Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:15307-86-5
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inquiryItems Standard Result CHARACERS A white crystalline Powder White crystalline powder IDENTIFICATION
Cas:15307-86-5
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inquiryUnique advantages of 1-(2,6-Dichlorophenyl)-2-indolinone Cas 15307-86-5 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White powder Storage:Cool dry place Package:1kg
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
1-(2,6-Dichlorophenyl)-2-indolinone Basic information Product Name: 1-(2,6-Dichlorophenyl)-2-indolinone Synonyms: 1-(2,6-DICHLOROPHENYL)-1,3-DIHYDRO-INDOLE-2-ONE;(N-1-(2,6-DICHLOROPHENYL
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inquiryOur advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be
Cas:15307-86-5
Min.Order:1 Kilogram
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Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:15307-86-5
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:15307-86-5
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Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present,
Cas:15307-86-5
Min.Order:1 Kilogram
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Type:Trading Company
inquiry1-(2,6-Dichlorophenyl)-2-indolinone CAS:15307-86-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quali
Cas:15307-86-5
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:15307-86-5
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inquiryHebei Mojin Biotechnology Co., Ltd,Our business covers more than 30 countries, most of the big customers come from Europe, America and other countries in the world, we can guarantee the quality and price. In recent decades, with the efforts of all em
Cas:15307-86-5
Min.Order:1 Gram
FOB Price: $50.0
Type:Trading Company
inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:15307-86-5
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Type:Lab/Research institutions
inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:white powder/ Refer to COA Storage:Refer to COA
Cas:15307-86-5
Min.Order:1 Kilogram
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Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:15307-86-5
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Product Name: 1-(2,6-Dichlorophenyl)-2-indolinone Synonyms: Diclofenac Free Base;Dichlofenac acid;Diclac;DiclofenaMic acid;DicloMelan;DicloreuMa;Transfenac;Voltaflan CAS: 15307-86-5 MF: C14H9Cl2NO MW: 278.13 EINECS: 239-348-5 Product C
Cas:15307-86-5
Min.Order:100 Gram
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:15307-86-5
Min.Order:4 Kilogram
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inquiryOur Advantages Production: Advanced chemical equipment with years of experience.Staffs for producing various extract products. Quality Control:A complete set of Testing Professional and Analysis Equipment ensures the Quality Requirements and Speci
Cas:15307-86-5
Min.Order:1 Kilogram
FOB Price: $150.0 / 180.0
Type:Trading Company
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:15307-86-5
Min.Order:10 Gram
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:15307-86-5
Min.Order:100 Gram
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Type:Lab/Research institutions
inquirymoderate price & quick delivery Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:prostaglandin synthetic inhibitor Tra
Cas:15307-86-5
Min.Order:1 Kilogram
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Type:Trading Company
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:15307-86-5
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:15307-86-5
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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inquiry[2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid diethylcarbamoylmethylcarbamoyloxymethyl ester
A
2-amino-N,N-diethylacetamide
B
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With human plasma In phosphate buffer at 37℃; pH=7.4; | A n/a B 100% |
