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Cas:15028-39-4
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inquiryAbout Product Technical Details H-PHG-OME HCL Chemical Properties Melting point 200 °C (dec.)(lit.) storage temp. Inert atmos
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
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inquiryH-PHG-OME HCL CAS:15028-39-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediat
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct Name: H-PHG-OME HCL Synonyms: L-PHENYLGLYCINE METHYL ESTER HYDROCHLORIDE;L-PHENYLGLYCINE METHYL ESTER HCL;L-PHENYLGLYCINE METHYL ESTER HYDROCHLORIDE SALT;H-(PH)GLY-OME HCL;H-PHG-OME HCL;(S)-(+)-2-PHENYLGLYCINE METHYL ESTER HYDROCHLORIDE;P
Cas:15028-39-4
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:15028-39-4
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inquiryProduct name: L-Phenylglycine Methyl Ester Hydrochloride CAS No.: 15028-39-4 Molecule Formula:C9H12ClNO2 Molecule Weight:201.65 Purity: 99.0% Package: 25kg/drum Description:White to off-white crystalline powder Manufacture Standards:E
Cas:15028-39-4
Min.Order:1 Kilogram
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:15028-39-4
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:15028-39-4
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inquiryWuhu Nuovo Chemical Technology Co., Ltd. was established in August 2014, mainly engaged in the development, production and sales of ionic liquids, ribose, nucleosides, nucleotides and related chemicals; Products are mainly used in new energy, new ma
Cas:15028-39-4
Min.Order:100 Gram
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Cas:15028-39-4
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiry1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification
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inquiryHigh purity, high success rate, short cycle and moderate priceAppearance:White powder solid Storage:Negative 20 degrees Celsius Package:5mg, 10mg 100mg, 1gram Application:Applied to various scientific research
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inquiryISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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inquiry(S)-methyl 2-((S)-1-phenylethylamino)-2-phenylacetate
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; palladium dihydroxide In methanol under 760.051 Torr; for 15h; | 100% |
With hydrogenchloride; palladium hydroxide on carbon; hydrogen In methanol; water under 760.051 Torr; for 15h; optical yield given as %ee; | 100% |
methanol
(S)-2-phenylglycine
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With thionyl chloride for 10h; Ambient temperature; | 99% |
With thionyl chloride for 8h; Heating; | 97% |
With thionyl chloride In methanol at 20℃; Cooling with ice; | 97% |
(S)-2-phenylglycine
2,2-dimethoxy-propane
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In water at 20℃; | 99% |
With hydrogenchloride at 20℃; for 18h; | 94% |
N-tert-butoxycarbonyl-L-phenylglycine methyl ester
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In dichloromethane; ethyl acetate at 20℃; for 0.833333h; Inert atmosphere; | 97% |
methanol
(S)-α-phenylglycinenitrile
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride | 88% |
With hydrogenchloride; water | 88% |
methanol
(R)-phenylglycine
A
L-2-phenylglycine methyl ester hydrochloride
B
D-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With thionyl chloride for 20h; Ambient temperature; | A n/a B 76% |
N-phthaloylglycine chloride
N-benzyliden-α-phenyl-glycine methyl ester
C
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In toluene at 20℃; Staudinger Ketene Cycloaddition; Reflux; Inert atmosphere; | A 11% B 4% C 29% |
(R)-methyl mandelate
A
L-2-phenylglycine methyl ester hydrochloride
B
D-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
e.e. = 76percent; Multistep reaction. Title compound not separated from byproducts; |
N-benzyliden-α-phenyl-glycine methyl ester
A
L-2-phenylglycine methyl ester hydrochloride
B
D-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Product distribution; multistep reaction; deracemisation was investigated by means of dipivaloyltartaric acids of different chirality in the presence of chiral amines of structure Ph-CHCH3-NHR; other temperature, acid, base; | |
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
N-benzylidenephenylglycine methyl ester
