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Cas:1074-36-8
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Cas:1074-36-8
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Cas:1074-36-8
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
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Cas:1074-36-8
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Type:Trading Company
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Type:Lab/Research institutions
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inquiryAppearance:White to Yellow to Green powder Storage:room temperature Package:25kg/drum Application:chemicals Transportation:Express/Sea/Air Port:any port in china
Cas:1074-36-8
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:1074-36-8
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry4-Mercaptobenzoic acid CAS:1074-36-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
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Min.Order:1 Gram
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Type:Lab/Research institutions
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Cas:1074-36-8
Min.Order:10 Kilogram
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Cas:1074-36-8
Min.Order:1 Gram
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Type:Trading Company
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Cas:1074-36-8
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Type:Lab/Research institutions
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Cas:1074-36-8
Min.Order:1 Gram
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Type:Lab/Research institutions
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Cas:1074-36-8
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryProduct name: 4-Mercaptobenzoic Acid CAS No.:1074-36-8 Molecule Formula:C7H6O2S Molecule Weight:154.18 Purity: 99% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:1074-36-8
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Min.Order:1 Kilogram
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Type:Trading Company
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Cas:1074-36-8
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Cas:1074-36-8
Min.Order:1 Metric Ton
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Type:Trading Company
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Type:Trading Company
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:1074-36-8
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Type:Lab/Research institutions
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Conditions | Yield |
---|---|
With sodiumsulfide nonahydrate; copper; ethane-1,2-dithiol In dimethyl sulfoxide at 90℃; for 12h; Inert atmosphere; Sealed tube; | 99% |
With sodiumsulfide nonahydrate; copper; ethane-1,2-dithiol In dimethyl sulfoxide at 100℃; for 20h; Inert atmosphere; Green chemistry; | 99% |
With copper(ll) sulfate pentahydrate; ethane-1,2-dithiol; potassium hydroxide In water; dimethyl sulfoxide at 90℃; for 20h; Inert atmosphere; | 94% |
With copper(l) iodide; thiourea; L-proline; sodium t-butanolate In dimethyl sulfoxide at 90℃; for 24h; Inert atmosphere; | 90% |
Stage #1: 4-iodobenzoic acid With copper(l) iodide; potassium carbonate; sulfur In N,N-dimethyl-formamide at 90℃; for 16h; Inert atmosphere; Stage #2: With sodium tetrahydroborate In N,N-dimethyl-formamide at 40℃; Inert atmosphere; Cooling with ice; | 87% |
S-(4-carbomethoxyphenyl) N,N-dimethylthiocarbamate
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water for 3h; Heating; | 97% |
With potassium hydroxide In methanol; water | 2.7 g |
With potassium hydroxide In methanol |
S-acetyl-4-mercaptobenzoic acid
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
With sodium thiomethoxide In methanol at 23℃; for 0.5h; | 94% |
4-mercaptobenzyl alcohol
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
With diethylene glycol dimethyl ether at 70℃; for 0.5h; Sonication; | 94% |
With oxygen at 120℃; for 16h; Green chemistry; | 84% |
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; ethane-1,2-dithiol; potassium hydroxide In water; dimethyl sulfoxide at 110℃; for 20h; Inert atmosphere; | 91% |
Multi-step reaction with 2 steps 1: copper(l) iodide; tetra(n-butyl)ammonium hydroxide; sulfur / water / 48 h / 80 °C / Inert atmosphere; Sealed tube 2: hydrogenchloride; zinc / water / Inert atmosphere; Cooling with ice View Scheme |
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
