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Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi

4,5-Dicyano-1,2-dichlorobenzene

Cas:139152-08-2

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Manufacturers

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

4,5-Dichlorophthalonitrile

Cas:139152-08-2

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Product Name: 4,5-DICHLOROPHTHALONITRILE Synonyms: 4,5-DICHLOROPHTHALONITRILE;1,2-DICHLORO-4,5-DICYANOBENZENE;4,5-Dichlorophthalonitrile 99%;4,5-DICHLOROPHTHALONITRILE 98+%;4,5-Dichloro-1,2-benzenedicarbonitrile;4,5-Dichlorobenzene-1,2

139152-08-2

Cas:139152-08-2

Min.Order:1 Gram

FOB Price: $8900.0

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 139152-08-2 with best quality

Cas:139152-08-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

1,2-Benzenedicarbonitrile,4,5-dichloro- 139152-08-2

Cas:139152-08-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1,2-Benzenedicarbonitrile,4,5-dichloro-

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

4,5-DICHLOROPHTHALONITRILE CAS:139152-08-2

Cas:139152-08-2

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Best Offer4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Trading Company

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Shanghai Minstar Chemical Co., Ltd

4,5-DICHLOROPHTHALONITRILE Chemical Properties Melting point 180-184 °C (lit.) Boiling point 312.4±42.0 °C(Predicted) density 1.48±0.1 g/cm3(Predicted) storage temp. Sealed in dry,Room Temperature InChIKey SRI

4,5-dichlorophthalonitrile

Cas:139152-08-2

Min.Order:1 Gram

FOB Price: $66.0

Type:Lab/Research institutions

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:1 Kilogram

Negotiable

Type:Other

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Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

4,5-Dichlorophthalonitrile cas no. 139152-08-2 98%

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as:

4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:1 Gram

Negotiable

Type:Manufacturers

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GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

4,5-Dichlorophthalonitrile

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

high purity, manufacturer Application:Intermediate

4,5-Dichlorophthalonitrile

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Manufacturers

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Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec 4,5-Dichlorophthalonitrile 5g

Cas:139152-08-2

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

4,5-Dichlorophthalonitrile

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xi`an Eastling Biotech Co., Ltd.

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou

4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

4,5-DICHLOROPHTHALONITRILEAppearance:Off-white powder Storage:Protected from light, stored hermetically and in a dry place Package:Fluoride barrel Application:additives Transportation:By air or courier or sea

4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Ocean Chemical Co., Ltd.

1.High purity, like 99%, 99.9%, 99.95%, 99.99%, 99.999%2.Quality control, test sample before shipping and keep sample for 3 years after shipping;3. Prompt shipment with professional documents;4. Packing as your request, with photo before shipment;5.

4,5-Dichlorophthalonitrile

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran

4,5-Dichlorophthalonitrile

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

HANGZHOU TIANYE CHEMICALS CO., LTD.

"HANGZHOU TIANYE CHEMICALS Co.LTD , Located in Eastern Science and Innovation Park Hangzhou .We are a high-tech enterprise specialized in technical research and development, production, development and trade of chemical products. We supply Multiple s

4,5-Dichlorophthalonitrile

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

DB BIOTECH CO., LTD

best seller Application:API

4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

4,5-DICHLOROPHTHALONITRILEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

4,5-DICHLOROPHTHALONITRILE

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemlyte Solutions

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

4,5-dichlorophthalonitrile

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Other

inquiry

Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

139152-08-2

Cas:139152-08-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

4,5-dichloro-1,2-benzenedicarboxamide
147699-62-5

4,5-dichloro-1,2-benzenedicarboxamide

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

Conditions
ConditionsYield
With trichlorophosphate In pyridine; methanol; water86%
With thionyl chloride; N,N-dimethyl-formamide 1) 0 - 5 deg C, 5 h, 2) r.t., 24 h;75%
With thionyl chloride In N,N-dimethyl-formamide at 0 - 20℃; for 29h;50%
With thionyl chloride In N,N-dimethyl-formamide at 0℃; for 12h; Inert atmosphere;50%
With thionyl chloride In N,N-dimethyl-formamide at 0℃; Inert atmosphere;1.48 g
phosgene
75-44-5

phosgene

4.5-dichloro-phthalic acid diamide

4.5-dichloro-phthalic acid diamide

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

Conditions
ConditionsYield
With N,N-dimethyl-aniline; chlorobenzene
4,5-dichlorophthalic anhydride
942-06-3

