CAS No.13774-85-1,Xenonfluoride oxide (XeF4O), (SP-5-21)- (9CI) Suppliers

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Shanghai united Scientific Co.,Ltd.

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Synthetic route

: xenon

: 7782-41-4
fluorine

A: 13693-09-9
xenon hexafluoride

: 13774-85-1
xenon oxide tetrafluoride

: 13709-61-0
xenon tetrafluoride

Conditions

Conditions	Yield
With NaF byproducts: CF4; NaF dried at 900°C, filled in HP-autoclave, Xe and F2 condensed at -196°C, mixt. warmed at 250°C for 1 d, excess of F2, XeF4, XeOF4 and CF4 removed in vac., Na2XeF8 (residue) warmed to 50-100°C, XeF6 recovered in vac.;	A 84% B n/a C n/a

...Expand

: 7631-99-4
sodium nitrate

: 13693-09-9
xenon hexafluoride

A: 13875-06-4
xenon dioxide difluoride

: 13774-85-1
xenon oxide tetrafluoride

C: sodium fluoride

Conditions

Conditions	Yield
byproducts: FNO2, Na2XeF8, NaXeF7; N2; mixt. prepd. at -196 °C; warmed to room temp.; then reaction at 70 °C for 10h;; cooled to -196 °C (vacuum); sepn. of volatile compounds on warmup to room temp. by fractional condensation; XeOF4 in -78 °C trap;;	A n/a B 82% C n/a

...Expand

: xenon hexafluoride

: 7732-18-5
water

: 13774-85-1
xenon oxide tetrafluoride

Conditions

Conditions	Yield
byproducts: HF; reactn. of XeF6 with air (satd. with H2O) in a flow apparatus until IR absorption of XeF6 decreases to 2% of the initial value and the total pressure reaches 600 Torr; gas mixt. (contg. XeF6 and XeOF4) is condensed into an U-tube at -78°C;; HF/air mixt. is pumped off at -78°C; warming to 20°C; further addn. of moist air; freezing of XeOF4; HF/air is pumped off;;	80%
In gas Ni vessel, condensation of H2O onto XeF6, storing at 20°C for 0.5 hours, then cooling to -78°C;; main amt. of HF is pumped off;;
byproducts: HF;

: 13693-09-9
xenon hexafluoride

: 7732-18-5
water

: 13774-85-1
xenon oxide tetrafluoride

Conditions

Conditions	Yield
In neat (no solvent) byproducts: HF; H2O condensed in an evacd. Ni vessel above XeF6, warmed to room temp., allowed to stand for 4 h before being agitated (danger of explosion), allowed to remain at room temp. for another 8 h;; vac. disd. into a Kel-F tube contg. NaF; XeOF4 distd. from this storage vesel as required;;
In not given (inert atm.); hydrolysis of xenon compd.; Schumacher G.A., Schrobilgen G.J., Inorg. Chem. 1984, 23, 2923-2929;

: xenon hexafluoride

: calcium oxide

: 13774-85-1
xenon oxide tetrafluoride

Conditions

Conditions	Yield
further products by reactn. of XeOF4 with CaO;;

: xenon

: 80937-33-3
oxygen

: 7782-41-4
fluorine

: 13774-85-1
xenon oxide tetrafluoride

Conditions

Conditions	Yield
thermal synthesis (Xe:F2:O2=1:2:10) at about 600°C;; low yield;;

...Expand

: 13875-06-4
xenon dioxide difluoride

: xenon hexafluoride

: 13774-85-1
xenon oxide tetrafluoride

Conditions

Conditions	Yield
slow react. with liquefaction;;

: xenon hexafluoride

: 112926-00-8, 7631-86-9
silica gel

: 13774-85-1
xenon oxide tetrafluoride

Conditions

Conditions	Yield
react. of XeF6 (about 6g) with wall of quartz vessel in a few days at 50°C;; dry ice /trichloro ethylene bath; SiF4 is pumped off;;
byproducts: SiF4; reaction of XeF6 with quartz or glass;

: 13693-09-9
xenon hexafluoride

: 13536-84-0
uranyl fluoride

A: 7783-81-5
uranium hexafluoride

: 13774-85-1
xenon oxide tetrafluoride

Conditions

Conditions	Yield
25°C;
25°C;

...Expand

: 12191-01-4
caesium fluoride * xenon oxide tetrafluoride

: 13774-85-1
xenon oxide tetrafluoride

Conditions

Conditions	Yield
In neat (no solvent) in vacuum at 20°C, slow loss of XeOF4; in a stream of N2 (1atm), weight loss is observed only above 60°C;;

