: POCl3, FeCl2; passing vapor of PCl5 over hot ilmenite;; |
Conditions | Yield |
---|---|
With chlorine glowing; | |
With chlorine 325 ° C; | |
With chlorine finely dispersed Ti at 30 °C with clean, dry Cl2 gas or Cl2 gas contg. less than 0.005% water; |
Conditions | Yield |
---|---|
In neat (no solvent) a stream of water-free HCl is used;; |
Conditions | Yield |
---|---|
In melt berillium oxide crucible with TiO2 and CaCl2 heated at 840°C for 2.5 h; TiCl4 vapor condencat not observed; | 0% |
Conditions | Yield |
---|---|
In neat (no solvent) passing stream of COCl2 over TiO2 at 450 °C;; |
Conditions | Yield |
---|---|
higher temp. in Pt pot; | |
higher temp. in Pt pot; |
Conditions | Yield |
---|---|
byproducts: CO, HCl; | |
byproducts: CO, HCl; |
titanium(IV) iodide
phosphorus trichloride
A
phosphorous triiodide
B
titanium tetrachloride
Conditions | Yield |
---|---|
In not given react. with TiI4;; | |
In not given react. with TiI4;; |
titanium tetrachloride
Conditions | Yield |
---|---|
byproducts: FeCl3; red heat, chlorination; | |
With tetrachloromethane red heat, in tube; | |
With COCl2 600 °C; |
2-(3-tert-butyl-2-hydroxy-5-methylbenzylthio)-6-tert-butyl-4-methylphenol
titanium tetrachloride
Conditions | Yield |
---|---|
In dichloromethane at 0 - 20℃; for 0.5h; | 100% |
Conditions | Yield |
---|---|
TiCl4 was added to deionized H2O, mixt. was stirred for 16 h at room temp., mixt was dialyzed in deionized H2O to pH 2.0; | 100% |
In hydrogenchloride other Radiation; soln. of TiCl4 in cold 2 M HCl, hydrolysed, TiOCl2 formed, soln. transferred to Teflon container, treated in microwave oven (2.45 GHz) at temp. of 120°C for 120 min, or at 140°C for 60 or 120 min, or at160°C for 5 or 30 min; washed (deionized H2O, ethanol, repeatedly), dried in oven at 60°C for 16 h, detd. by XRD, mixt. of rutile and anatase obtained; | 99% |
In hydrogenchloride other Radiation; soln. of TiCl4 in cold 2 M HCl, hydrolysed, TiOCl2 formed, soln. transferred to Teflon container, treated in microwave oven (2.45 GHz) at temp. of 160°C for 60 min; washed (deionized H2O, ethanol, repeatedly), dried in oven at 60°C for 16 h, detd. by XRD, mixt. of rutile and anatase obtained; | 98% |
Conditions | Yield |
---|---|
In dichloromethane (Ar), at 0°C, dropwise addn. of TiCl4 with stirring, stirred for 15 min, brought to 25°C, stirred for 45 min; evapd. in vacuo, elem. anal.; | 100% |
N,N,N,N,-tetramethylethylenediamine
titanium tetrachloride
tetrachloro(N,N,N',N'-tetramethylethane-1,2-diamine)titanium(IV)
Conditions | Yield |
---|---|
In hexane at 0℃; for 1h; Inert atmosphere; | 100% |
In benzene solns. mixed at 10-20°C; filtered, washed (benzene), dried (vac.); elem. anal.; | >99 |
In pentane solns. mixed at 10-20°C; filtered, washed (pentane), dried (vac.); elem. anal.; | >99 |
α-naphthol
titanium tetrachloride
[dichlorobis(1-naphtholate)titanium(IV)]
Conditions | Yield |
---|---|
In toluene byproducts: HCl; N2, vigorously refluxed for 12 h; cooled, filtered, solvent removed; | 100% |
Conditions | Yield |
---|---|
In benzene under moisture-free conditions; freshly distd. TiCl4 added to a soln. of thioaldehyde; mixt. stirred (2 h, room temp.); filtered; washed (pentane); dried (high vac., room temp.); elem. anal.; | 100% |
2-{[(1-methylethyl)imino]methyl}phenol
titanium tetrachloride
bis(κN,κO-N-isopropylsalicylaldiminato)TiCl2