4,5-dichlorophthalic anhydride

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 98 percent / formamide / 3 h / Heating
2: 72 percent / 25-33percent NH4OH / 48 h / Ambient temperature
3: 75 percent / SOCl2, DMF / 1) 0 - 5 deg C, 5 h, 2) r.t., 24 h
View Scheme
Multi-step reaction with 3 steps
1: formamide / 3 h / Reflux
2: ammonium hydroxide / 48 h / 20 °C
3: thionyl chloride / N,N-dimethyl-formamide / 29 h / 0 - 20 °C
View Scheme
4,5-dichlorophthalimide
15997-89-4

4,5-dichlorophthalimide

hydrazine hydrate (1 mol)

hydrazine hydrate (1 mol)

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 72 percent / 25-33percent NH4OH / 48 h / Ambient temperature
2: 75 percent / SOCl2, DMF / 1) 0 - 5 deg C, 5 h, 2) r.t., 24 h
View Scheme
4,5-dichlorophthalic acid
56962-08-4

4,5-dichlorophthalic acid

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 93 percent / acetic anhydride / 5 h / Heating
2: 98 percent / formamide / 3 h / Heating
3: 72 percent / 25-33percent NH4OH / 48 h / Ambient temperature
4: 75 percent / SOCl2, DMF / 1) 0 - 5 deg C, 5 h, 2) r.t., 24 h
View Scheme
Multi-step reaction with 4 steps
1: acetic anhydride / 5 h / Reflux
2: formamide / 3 h / Reflux
3: ammonium hydroxide / 48 h / 20 °C
4: thionyl chloride / N,N-dimethyl-formamide / 29 h / 0 - 20 °C
View Scheme
Multi-step reaction with 3 steps
1: formamide / 4 h / 140 - 180 °C
2: ammonium hydroxide / dimethyl sulfoxide / 6 h / 0 - 20 °C
3: thionyl chloride / N,N-dimethyl-formamide / 12 h / 0 °C / Inert atmosphere
View Scheme
Multi-step reaction with 3 steps
1: formamide / 4 h / 140 - 180 °C
2: ammonia / dimethyl sulfoxide / 6 h / 25 °C / Cooling with ice
3: thionyl chloride / N,N-dimethyl-formamide / 0 °C / Inert atmosphere
View Scheme
4,5-dichlorophthalimide
15997-89-4

4,5-dichlorophthalimide

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: ammonium hydroxide / 48 h / 20 °C
2: thionyl chloride / N,N-dimethyl-formamide / 29 h / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: ammonium hydroxide / dimethyl sulfoxide / 6 h / 0 - 20 °C
2: thionyl chloride / N,N-dimethyl-formamide / 12 h / 0 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: ammonia / dimethyl sulfoxide / 6 h / 25 °C / Cooling with ice
2: thionyl chloride / N,N-dimethyl-formamide / 0 °C / Inert atmosphere
View Scheme
1-Adamantanethiol
34301-54-7

1-Adamantanethiol

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

C28H32N2S2
1417158-52-1

C28H32N2S2

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 20h;99%
n-Heptyl Resorcinol
18979-76-5

n-Heptyl Resorcinol

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4,5-bis(3-heptyloxyphenoxy)phthalonitrile

