CAS No.13569-75-0,CHROMIUM (IC) IODIDE Suppliers

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Product Introduction： Anhydrous Tri Chromium(III) iodide Anhydrous Tri Chromium(III) iodide Purity：99.9% Overview Anhydrous Tri Chromium(III) iodide Purity：99.9% Technical Parameter Anhydrous Tri Chromium(III) iodide Purity：99.9% Appearan

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Chromium iodide (CrI3)Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Protect them

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Synthetic route

: 7440-47-3
chromium

: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
With iodine
With iodine

: 7440-47-3
chromium

: 10034-85-2
hydrogen iodide

A: chromium(II) iodide

B: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
In water byproducts: H2; Cr dissolves at room temp. in aq. HI at concns. 2.2-2.4 Mol/l; at elevated temps. the concn. may be 1.70-2.00 Mol/l; the products CrI2 and CrI3 form an equilibrium.; no products isolated;;
min. concn. of HI for dissolution of Cr in cold and warm given;
min. concn. of HI for dissolution of Cr in cold and warm given;
In water byproducts: H2; Cr dissolves at room temp. in aq. HI at concns. 2.2-2.4 Mol/l; at elevated temps. the concn. may be 1.70-2.00 Mol/l; the products CrI2 and CrI3 form an equilibrium.; no products isolated;;

...Expand

: chromium(III) sulphide

: 7784-23-8
aluminium(III) iodide

: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
In neat (no solvent) byproducts: Al2S3; react. at 350 °C. 48 h;; extraction with H2O;;
In neat (no solvent) byproducts: Al2S3; react. at 350 °C. 48 h;; extraction with H2O;;

: 7440-47-3
chromium

: 7553-56-2
iodine

: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
In neat (no solvent) enclosing Cr and I2 under high vac. in a sublimation tube; heating Cr up to 475 °C; react. with I2 vapor (formed by heating I2 up to 225 °C), 24h;;
In neat (no solvent) enclosing Cr and I2 under high vac. in a sublimation tube; heating Cr up to 475 °C; react. with I2 vapor (formed by heating I2 up to 225 °C), 24h;;
In neat (no solvent) react. of gaseous I2 (in carrier gas N2) with Cr at 1200 °C;;
In neat (no solvent, solid phase) High Pressure; Cr and I2 were heated for 12 h in sealed, evaculated tube at 170-450°C;

: chromium(II) iodide

: 7553-56-2
iodine

: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
In neat (no solvent) react. of CrI2 with I2 vapor (1 atm) at 500 °C;;
In neat (no solvent) react. of CrI2 with I2 vapor (1 atm) at 500 °C;;

: potassium iodochromat(VI)

: 10034-85-2
hydrogen iodide

A: 13569-75-0
chromium(III) iodide

B: 7553-56-2
iodine

Conditions

Conditions	Yield
In water byproducts: KI; decompn. by boiling HI soln.;;
In water byproducts: KI; decompn. by boiling HI soln.;;

...Expand

: 4Cr(3+)*2H(1+)*7SO4(2-)=Cr4H2(SO4)7

: 10034-85-2
hydrogen iodide

: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
In further solvent(s) byproducts: H2S, H2O, I2; boiling with HI soln.;;
In further solvent(s) byproducts: H2S, H2O, I2; boiling with HI soln.;;

: 27303-69-1
tris(η3-allyl)chromium

: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
With I2 In tetrahydrofuran byproducts: C3H5I;	>99

: chromium(II) iodide

: 10034-85-2
hydrogen iodide

: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
In not given byproducts: H2; equilibrium;;
In not given byproducts: H2; equilibrium;;

: 10034-85-2
hydrogen iodide

: 10025-73-7
chromium(III) chloride

: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
In further solvent(s) react. of CrCl3 and concd. HI soln. (D=1.70);; not isolated;;
In further solvent(s) react. of CrCl3 and concd. HI soln. (D=1.70);; not isolated;;

: lead(II) chromate

: 10034-85-2
hydrogen iodide

: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
In water excess HI soln.;;

: 3Li(1+)*Cr(CH3)6(3-)*3(C4H8O2)=Li3Cr(CH3)6*3(C4H8O2)

A: 13569-75-0
chromium(III) iodide

B: lithium iodide * 2 dioxane

Conditions

Conditions	Yield
With iodine byproducts: CH3I; quant.;

: 3Li(1+)*Cr(CH3)6(3-)*3(C4H8O2)=Li3Cr(CH3)6*3(C4H8O2)

A: 13569-75-0
chromium(III) iodide

B: Li(1+)*I3(1-)=LiI3

Conditions

Conditions	Yield
With iodine byproducts: CH3I; quant.;
With iodine byproducts: CH3I; quant.;

: 2Na(1+)*Cr(3+)*5C6H5(1-)*3(C2H5)2O=Na2Cr(C6H5)5*3(C2H5)2O

A: 591-50-4
iodobenzene

B: 92-52-4
biphenyl

C: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
With iodine byproducts: NaI;
With I2 byproducts: NaI;

...Expand

: Li(1+)*{Cr(C6H4OCH3)4}(1-)*(C2H5)2O=Li{Cr(C6H4OCH3)4}*(C2H5)2O

: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
With I2 byproducts: LiI, o-IC6H4OCH3;