: xenon hexafluoride

: 13774-85-1
xenon oxide tetrafluoride

Conditions

Conditions	Yield
In neat (no solvent) on heating of XeF6 in a closed quartz vessel during some days at 50°C untill disappearing of pale yellow color of XeF6; 2XeF6 + SiO2 -> 2XeOF4 + SiF4;;
With water byproducts: HF; on hydrolysis with stoechiometric amt. of H2O: XeF6 + H2O -> 2HF + XeOF4;;
With glass

: 13693-09-9
xenon hexafluoride

: 7732-18-5
water

A: 13875-06-4
xenon dioxide difluoride

: 13774-85-1
xenon oxide tetrafluoride

Conditions

Conditions	Yield
In hydrogen fluoride enriched water (26.5% (17)O, 37.0% (18)O); mole ratio XeF6:H2O = 1:1.22;

...Expand

: 13693-09-9
xenon hexafluoride

: 57458-27-2
teflic acid

: 13774-85-1
xenon oxide tetrafluoride

B: F5XeOTeF5

Conditions

Conditions	Yield
In further solvent(s) soln. of educts in freon-114 condensed in NMR tube, melted in vac., warmed to room temp., not sepd., detected by NMR;	A <1 B 0%

...Expand

: F12O8Os2Xe2

: 13774-85-1
xenon oxide tetrafluoride

B: 24762-17-2, 58800-18-3
osmium trioxide difluoride

Conditions

Conditions	Yield
In neat (no solvent, solid phase) (inert atm.); keeping at room temp. for 21 d; Raman spectroscopy;

: 13774-85-1
xenon oxide tetrafluoride

: 40934-88-1
boron tris{pentafluoro-oxotellurate(VI)}

: 68854-32-0
OXe(OTeF5)4

Conditions

Conditions	Yield
In further solvent(s) byproducts: BF3; bor compd. filled in FEP reactor, soln. of XeOF4 in freon-114 (condensed in vac. app.) added, mixt. warmed to -65°C, BF3 removed in vac.for -78 to -25°C; sublimation in vac; elem. anal.;	89%
In trichlorofluoromethane byproducts: BF3; XeOF4 cooled to -196°C, solvent condensed to the vessel, briefly warmed to -80°C, B(OTeF5)3 added (-196°C, drybox), sealed, evacd., warmed to -80°C, pressurized with N2 (1 atm), slowly warmed, agitated (<0°C);; pumping of volatiles at -80°C overnight;;
In further solvent(s) byproducts: BF3; in n-C5F12 at -30°C;

: 13774-85-1
xenon oxide tetrafluoride

: 7732-18-5
water

: 13776-58-4
xenon trioxide

Conditions

Conditions	Yield
byproducts: HF;

: 13774-85-1
xenon oxide tetrafluoride

: 13400-13-0
cesium fluoride

: 12191-01-4
caesium fluoride * xenon oxide tetrafluoride

Conditions

Conditions	Yield
In neat (no solvent) in poly(trichlorofluoro ethylene) vessels; excess XeOF4 is distd. onto CsF (pretreated with F2); 12h at 50°C in closed vessel; subsequent distn. of excess XeOF4;

: 13774-85-1
xenon oxide tetrafluoride

: 13776-58-4
xenon trioxide

A: 13709-36-9
xenon difluoride

B: 13875-06-4
xenon dioxide difluoride

Conditions

Conditions	Yield
In water formation of homogenous liquid on cautious heating of aq. soln. of XeO3 in polytrichloro ethylene vessel (vacuum, dehydration), condensation of XeOF4 on educt during cooling at -78°C, 12h;; fractionating distn. of liquid (which contains XeO2F2, XeOF4 and XeF2), purification of XeO2F2 on mass spectroscopy;;

...Expand

: 13774-85-1
xenon oxide tetrafluoride

A: 13709-36-9
xenon difluoride

B: 13709-61-0
xenon(IV) fluoride

C: 80937-33-3
oxygen

D: 7782-41-4
fluorine

Conditions

Conditions	Yield
400°C;

...Expand

: 13774-85-1
xenon oxide tetrafluoride

: xenon

Conditions

Conditions	Yield
With hydrogen byproducts: H2O, HF;
With hydrogen

: 13774-85-1
xenon oxide tetrafluoride

: 13776-58-4
xenon trioxide

Conditions

Conditions	Yield
With water hydrolysis with different intermediates, finally XeO3 is obtained;;
With H2O hydrolysis with different intermediates, finally XeO3 is obtained;;
With H2O