4,5-bis(3-heptyloxyphenoxy)phthalonitrile

Conditions
ConditionsYield
Stage #1: n-Heptyl Resorcinol With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 0.166667h; Inert atmosphere;
Stage #2: 4,5-dichlorophthalonitrile In N,N-dimethyl-formamide at 100℃; for 1.83h; Inert atmosphere;
98.7%
4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4-t-butylbenzenethiol
2396-68-1

4-t-butylbenzenethiol

3,6-bis[(tert-butylphenyl)sulfanyl]phthalonitrile
1130308-49-4

3,6-bis[(tert-butylphenyl)sulfanyl]phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide at 20℃; for 20h;98%
2,3-dihydroxytriptycene
928880-37-9

2,3-dihydroxytriptycene

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4,5-(1,2-dioxytriptycene)phthalonitrile

4,5-(1,2-dioxytriptycene)phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 6h; Inert atmosphere;98%
ethyl-3-hydroxybenzoate
7781-98-8

ethyl-3-hydroxybenzoate

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4,5-bis(3-ethoxycarbonylphenoxy)phthalonitrile

4,5-bis(3-ethoxycarbonylphenoxy)phthalonitrile

Conditions
ConditionsYield
With potassium carbonate97%
4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4-aminotiophenol
1193-02-8

4-aminotiophenol

4,5-bis((4-aminophenyl)thio)phthalonitrile

4,5-bis((4-aminophenyl)thio)phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 40℃; for 12h; Inert atmosphere;97%
5-Hydroxy-2-methylpyridine
1121-78-4

5-Hydroxy-2-methylpyridine

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4,5-bis(4′-methylpyridin-3′-yloxy)phthalonitrile

4,5-bis(4′-methylpyridin-3′-yloxy)phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 3h; Inert atmosphere;97%
3-(9H-carbazol-9-yl)phenylboronic acid
864377-33-3

3-(9H-carbazol-9-yl)phenylboronic acid

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

3,3’’-di(9H-carbazol-9-yl)-[1,1’:2′ ,1’’-terphenyl]-4′,5′-dicarbonitrile

3,3’’-di(9H-carbazol-9-yl)-[1,1’:2′ ,1’’-terphenyl]-4′,5′-dicarbonitrile

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water for 12h; Reflux; Inert atmosphere;97%
4-tritylphenol
978-86-9

4-tritylphenol

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

bis{4,5-[4-(triphenylmethyl)phenoxy]}-1,2-dicyanobenzene
356098-74-3

bis{4,5-[4-(triphenylmethyl)phenoxy]}-1,2-dicyanobenzene

Conditions
ConditionsYield
Stage #1: 4-tritylphenol With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 0.166667h; Inert atmosphere;
Stage #2: 4,5-dichlorophthalonitrile In N,N-dimethyl-formamide at 120℃; for 2h; Inert atmosphere;
96%
2-aminopyridine
504-29-0

2-aminopyridine

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

1,3-bis(2-pyridylimino)-5,6-dichloroisoindole
1386999-76-3

1,3-bis(2-pyridylimino)-5,6-dichloroisoindole

Conditions
ConditionsYield
With calcium chloride In butan-1-ol for 48h; Reflux; Inert atmosphere;96%
4-mercaptobenzoic acid
1074-36-8

4-mercaptobenzoic acid

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4,4′-((4,5-dicyano-1,2-phenylene)bis(sulfanediyl))dibenzoic acid

4,4′-((4,5-dicyano-1,2-phenylene)bis(sulfanediyl))dibenzoic acid

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 24h; Inert atmosphere;96%
4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

3-(n-octyloxy)thiophenol
162557-60-0

3-(n-octyloxy)thiophenol

4,5-bis((3-(octyloxy)phenyl)thio)phthalonitrile

4,5-bis((3-(octyloxy)phenyl)thio)phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 7h; Inert atmosphere;95.1%
(4-hydroxyphenyl)methanol
623-05-2

(4-hydroxyphenyl)methanol

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4-chloro-5-[4-(hydroxymethyl)phenoxy]phthalonitrile
649553-05-9