With potassium hydroxide In methanol at 20℃; for 18h; | 78% |
dimethyl 4,4'-dithiobisbenzoate
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
With acetic acid; zinc for 4h; Heating; | 42% |
Conditions | Yield |
---|---|
With acetic acid; zinc for 4h; Heating; | 38% |
With triphenylphosphine In 1,4-dioxane; water at 30℃; Rate constant; | |
With sodium carbonate; aluminium |
p-carboxyphenylsulfonyl chloride
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
With acetic acid; zinc at 90 - 100℃; | |
With acetic acid; zinc |
potassium ethyl xanthogenate
4-amino-benzoic acid
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water; sodium nitrite Erwaermen des Reaktionsprodukts mit aethanol. Kalilauge; | |
With hydrogenchloride; sodium hydroxide; sodium nitrite In water; acetic acid |
Conditions | Yield |
---|---|
With n-butyllithium; diethyl ether anschliessendes Behandeln mit Kohlendioxid; |
4-amino-benzoic acid
A
4,4'-Dithiobisbenzoic acid
B
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
With hydrogenchloride; potassium ethyl xanthogenate; sodium nitrite Yield given. Multistep reaction. Yields of byproduct given; |
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
With buffer (pH=11) at 20℃; | |
With buffer (pH=11) at 20℃; Rate constant; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; sulfur 1.) 340 deg C, NaOH-KOH melt, 3 min.; 2.) water; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; sulfur 1.) 360 deg C, NaOH-KOH melt, 3 min.; 2.) water; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
(i) aq. HCl, NaNO2, (ii) potassium ethyl xanthate, (iii) KOH, EtOH; Multistep reaction; |
hydrogenchloride
p-carboxyphenylsulfonyl chloride
acetic acid
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
In [D3]acetonitrile; water-d2 Equilibrium constant; |
A
4-mercaptobenzoic acid
B
(E)-2-cyano-3-phenylacrylamide
Conditions | Yield |
---|---|
In [D3]acetonitrile; water-d2 Equilibrium constant; |
A
4-mercaptobenzoic acid
B
(E)-3-(2-chlorophenyl)-2-cyanoacrylamide
Conditions | Yield |
---|---|
In [D3]acetonitrile; water-d2 Equilibrium constant; |
4-mercaptobenzaldehyde
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
With potassium permanganate In water; acetonitrile |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. phosphate buffer; dimethyl sulfoxide / 0.5 h 2: pH 7.4 View Scheme |
Conditions | Yield |
---|---|
pH=7.4; chemoselective reaction; |
Conditions | Yield |
---|---|
With GLUTATHIONE pH=7.4; |
4-mercaptobenzoic acid
2,4-Diamino-5-ethylpyrrolo<2,3-d>pyrimidine
4-[(2,4-diamino-5-ethyl-7H-pyrrolo[2,3-d]pyrimidin-6-yl)sulfanyl]benzoic acid
Conditions | Yield |
---|---|
With iodine In ethanol; water Heating; | 100% |
Conditions | Yield |
---|---|
Stage #1: 4-mercaptobenzoic acid With dihydrogen peroxide; triethylamine In methanol; water at 5 - 25℃; for 0.666667h; Stage #2: With hydrogenchloride In methanol; water at 5 - 25℃; for 1h; | 99.5% |
With iodine; triethylamine In ethanol for 16h; | 98% |
With manganese(II)carbonate; 3,4,5-trihydroxybenzoic acid; oxygen; sodium carbonate In water at 80℃; under 2250.23 Torr; for 4h; pH=9; Schlenk technique; Green chemistry; | 98% |
Conditions | Yield |
---|---|
With dihydrogen peroxide; triethylamine In methanol; water at 25℃; for 0.5h; | 99.5% |
2-chloro-1-[(2-iodophenyl)methyl]-1H-benzo[d]imidazole
4-mercaptobenzoic acid
4-({1-[(2-iodophenyl)methyl]-1H-benzo[d]imidazol-2-yl}sulfanyl)benzene-1-carboxylic acid
Conditions | Yield |
---|---|
With potassium tert-butylate In ethanol Heating; | 99% |
cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate
4-mercaptobenzoic acid
4-{[trans-3-(piperidin-1-yl)cyclobutyl]sulfanyl}benzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-mercaptobenzoic acid With sodium thiosulfate In N,N-dimethyl-formamide for 1h; Molecular sieve; Stage #2: cis-3-(piperidin-1-yl)cyclobutyl 4-bromobenzenesulfonate With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20 - 50℃; for 14h; | 99% |
4-mercaptobenzoic acid
2,5-dibromobenzene-1,4-dinitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 24h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 24h; Inert atmosphere; | 99% |
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 48h; Inert atmosphere; | 35% |
4-mercaptobenzoic acid
acetic anhydride
S-acetyl-4-mercaptobenzoic acid
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; for 6h; Inert atmosphere; | 98% |
With pyridine | 88% |
With potassium hydroxide; acetic acid | 79% |
In pyridine at 0 - 20℃; |