A
L-2-phenylglycine methyl ester hydrochloride
B
D-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With (-)-O,O′-di-pivaloyl-L-tartaric acid; lithium (R)-N-methyl-N-α-methylbenzyl amide Product distribution; other lithium amides and diacyltartaric acides; | |
With (R)-PhCH(CH3)NLiCH2CH3; (3R) HOOCCH(OCOtC4H9)CH(OCOtC4H9)COOH 1.) THF, - 50 deg C; 2.) THF, -70 deg C; Yield given. Multistep reaction. Yields of byproduct given; |
methyl N-4'-methoxybenzylidenephenylglycinate
A
L-2-phenylglycine methyl ester hydrochloride
B
D-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With (-)-O,O′-di-pivaloyl-L-tartaric acid; lithium diisopropyl amide In tetrahydrofuran; diethyl ether at -105℃; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
N-<(R)-2-hydroxy-1-phenylethyl>-(S)-2-aminobenzeneacetic acid methyl ester
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With lead(IV) acetate; hydrogenchloride 1.) CH2Cl2, MeOH, 0 deg C; Yield given. Multistep reaction; |
N-paradimethylaminobenzylidene phenylglycinate de methyle
A
L-2-phenylglycine methyl ester hydrochloride
B
D-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
(R) N-benzylidene phenylglycinate de methyle
A
L-2-phenylglycine methyl ester hydrochloride
B
D-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; |
benzaldehyde
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: Na2SO4 / methanol / 24 h / 20 °C 2: LiClO4 / acetonitrile / 20 °C 3: 91 percent / ceric ammonium nitrate / acetonitrile; H2O / 4 h / 20 °C 4: 88 percent / HCl View Scheme |
[(S)-1-(4-Methoxy-phenyl)-ethyl]-[1-phenyl-meth-(E)-ylidene]-amine
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: LiClO4 / acetonitrile / 20 °C 2: 91 percent / ceric ammonium nitrate / acetonitrile; H2O / 4 h / 20 °C 3: 88 percent / HCl View Scheme |
(S)-[(S)-1-(4-Methoxy-phenyl)-ethylamino]-phenyl-acetonitrile
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 91 percent / ceric ammonium nitrate / acetonitrile; H2O / 4 h / 20 °C 2: 88 percent / HCl View Scheme |
DL-2-phenylglycine methyl ester hydrochloride
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) Et3N 2.) 3 Angstroem molecular sieves / 1.) Et2O, room temp., 1 h 2.) Et2O, room temp., 48 h View Scheme |
phenylglycin
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 95 percent / SOCl2 / 2 h at 45 deg C, 2 h at room temp. 2: 1.) Et3N 2.) 3 Angstroem molecular sieves / 1.) Et2O, room temp., 1 h 2.) Et2O, room temp., 48 h View Scheme |
benzaldehyde
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: CHCl3 / 1 h / Ambient temperature; other aldehydes 2: methanol / 8 h / Ambient temperature 3: HCl / methanol / 5 h / Ambient temperature 4: 1.) Pb(OAc)4, 2.) dil. HCl / 1.) CH2Cl2, MeOH, 0 deg C View Scheme |
β-[(phenylmethylene)amino]-[R-(E)-]-benzeneethanol
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: methanol / 8 h / Ambient temperature 2: HCl / methanol / 5 h / Ambient temperature 3: 1.) Pb(OAc)4, 2.) dil. HCl / 1.) CH2Cl2, MeOH, 0 deg C View Scheme |
N-<(R)-2-hydroxy-1-phenylethyl>-(S)-α-aminobenzeneacetonitrile
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: HCl / methanol / 5 h / Ambient temperature 2: 1.) Pb(OAc)4, 2.) dil. HCl / 1.) CH2Cl2, MeOH, 0 deg C View Scheme |
DL-2-phenylglycine methyl ester hydrochloride
A
L-2-phenylglycine methyl ester hydrochloride
B
D-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With sodium hexaflorophosphate; 1,3,5-Tris{[(S,S)-4,5-diphenyl-2-oxazolinyl]methyl}-2,4,6-triethylbenzene In water-d2; chloroform-d1 at 25℃; Resolution of racemate; optical yield given as %ee; | |
With chiral stationary phase including (R)-naphthylethyl-carbamate-functionalized CF6 In ethanol; n-heptane; trifluoroacetic acid at 20℃; Purification / work up; |
[(S)-1-(4-Methoxy-phenyl)-ethyl]-[1-phenyl-meth-(E)-ylidene]-amine
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: lithium perchlorate / acetonitrile / 20 °C 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C / aq. phosphate buffer 3: hydrogenchloride; water View Scheme |
(S)-methyl 2-(benzyloxycarbonylamino)-2-phenylacetate
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen; acetic acid In water |
methanol
(2S)-2-amino-3-(3-nitrophenyl)propanoic acid
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With thionyl chloride at 20℃; Cooling with ice; |
methanol
(2S)-2-[(tert-butoxycarbonyl)amino]-2-phenylethanoic acid