4-chloro-5-[4-(hydroxymethyl)phenoxy]phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In acetone for 24h; Heating;95%
4-sulfanylphenol
637-89-8

4-sulfanylphenol

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4,5-bis((4-hydroxyphenyl)thio)phthalonitrile
1210049-82-3

4,5-bis((4-hydroxyphenyl)thio)phthalonitrile

Conditions
ConditionsYield
Stage #1: 4-sulfanylphenol With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 0.5h; Inert atmosphere;
Stage #2: 4,5-dichlorophthalonitrile In N,N-dimethyl-formamide for 24h; Inert atmosphere;
95%
Stage #1: 4-sulfanylphenol With potassium carbonate In dimethyl sulfoxide at 20℃; for 0.5h; Inert atmosphere;
Stage #2: 4,5-dichlorophthalonitrile In dimethyl sulfoxide at 90℃; for 12h; Inert atmosphere;
91%
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 24h; Inert atmosphere;75%
4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

Quinoline-2-thiol
2637-37-8

Quinoline-2-thiol

4,5-[2-mercaptoquinoline]phthalonitrile

4,5-[2-mercaptoquinoline]phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2.5h; Inert atmosphere;95%
1-methyl-2-(1-thiohex-6-yl)-1,2-closo-dodecaborane

1-methyl-2-(1-thiohex-6-yl)-1,2-closo-dodecaborane

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

C26H52B20N2S2

C26H52B20N2S2

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide at 45℃; for 4h;95%
4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

triethyl phosphite
122-52-1

triethyl phosphite

tetraethyl (4,5-dicyano-1,2-phenylene)bisphosphonate

tetraethyl (4,5-dicyano-1,2-phenylene)bisphosphonate

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0) at 230℃; under 5171.62 Torr; for 0.75h; Microwave irradiation;95%
1-(3-mercapto)propyl-3,5,7,9,11,13,15-isobutylpentacyclo[9.5.1.13,9.15,15.17,13]octasiloxane
480438-85-5

1-(3-mercapto)propyl-3,5,7,9,11,13,15-isobutylpentacyclo[9.5.1.13,9.15,15.17,13]octasiloxane

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4,5-bis(mercaptopropylisobutyl-POSS)phthalonitrile
1035113-11-1

4,5-bis(mercaptopropylisobutyl-POSS)phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In tetrahydrofuran for 48h; Heating;94%
4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4-methoxy-phenol
150-76-5

4-methoxy-phenol

4,5-bis(4-methoxyphenoxy)phthalonitrile
147699-64-7

4,5-bis(4-methoxyphenoxy)phthalonitrile

Conditions
ConditionsYield
Stage #1: 4-methoxy-phenol With potassium carbonate In N,N-dimethyl acetamide at 110℃; for 0.25h; Inert atmosphere;
Stage #2: 4,5-dichlorophthalonitrile In N,N-dimethyl acetamide at 110℃; for 3h; Inert atmosphere;
93.4%
With potassium carbonate In dimethyl sulfoxide at 90℃; for 0.5h;72%
1-butanethiol
109-79-5

1-butanethiol

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

1,2-dibutylthio-4,5-dicyanobenzene
165284-85-5

1,2-dibutylthio-4,5-dicyanobenzene

Conditions
ConditionsYield
With copper(I) oxide; sodium hydride In N,N-dimethyl-formamide for 3h; Condensation; Heating;93%
With N,N-dimethyl acetamide; potassium carbonate at 90℃; for 8h; Inert atmosphere;72%
With potassium carbonate In N,N-dimethyl acetamide at 90℃; for 12h; Inert atmosphere;
15-thiol-13,17-dioxa nonacosane
309275-22-7