3,4-epoxyheptan-2-one
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
sodium hydroxide In water at 30℃; for 1h; pH=6.0; | 98% |
1-[2-(2-bromophenyl)ethyl]-2-chloro-1H-benzo[d]imidazole
4-mercaptobenzoic acid
4-{1-[2-(2-bromo-phenyl)-ethyl]-1H-benzoimidazol-2-ylsulfanyl}-benzoic acid
Conditions | Yield |
---|---|
With potassium tert-butylate In ethanol Heating; | 98% |
2-chloro-1-[(4-phenylselanyl)butyl]-1H-benzo[d]imidazole
4-mercaptobenzoic acid
4-({1-[(4-phenylselanyl)butyl]-1H-benzo[d]imidazol-2-yl}sulfanyl)benzoic acid
Conditions | Yield |
---|---|
98% |
2-chloro-1-[(5-phenylselanyl)pentyl]-1H-benzo[d]imidazole
4-mercaptobenzoic acid
4-({1-[(5-phenylselanyl)pentyl]-1H-benzo[d]imidazol-2-yl}sulfanyl)benzoic acid
Conditions | Yield |
---|---|
98% |
Conditions | Yield |
---|---|
With sulfuric acid Reflux; | 97.7% |
With sulfuric acid at 90℃; for 24h; | 95% |
With sulfuric acid for 15h; Reflux; | 90% |
4-mercaptobenzoic acid
4-mercaptobenzyl alcohol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 6h; Inert atmosphere; | 97% |
With lithium aluminium tetrahydride In tetrahydrofuran for 16.5h; Inert atmosphere; Reflux; | 93% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 16h; Inert atmosphere; | 82% |
4-mercaptobenzoic acid
2-bromoethanol
4-((2-hydroxyethyl)thio)benzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-mercaptobenzoic acid With sodium hydroxide at 80℃; for 0.75h; Stage #2: 2-bromoethanol for 2h; Stage #3: With hydrogenchloride In water | 97% |
With triethylamine In sodium hydroxide; dichloromethane | 34.21 g (56.7%) |
Conditions | Yield |
---|---|
With thionyl chloride at 80℃; for 168h; | 97% |
2,3-epoxy-2-methyl-2,3-dihydro-1,4-naphthoquinone
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
sodium hydroxide In water at 30℃; for 4h; | 96% |
4-mercaptobenzoic acid
tetrakis(pentafluorophenyl)porphyrin
Conditions | Yield |
---|---|
Stage #1: 4-mercaptobenzoic acid With pyridine In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: tetrakis(pentafluorophenyl)porphyrin In N,N-dimethyl-formamide for 48h; | 96% |
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 1h; | 80% |
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-mercaptobenzoic acid With potassium hydroxide In ethanol; water at 20℃; for 0.333333h; Stage #2: chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I) In ethanol; water at 20℃; for 5h; | 96% |
With sodium methylate In methanol; dichloromethane for 2h; | 84% |
4-mercaptobenzoic acid
4,5-dichlorophthalonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 24h; Inert atmosphere; | 96% |
di-tert-butyl dicarbonate
4-mercaptobenzoic acid
4-{[(tertbutoxy)carbonyl]sulfanyl}benzoic acid
Conditions | Yield |
---|---|
With dmap; triethylamine In tetrahydrofuran at 20℃; for 3h; | 95% |
With dmap; triethylamine In tetrahydrofuran at 20℃; | 82% |
7-oxabicyclo[4.1.0]heptan-2-one
4-mercaptobenzoic acid
2-(4-carboxyphenylthio)cyclohex-2-en-1-one
Conditions | Yield |
---|---|
sodium hydroxide In water at 30℃; for 1h; pH=6.0; | 95% |
Conditions | Yield |
---|---|
With cetyltrimethylammonium hydroxide In water at 30℃; for 12h; | 95% |
4-mercaptobenzoic acid
2,4-Diamino-5-methylpyrrolo<2,3-d>pyrimidine
4-(2,4-diamino-5-methylpyrrolo[2,3-d]pyrimidin-6-ylthio)benzoic acid
Conditions | Yield |
---|---|
With water; iodine In ethanol for 2h; Heating; | 95% |
Stage #1: 4-mercaptobenzoic acid; 2,4-Diamino-5-methylpyrrolo<2,3-d>pyrimidine In ethanol; water for 0.0833333h; Reflux; Stage #2: With iodine In ethanol; water for 3h; Reflux; |
chloro-η(3)-(bis(diphenylphosphinoethyl)phenylphosphine)rhodium(I)
4-mercaptobenzoic acid
(4-carboxybenzenethiolato)(bis(diphenylphosphanylethyl)phenylphosphane)rhodium(I)
Conditions | Yield |
---|---|
With N(CH2CH2CH2CH3)3 In tetrahydrofuran byproducts: (NH(CH2CH2CH2CH3)3)Cl; (N2); a soln. of ligand added over 30 min to a soln. of Rh complex and N(C4H9)3 at room temp., stirred overnight; evapd. (vac.), washed (toluene and n-hexane), dissolved in THF, pptd. (n-hexane), dried (vac.); elem. anal.; | 95% |
4-mercaptobenzoic acid
4,4'-Dimethoxybenzhydrol
4-[bis(4-methoxyphenyl)methylthio]benzoic acid
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0) In water at 80℃; for 1h; Sealed tube; | 95% |
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 12h; Williamson Ether Synthesis; Reflux; | 95% |
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 12h; Williamson Ether Synthesis; Reflux; | 95% |
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