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With thionyl chloride at 0 - 23℃; Inert atmosphere; |
2,2-dimethyl-4-pentenal
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Stage #1: L-2-phenylglycine methyl ester hydrochloride With triethylamine In dichloromethane at 20℃; for 1h; Stage #2: 2,2-dimethyl-4-pentenal With magnesium sulfate In dichloromethane Further stages.; | 100% |
L-2-phenylglycine methyl ester hydrochloride
(4R,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolane-4-carbaldehyde
Conditions | Yield |
---|---|
Stage #1: L-2-phenylglycine methyl ester hydrochloride With triethylamine In dichloromethane at 20℃; for 1h; Stage #2: (4R,5R)-2,2-dimethyl-5-vinyl-[1,3]dioxolane-4-carbaldehyde With magnesium sulfate In dichloromethane Further stages.; | 100% |
L-2-phenylglycine methyl ester hydrochloride
trifluoroacetic anhydride
(S)-(+)-2-phenyl-N-(trifluoroacetyl)glycine methyl ester
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at -78 - 20℃; for 16h; | 100% |
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In 1,2-dichloro-ethane at 0 - 20℃; for 1.16667h; | 100% |
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane | 100% |
di-tert-butyl dicarbonate
L-2-phenylglycine methyl ester hydrochloride
N-tert-butoxycarbonyl-L-phenylglycine methyl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 38h; | 99% |
Stage #1: L-2-phenylglycine methyl ester hydrochloride With potassium carbonate In water for 1h; Stage #2: di-tert-butyl dicarbonate With guanidine hydrochloride In ethanol at 35 - 40℃; for 0.25h; | 91% |
Stage #1: L-2-phenylglycine methyl ester hydrochloride With triethylamine In tetrahydrofuran for 0.333333h; Cooling; Stage #2: di-tert-butyl dicarbonate In tetrahydrofuran at 20℃; for 24h; | 90% |
In 1,4-dioxane for 18h; Ambient temperature; Yield given; | |
With triethylamine In methanol at 0 - 18℃; for 2h; |
pyridine-3-carbonyl chloride hydrochloride
L-2-phenylglycine methyl ester hydrochloride
N-nicotinylphenylglycine methyl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; | 99% |
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
With 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol In N,N-dimethyl-formamide at 0 - 20℃; for 3h; | 99% |
L-2-phenylglycine methyl ester hydrochloride
methylamine
(S)-2-amino-N-methyl-2-phenylacetamide
Conditions | Yield |
---|---|
In water at 10 - 20℃; for 75h; | 98% |
oxalyl dichloride
L-2-phenylglycine methyl ester hydrochloride
(S)-[((S)-Methoxycarbonyl-phenyl-methyl)-aminooxalyl]-amino)-phenyl-acetic acid methyl ester
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 0℃; for 3h; | 98% |
L-2-phenylglycine methyl ester hydrochloride
Trimethylenediamine
(2S)-N1-(3-aminopropyl)-2-phenylglycinamide
Conditions | Yield |
---|---|
Stage #1: L-2-phenylglycine methyl ester hydrochloride With triethylamine In methanol; diethyl ether Stage #2: Trimethylenediamine at 20℃; for 19h; Further stages.; | 98% |
L-2-phenylglycine methyl ester hydrochloride
Conditions | Yield |
---|---|
Stage #1: L-2-phenylglycine methyl ester hydrochloride With ammonia; sodium hydroxide In chloroform; water Stage #2: With deuteromethanol | 98% |
L-2-phenylglycine methyl ester hydrochloride
(S)-methyl 2-amino-2-(3-nitrophenyl)acetate
Conditions | Yield |
---|---|
Stage #1: L-2-phenylglycine methyl ester hydrochloride With sulfuric acid; nitric acid at -10 - 20℃; Stage #2: With ammonium hydroxide In water pH=9; Cooling with ice; | 97% |
Stage #1: L-2-phenylglycine methyl ester hydrochloride With sulfuric acid; nitric acid at 0℃; for 4h; Stage #2: With water; sodium hydrogencarbonate In ethyl acetate at 0℃; | 2% |
L-2-phenylglycine methyl ester hydrochloride
methyl (2S)-amino(cyclohexyl)ethanoate hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen In methanol; water at 20℃; under 760.051 Torr; for 24h; | 97% |
potassium cyanate
L-2-phenylglycine methyl ester hydrochloride
(5S)-5-phenyl-2,4-imidazolinedione
Conditions | Yield |
---|---|
Stage #1: potassium cyanate; L-2-phenylglycine methyl ester hydrochloride In water Milling; Green chemistry; Stage #2: With caesium carbonate; triethylamine In water Green chemistry; | 97% |
L-2-phenylglycine methyl ester hydrochloride
benzaldehyde
Conditions | Yield |
---|---|
Stage #1: L-2-phenylglycine methyl ester hydrochloride With triethylamine In dichloromethane for 0.5h; Stage #2: benzaldehyde With magnesium sulfate In dichloromethane | 96.8% |
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