[2-(2,6-dichloro-phenylamino)-phenyl]-acetic acid 1-diethylcarbamoyl-2-phenyl-ethylcarbamoyloxymethyl ester
A
[2-(2,6-dichloroanilino)phenyl]acetic acid
B
N-(phenylalanyl)-N,N-diethylamine
Conditions | Yield |
---|---|
With human plasma In phosphate buffer at 37℃; pH=7.4; | A 100% B n/a |
diclofenac sodium
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With hydrogenchloride In water; acetone at 20 - 45℃; for 3h; pH=1.4 - 1.6; Solvent; | 99% |
With hydrogenchloride In water Cooling with ice; | 90% |
With hydrogenchloride In water at 0 - 20℃; | 70% |
2,6-Dichlorophenol
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 60 - 100℃; for 8h; Temperature; Reagent/catalyst; | 95% |
N,N-dimethyl-o-(2,6-dichloroanilino)phenylacetamide
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol; water | 92.9% |
2-[(2,6-dichlorophenyl)-N-benzylamino]-phenylacetic acid
water
1,2-dichloro-benzene
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
In tetrahydrofuran; hexane; toluene | 91.2% |
2-<(2,6-dichlorophenyl)amino>-α-(methylthio)phenylacetic acid
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With nickel In ethanol Heating; | 85% |
1-(2,6-dichlorophenyl)indolin-2-one
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
In hydrogenchloride; toluene liquid HCl; | 84.4% |
Naprelan
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With hydrogenchloride In water at 20℃; | 82.2% |
ortho-bromophenylacetic acid
2,6-Dichloroaniline
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With D-myo-inositol; copper; caesium carbonate In water at 100℃; for 30h; | 82% |
2'-chloro-benzeneacetic acid
2,6-Dichloroaniline
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With copper(l) iodide; potassium carbonate; potassium iodide In 1,4-dioxane at 130 - 150℃; for 7h; Concentration; Solvent; Inert atmosphere; | 80% |
With copper(l) iodide; potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 165℃; for 12h; Ullmann Condensation; Sealed tube; | 34% |
With copper(I) chloride; potassium carbonate; potassium iodide In N,N-dimethyl-formamide; xylene at 150 - 152℃; for 5h; |
o-(N-allyl-2,6-dichloroanilino)phenylacetic acid
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane; water; benzene | 72% |
ortho-bromophenylacetic acid
2,6-Dichloroaniline
diethylene glycol
A
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With L-2-O-methyl-chiro-inositol; copper(II) acetate monohydrate; potassium carbonate at 110℃; for 12h; Inert atmosphere; | A 72% B 17% |
2-(2-iodophenyl)acetonitrile
2,6-Dichloroaniline
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
Stage #1: 2-(2-iodophenyl)acetonitrile With potassium hydroxide In ethanol at 80℃; for 12h; Inert atmosphere; Sealed tube; Stage #2: 2,6-Dichloroaniline With copper(l) iodide; potassium carbonate In toluene at 100℃; for 12h; Inert atmosphere; Sealed tube; | 70% |
potassium 2-iodophenylacetate
2,6-Dichloroaniline
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; copper(l) iodide; potassium carbonate at 100℃; Ullmann coupling; | 61% |
2-<(2,6-Dichlorphenacyl)amino>phenylessigsaeure-2-oxopropylester
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With buffer pH 8.0 In 1,4-dioxane; acetonitrile at 57℃; half-life time of hydrolysis at different pH; |
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
at 37℃; Rate constant; t1/2, simulated gastric fluid, rate plasma, further reagents, temperatures; |
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
at 37℃; Rate constant; t1/2, simulated gastric fluid, rate plasma, further reagents; |
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
at 37℃; Rate constant; t1/2, simulated gastric fluid, rate plasma, further reagents; |
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With NADPH-generating system; rat liver homogenate at 37℃; Enzyme kinetics; Hydrolysis; Enzymatic reaction; |
diclofenac sodium
A
2-oxoindole
B
2,6-Dichlorophenol
C
1-(2,6-dichlorophenyl)indolin-2-one