: (C6H5)6CrLi3*2.5 diethylether

A: 92-52-4
biphenyl

B: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
With I2 byproducts: C6H5I, LiI;

: Li2Cr2(C6H5)6* 3 diethylether

: 13569-75-0
chromium(III) iodide

Conditions

Conditions	Yield
With I2 byproducts: LiI, NaI, biphenyl;

: chromium(II) iodide

: 13569-75-0
chromium(III) iodide

: 7440-47-3
chromium

Conditions

Conditions	Yield
1000-1400°C, E-3-760 torr;
1000-1400°C, E-3-760 torr;

: 13569-75-0
chromium(III) iodide

: 7440-47-3
chromium

Conditions

Conditions	Yield
heating in air-tight sealed crucible at 800-1000°C;
byproducts: iodine; thermal dissocn. in a sealed, evacuated quartz vessel at 800°C; Cr pptd. to Cr wire streching out between two Ni-electrodes at 1100°C;
With D-Fructose; hydrogen iodide; boric acid In not given Electrolysis; 100 g/l Cr; 25 g/l boric acid; 2.5 g/l HI; 20°C; 5V; interelectrode distance 5 cm; 10 A/dm**2;

: chromium(II) iodide

: 13569-75-0
chromium(III) iodide

: chromium(I) iodide

Conditions

Conditions	Yield
In neat (no solvent) thermal decompn. at 400-700 °C;;
In neat (no solvent) thermal decompn. at 400-700 °C;;

: lithium nitride

: 13569-75-0
chromium(III) iodide

: dichromium nitride

Conditions

Conditions	Yield
In neat (no solvent, solid phase) CrI3 was reacted with Li3N in steel reactor; washed with water, filtered;

: 13569-75-0
chromium(III) iodide

: chromium(II) iodide

Conditions

Conditions	Yield
In neat (no solvent) byproducts: I2; dissociation at 490-664 °C to gaseous I2 and CrI2;;
In neat (no solvent) thermal decompn. at 500 °C under vac.;; sublimation at 700 °C in vac.;;
With H2 In neat (no solvent) redn. in a stream of H2 at 300-350 °C;;

: 13569-75-0
chromium(III) iodide

: 7664-41-7
ammonia

: diiodoethoxotriamminechromium(III)

Conditions

Conditions	Yield
With diethyl ether In diethyl ether passing dry NH3 into a soln. of chromium(III) iodide in ether;;
With ether In diethyl ether passing dry NH3 into a soln. of chromium(III) iodide in ether;;

: 13569-75-0
chromium(III) iodide

: (3-methyl-4.5.6.7-tetrahydro-indenyl)MgBr

: (3-methyl-4.5.6.7-tetrahydro-indenyl)2CrI

Conditions

Conditions	Yield
In diethyl ether
In diethyl ether

: lithium nitride

: 13569-75-0
chromium(III) iodide

: ammonium chloride

A: dichromium nitride

: chromium nitride

Conditions

Conditions	Yield
In neat (no solvent, solid phase) CrI3 was reacted with Li3N and NH4Cl in steel reactor; washed with water, filtered;

...Expand

: 13569-75-0
chromium(III) iodide

: rubidium chloride

: 7440-47-3
chromium

: rubidium iodide

: Rb2CrClI3

Conditions

Conditions	Yield
In neat (no solvent) resublimed Rb-halogenides and CrI3 (from the elements in an evacuated quartz tube at 500°C) are sealed (together with Cr) in an evacuated quartz tube, heating at 600°C for 48 h; filtn. at 600°C through a quartz filter (to remove excess Cr),cooling, grounding to powder, remelting, quenching to room temp., chemical analysis, desired product could not be isolated;	0%

...Expand

: 13569-75-0
chromium(III) iodide

: 146-84-9
silver picrate

: 148940-98-1
chromium(III) picrate

Conditions

Conditions	Yield
In water reaction of CrI3 and Ag picrate in an aq. soln.; recrystn. from methanol, molecular weight detn.;	85-90

: 13569-75-0
chromium(III) iodide

: 81118-79-8
phenyl pyruvic acid thiosemicarbazone

: {Cr(phenylpyruvic acid thiosemicarbazone-H)2}I

Conditions

Conditions	Yield
In ethanol hot ethanolic solns. mixed together, refluxed on a water-bath for about 4 h; cooled, filtered, washed with ethanol, dried (electric oven, 60°C); elem. anal.;

: 13569-75-0
chromium(III) iodide

: 81118-82-3
phenyl pyruvic acid semicarbazone

: {Cr(phenylpyruvic acid semicarbazone-H)2}I

Conditions

Conditions	Yield
In ethanol hot ethanolic solns. mixed together, refluxed on a water-bath for about 4 h; cooled, filtered, washed with ethanol, dried (electric oven, 60°C); elem. anal.;

: 13569-75-0
chromium(III) iodide

: 81118-81-2
(4-methylphenyl)pyruvic acid thiosemicarbazone

: {Cr((4-methylphenyl)pyruvic acid thiosemicarbazone-H)2}I

Conditions

Conditions	Yield
In ethanol hot ethanolic solns. mixed together, refluxed on a water-bath for about 4 h; cooled, filtered, washed with ethanol, dried (electric oven, 60°C); elem. anal.;

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