: 13774-85-1
xenon oxide tetrafluoride

A: 13709-61-0
xenon(IV) fluoride

B: 80937-33-3
oxygen

Conditions

Conditions	Yield
300°C;

: 7631-99-4
sodium nitrate

: 13774-85-1
xenon oxide tetrafluoride

A: 13875-06-4
xenon dioxide difluoride

B: 10022-50-1
nitrylfluoride

C: sodium fluoride

...Expand

: 13774-85-1
xenon oxide tetrafluoride

: 112926-00-8, 7631-86-9
silica gel

: 13776-58-4
xenon trioxide

Conditions

Conditions	Yield
byproducts: SiF4; slow react. with quartz;;
byproducts: SiF4;
byproducts: SiF4; slow react. with quartz;;

: rubidium fluoride

: 13774-85-1
xenon oxide tetrafluoride

: 3 rubidium fluoride * 2 xenon oxide tetrafluoride

Conditions

Conditions	Yield
In neat (no solvent) in poly(trichlorofluoro ethylene) vessels; excess XeOF4 is distd. onto RbF (pretreated with F2); 12h at 50°C in closed vessel; subsequent distn. of excess XeOF4;

: potassium fluoride

: 13774-85-1
xenon oxide tetrafluoride

: 3 potassium fluoride * xenon oxide tetrafluoride

Conditions

Conditions	Yield
In neat (no solvent) in poly(trichlorofluoro ethylene) vessels; excess XeOF4 is distd. onto KF (pretreated with F2); 12h at 50°C in closed vessel; subsequent distn. of excess XeOF4;

: 13774-85-1
xenon oxide tetrafluoride

: 7783-70-2
antimony pentafluoride

: xenon oxide tetrafluoride * 2 SbF5

Conditions

Conditions	Yield
on heating of XeOF4 with SbF5, formation of white ppt.;; on pumping off of excess SbF5 untill constant weight;;

: 7783-72-4, 44247-54-3
vanadium pentafluoride

: 13774-85-1
xenon oxide tetrafluoride

: 2 xenon oxide tetrafluoride * VF5

Conditions

Conditions	Yield
storing XeOF4 with fourfold excess of VF5 at 20°C;; volatile components are pumped off until vapor pressure of remaining liquid is about 30 Torr;
addition of an excess of VF5 to XeoF4; reaction within several days in a Ni tube at 25°C; evaporation at 25°C;;

: 13774-85-1
xenon oxide tetrafluoride

: 40934-88-1
boron tris{pentafluoro-oxotellurate(VI)}

: 68854-32-0
OXe(OTeF5)4

: 91108-43-9
OXeF3(OTeF5)

: 68889-95-2
OXeF2(OTeF5)2

: 68854-35-3
OXeF2(OTeF5)2

: 68854-36-4
OXeF(OTeF5)3

Conditions

Conditions	Yield
In further solvent(s) byproducts: BF3; Bor-compd. filled in NMR-tube, freon-114 and XeOF4 condensed to, mixt. warmed to -40°C, BF3 and teil of solvents removed at -30°C; not sepd.; detected by NMR;

...Expand

: 13774-85-1
xenon oxide tetrafluoride

: 68854-32-0
OXe(OTeF5)4

: 91108-43-9
OXeF3(OTeF5)

: 68889-95-2
OXeF2(OTeF5)2

: 68854-35-3
OXeF2(OTeF5)2

: 68854-36-4
OXeF(OTeF5)3

Conditions

Conditions	Yield
In further solvent(s) OXe(OTeF5)4 filled in NMR tube, XeOF4 and freon 114 condensed to, melted in vac.; not sepd., detected by NMR;

...Expand

: 13774-85-1
xenon oxide tetrafluoride

: 13400-13-0
cesium fluoride

A: 12191-01-4
caesium fluoride * xenon oxide tetrafluoride

: 76077-76-4
Cs(1+)*(XeOF4)3F(1-)=Cs((XeOF4)3F)

Conditions

Conditions	Yield
In neat (no solvent) an excess of XeOF4 was vac. distd. onto CsF (dried at 350°C under vac. for 1.5 d), 2 d; unreacted XeOF4 was removed at 0°C by static distn. into FEP vessel cooled to -196°C for 1 h; for isolation of Cs(XeOF5) an excess of XeOF4 and Cs((XeOF4)3F) was removed by dynamic vac. distn. at room temp. for 1 h;

...Expand

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