D
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
In phosphate buffer at 45℃; Kinetics; Thermodynamic data; Further Variations:; pH-values; Temperatures; |
aceclofenac
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With sodium hydroxide for 3h; Heating; |
N-phenyl-2,6-dichloroaniline
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: benzene / 6 h / Heating 2: 91 percent / m-chloroperbenzoic acid / CH2Cl2 / 1 h / Ambient temperature 3: 84 percent / p-toluenesulfonic acid / benzene / 0.5 h / Heating 4: 91 percent / 2N NaOH / ethanol / 48 h / Heating 5: 85 percent / Raney nickel / ethanol / Heating View Scheme | |
Multi-step reaction with 5 steps 1: benzene / 6 h / Heating 2: N-chlorosuccinimide / CCl4 / 1 h / Ambient temperature 3: SnCl4 / CCl4 / 0.83 h / Ambient temperature 4: 91 percent / 2N NaOH / ethanol / 48 h / Heating 5: 85 percent / Raney nickel / ethanol / Heating View Scheme |
N-(2,6-dichlorophenyl)-α-(methylthio)acetanilide
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 91 percent / m-chloroperbenzoic acid / CH2Cl2 / 1 h / Ambient temperature 2: 84 percent / p-toluenesulfonic acid / benzene / 0.5 h / Heating 3: 91 percent / 2N NaOH / ethanol / 48 h / Heating 4: 85 percent / Raney nickel / ethanol / Heating View Scheme | |
Multi-step reaction with 4 steps 1: N-chlorosuccinimide / CCl4 / 1 h / Ambient temperature 2: SnCl4 / CCl4 / 0.83 h / Ambient temperature 3: 91 percent / 2N NaOH / ethanol / 48 h / Heating 4: 85 percent / Raney nickel / ethanol / Heating View Scheme |
1-(2,6-dichlorophenyl)-3-(methylthio)oxindole
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 91 percent / 2N NaOH / ethanol / 48 h / Heating 2: 85 percent / Raney nickel / ethanol / Heating View Scheme |
N-(2,6-dichlorophenyl)-α-(methylsulfinyl)acetanilide
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 84 percent / p-toluenesulfonic acid / benzene / 0.5 h / Heating 2: 91 percent / 2N NaOH / ethanol / 48 h / Heating 3: 85 percent / Raney nickel / ethanol / Heating View Scheme |
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SnCl4 / CCl4 / 0.83 h / Ambient temperature 2: 91 percent / 2N NaOH / ethanol / 48 h / Heating 3: 85 percent / Raney nickel / ethanol / Heating View Scheme |
4-((3,3-dimethylbutoxy)carbonyloxy)benzyl 2-(2-(2,6-dichlorophenylamino)phenyl)acetate
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With water at 37℃; pH=7.4; Kinetics; |
bromoacetic acid tert-butyl ester
[2-(2,6-dichloroanilino)phenyl]acetic acid
2-((2,6-dichlorophenyl)amino)phenylacetoxyacetic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In DMF (N,N-dimethyl-formamide) at 20℃; | 100% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
(+)-O-Demethyltramadol
Conditions | Yield |
---|---|
With water In acetonitrile at 20℃; under 760.051 Torr; Product distribution / selectivity; | 100% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
(±)-cis-2-[(dimethylamino)methyl]-1-(3-hydroxyphenyl)cyclohexanol
Conditions | Yield |
---|---|
In isopropyl alcohol at 20℃; Product distribution / selectivity; | 100% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
O-desmethyltramadol
Conditions | Yield |
---|---|
In isopropyl alcohol at 20℃; Product distribution / selectivity; | 100% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
1-Adamantanamine
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With copper diacetate; sodium carbonate; (3aR,3a'R,8aS,8a'S)-2,2'-(propane-2,2-diyl)bis(8,8a-dihydro-3aH-indeno[1,2-d]oxazole) In dichloromethane; water at 30℃; for 12h; enantioselective reaction; | 99% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 0.5h; Acylation; | 98% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
(2E)-3-phenyl-2-propen-1-ol
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide at 20℃; for 4h; | 98% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
diazomethyl-trimethyl-silane
2-[(2,6-dichlorophenyl)amino]phenylacetic acid methyl ester
Conditions | Yield |
---|---|