Conditions | Yield |
---|---|
With 1,1,1,3,3,3-hexamethyldisilazane In dichloromethane; toluene (under Ar, Schlenk); hexamethyldisilazane added to soln. of ligand in CH2Cl2, stirred overnight, evapd. under vac. at 50°C, ligand in toluene added to toluene soln. of TiCl4 at -78°C, warmed to ambient temp., stirred overnight; heated at 50°C under vac.; elem. anal.; | 100% |
Conditions | Yield |
---|---|
In benzene under moisture-free conditions; equimolar quantity of freshly distd. TiCl4 added to a soln. of thioaldehyde; mixt. stirred (2 h, room temp.); filtered; washed (pentane); dried (high vac., room temp.); elem. anal.; | 100% |
titanium tetrachloride
Conditions | Yield |
---|---|
In dichloromethane Ar-atmosphere; stirring of equiv. amts. of ligand and TiCl4 for 2 h at room temp.; concn. (vac.), washing (ether, ether/petroleum ether=1/1), recrystn. (CHCl3); elem. anal.; | 100% |
N-(1-adamantyl)-salicylaldamine
titanium tetrachloride
bis(κN,κO-N-adamantylsalicylaldiminato)TiCl2
Conditions | Yield |
---|---|
With 1,1,1,3,3,3-hexamethyldisilazane In dichloromethane; toluene (under Ar, Schlenk); hexamethyldisilazane added to soln. of ligand in CH2Cl2, stirred overnight, evapd. under vac. at 50°C, ligand in toluene added to toluene soln. of TiCl4 at -78°C, warmed to ambient temp., stirred overnight; heated at 50°C under vac.; elem. anal.; | 100% |
adamantyl-N-(3-tert-butylsalicylaldimine)
titanium tetrachloride
bis(κN,κO-N-adamantyl-3-tert-butylsalicylaldiminato)TiCl2
Conditions | Yield |
---|---|
In toluene (under Ar, Schlenk); ligand in toluene added to toluene soln. of TiCl4 at -78°C, warmed to ambient temp., stirred overnight; elem. anal.; | 100% |
titanium tetrachloride
Conditions | Yield |
---|---|
In dichloromethane ligand dissolved in CH2Cl2; soln. of TiCl4 in CH2Cl2 added; stirred for 1 h; solvent evapd. in vac.; taken up in Et2O; stirred for 5 min; ether layerdecanted; hexane-Et2O added to residue; stirred briefly; decanted; drie d in vac.; | 100% |
HOC6H2Br2CH2N(CH3)C2H4NCHC6H2(OH)(C(CH3)3)2
titanium tetrachloride
C25H32Br2Cl2N2O2Ti
Conditions | Yield |
---|---|
In toluene for 0.25h; | 100% |
Conditions | Yield |
---|---|
With titanium(IV) isopropylate In toluene at -30℃; | 100% |
Conditions | Yield |
---|---|
In toluene Schlenk technique; Inert atmosphere; Glovebox; | 100% |
Conditions | Yield |
---|---|
Stage #1: tetrahydrofuran; C34H36N2O2 With n-butyllithium In hexane at -78 - 20℃; for 2.16667h; Stage #2: titanium tetrachloride In hexane at -78 - 20℃; for 18.3333h; | 100% |
1-(2,6-diisopropylphenyl)-3-(2-hydroxyphenyl)-4,5-dihydro-imidazolyl chloride
titanium tetrachloride
Conditions | Yield |
---|---|
Stage #1: 1-(2,6-diisopropylphenyl)-3-(2-hydroxyphenyl)-4,5-dihydroimidazolium chloride With potassium hexamethylsilazane In tetrahydrofuran at 20℃; for 0.166667h; Stage #2: titanium tetrachloride In tetrahydrofuran; toluene at 20℃; for 2h; | 100% |
Conditions | Yield |
---|---|
In hexane at 0℃; for 1h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In toluene at -78 - 20℃; for 21h; Schlenk technique; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In toluene at -78 - 100℃; for 13h; | 99.4% |
Conditions | Yield |
---|---|
With calcium hydroxide for 2h; Autoclave; Cooling with ice; Inert atmosphere; Green chemistry; | 99.3% |
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