15-thiol-13,17-dioxa nonacosane

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

1,2-di(13,17-dioxa nonacosane-15-sulfanyl) phthalonitrile
309275-24-9

1,2-di(13,17-dioxa nonacosane-15-sulfanyl) phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide at 50℃; for 48h;93%
morpholine
110-91-8

morpholine

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4-chloro-5-morpholinophthalonitrile
309735-19-1

4-chloro-5-morpholinophthalonitrile

Conditions
ConditionsYield
at 20℃; for 24h; Inert atmosphere;93%
4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

3-Dimethylaminophenol
99-07-0

3-Dimethylaminophenol

4,5-bis[3-(dimethylamino)phenoxy]phthalonitrile

4,5-bis[3-(dimethylamino)phenoxy]phthalonitrile

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 18h; Inert atmosphere;93%
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 18h;93%
4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

2-methoxy-phenol
90-05-1

2-methoxy-phenol

4,5-bis(2-methoxyphenoxy)phthalonitrile

4,5-bis(2-methoxyphenoxy)phthalonitrile

Conditions
ConditionsYield
Stage #1: 2-methoxy-phenol With potassium carbonate In N,N-dimethyl acetamide at 110℃; for 0.25h; Inert atmosphere;
Stage #2: 4,5-dichlorophthalonitrile In N,N-dimethyl acetamide at 110℃; for 3h; Inert atmosphere;
92.8%
5-chloro-2-pyridylamine
1072-98-6

5-chloro-2-pyridylamine

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

C18H9Cl4N5
1109281-07-3

C18H9Cl4N5

Conditions
ConditionsYield
With calcium chloride In hexan-1-ol for 18h; Reflux; Inert atmosphere;92%
4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

phenylboronic acid
98-80-6

phenylboronic acid

1,2-dicyano-4,5-diphenylbenzene
36360-44-8

1,2-dicyano-4,5-diphenylbenzene

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; sodium bromide In 1,4-dioxane; water for 6h; Suzuki-Miyaura cross coupling; Inert atmosphere; Heating;92%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; sodium bromide In 1,4-dioxane; water for 5.5h; Inert atmosphere; Heating;75%
caffeic acid
331-39-5

caffeic acid

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

C17H8N2O4
1446888-26-1

C17H8N2O4

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide at 20℃; for 48h; Inert atmosphere;92%
3,5-Di-tert-butylphenol
1138-52-9

3,5-Di-tert-butylphenol

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

4,5-bis(3,5-di-tert-butylphenoxy)-1,2-dicyanobenzene
405066-84-4

4,5-bis(3,5-di-tert-butylphenoxy)-1,2-dicyanobenzene

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide at 90℃; for 0.5h;91%
With potassium carbonate In dimethyl sulfoxide at 90℃; Inert atmosphere;90%
4-tert-Butylcatechol
98-29-3

4-tert-Butylcatechol

4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

7-tert-butyldibenzo [b,e] [1,4] dioxine-2,3-dicarbonitrile

7-tert-butyldibenzo [b,e] [1,4] dioxine-2,3-dicarbonitrile

Conditions
ConditionsYield
Stage #1: 4-tert-Butylcatechol; 4,5-dichlorophthalonitrile With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2h; Inert atmosphere;
Stage #2: In N,N-dimethyl-formamide at 80℃; for 24h; Inert atmosphere;
91%
4,5-dichlorophthalonitrile
139152-08-2

4,5-dichlorophthalonitrile

thiophenol
108-98-5

thiophenol

4,5-bis(phenylthio)-1,2-dicyanobenzene
147699-67-0

4,5-bis(phenylthio)-1,2-dicyanobenzene

Conditions
ConditionsYield
With potassium carbonate In acetone at 20℃; for 15h;90%
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 12h; Inert atmosphere;82%
With potassium carbonate In dimethyl sulfoxide for 12h; Inert atmosphere;75%
With potassium carbonate In dimethyl sulfoxide at 90℃; for 0.5h;51%
With potassium carbonate In dimethyl sulfoxide at 90℃; for 0.5h;46%

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