In methanol; hexane; benzene at 25℃; for 1h; | 96% |
With methanol In Dimethyl ether |
methanol
[2-(2,6-dichloroanilino)phenyl]acetic acid
2-[(2,6-dichlorophenyl)amino]phenylacetic acid methyl ester
Conditions | Yield |
---|---|
With sulfuric acid for 0.25h; Reflux; | 96% |
Stage #1: methanol; [2-(2,6-dichloroanilino)phenyl]acetic acid With hydrogenchloride In water for 6h; Reflux; Stage #2: With sodium carbonate In water | 91% |
Stage #1: methanol; [2-(2,6-dichloroanilino)phenyl]acetic acid With hydrogenchloride In water for 6h; Reflux; Stage #2: With sodium hydrogencarbonate In water Cooling with ice; Saturated solution; | 91% |
1-hydroxy-pyrrolidine-2,5-dione
[2-(2,6-dichloroanilino)phenyl]acetic acid
acetic acid N-oxysuccinimide ester
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In 1,4-dioxane for 8h; Ambient temperature; | 95% |
With dicyclohexyl-carbodiimide In dichloromethane for 1h; | 90% |
With dicyclohexyl-carbodiimide In tetrahydrofuran at 5℃; | |
Stage #1: 1-hydroxy-pyrrolidine-2,5-dione; [2-(2,6-dichloroanilino)phenyl]acetic acid In tetrahydrofuran at 0 - 5℃; for 0.166667h; Inert atmosphere; Stage #2: With dicyclohexyl-carbodiimide In tetrahydrofuran at 20℃; Inert atmosphere; | |
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; Inert atmosphere; |
chlorosulfuric acid chloromethyl ester
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate In dichloromethane; water at 20℃; for 1h; | 95% |
With Bu4HSO4 In dichloromethane; water at 20℃; for 1h; |
[2-(2,6-dichloroanilino)phenyl]acetic acid
(5-methyl-2-phenyl-1,3-dioxan-5-yl)methyl 4-hydroxybenzoate
(5-methyl-2-phenyl-1,3-dioxan-5-yl)methyl 4-(2-(2-((2,6-dichlorophenyl)amino)phenyl)acetoxy)benzoate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran; dichloromethane at 0 - 20℃; for 18h; | 95% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
[(2R)-2-aminopropyl]carbamic acid,1,1-dimethylethyl ester
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 1.5h; Cooling with ice; | 95% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
1-(2,6-dichlorophenyl)indolin-2-one
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 0.5h; | 94% |
With thionyl chloride In dichloromethane; ethyl acetate at 50℃; for 2h; Concentration; Temperature; | 92% |
With hydrogenchloride In acetonitrile at 78.85℃; for 5h; Rate constant; Kinetics; Mechanism; energy data: ΔH(activ.), ΔS(activ.); ΔE(activ.)var. amount of acetonitrile, var. temp.; |
[2-(2,6-dichloroanilino)phenyl]acetic acid
3-{Methyl{[(nitrosothio)cyclohexyl]methyl}amino)propan-1-ol
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 0.5h; Acylation; | 94% |
Conditions | Yield |
---|---|
In acetone at 50 - 55℃; for 2h; pH=8.5 - 10.0; | 93.7% |
2,2-dimethyl-1,3-dioxolane
[2-(2,6-dichloroanilino)phenyl]acetic acid
A
1-(2,6-dichlorophenyl)indolin-2-one
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In ethanol Cyclization; | A n/a B 93% |
1-pyrrolidineethanol
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
In acetone | 92% |
Magnolol
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 1h; | 92% |
With dmap In dichloromethane at 25 - 30℃; | 92% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine In N,N-dimethyl acetamide at 100℃; for 12h; Inert atmosphere; Molecular sieve; | 92% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
2-ethyl-2-(nitrosothio)butan-1-ol
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 0.5h; Acylation; | 91% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
ethanolamine
Conditions | Yield |
---|---|
In acetone | 90% |
[2-(2,6-dichloroanilino)phenyl]acetic acid
2-(2-tert-butyloxycarbonylaminoethoxy)ethanol
[2-(2,6-dichlorophenylamino)phenyl]acetic acid 2-(2-tert-butoxycarbonylaminoethoxy)ethyl ester
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 1h; | 90% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 4h; Cooling with ice; | 1.166 g |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 35℃; for 2h; | 2.44 g |
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