CAS No.180181-93-5,3-N-FMOC-3-PHENYLPROPIONIC ACID Suppliers

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Henan Wentao Chemical Product Co., Ltd.

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beta-[[(9H-Fluoren-9-ylmethoxy)carbonyl]amino]benzenepropanoic acid

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3-((((9H-Fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

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Fmoc-3-amino-3-phenylpropionic acid 180181-93-5

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Benzenepropanoic acid, b-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]-

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ENAO Chemical Co, Limited

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3-((((9H-Fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

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Finetech Industry Limited

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Fmoc-3-amino-3-phenylpropionic acid

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Pure Chemistry Scientific Inc.

Fmoc-3-amino-3-phenylpropionic acid Application:2055632

Fmoc-3-amino-3-phenylpropionic acid

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Wuhan Chemwish Technology Co., Ltd

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Fmoc-3-amino-3-phenylpropionic acid

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NovaChemistry

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Fmoc-DL-3-amino-3-phenylpropionic acid

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InnovaChem Technology, Inc.

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Benzenepropanoic acid, b-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]-

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Benzenepropanoic acid, b-[[(9H-fluoren-9-ylmethoxy)carbonyl]amino]-

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Synthetic route

: 28920-43-6
(fluorenylmethoxy)carbonyl chloride

: 3646-50-2
3-Amino-3-phenylpropionic acid

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

Conditions

Conditions	Yield
With sodium hydrogencarbonate In 1,4-dioxane; water at 0 - 20℃; for 25h;	100%
With sodium hydroxide In 1,4-dioxane at 20℃; for 4h;	77%
With N-ethyl-N,N-diisopropylamine

: (±)-(9H-fluoren-9-yl)methyl 5-oxo-3-phenylisoxazolidine-2-carboxylate

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

Conditions

Conditions	Yield
With acetic acid; zinc In tetrahydrofuran; water at 40℃; for 4h; Inert atmosphere; chemoselective reaction;	95%

: 3646-50-2
3-Amino-3-phenylpropionic acid

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

Conditions

Conditions	Yield
With sodium hydrogencarbonate In water; acetone at 0℃; for 3h;

: 100-52-7
benzaldehyde

: 190656-01-0
N-(9-fluorenylmethoxycarbonyloxy)hydroxylamine

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: sodium 2,2-dimethyl-4-oxo-4H-1,3-dioxin-6-olate / ethyl acetate / 4 h / 40 °C / Inert atmosphere 2: acetic acid; zinc / tetrahydrofuran; water / 4 h / 40 °C / Inert atmosphere View Scheme

: 29022-11-5
N-(fluoren-9-ylmethoxycarbonyl)glycine

: 18856-63-8
(4-ethylphenyl)isothiocyanate

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: 2-{2-[(Z)-4-Ethyl-phenylimino]-6-oxo-4-phenyl-tetrahydro-pyrimidin-1-yl}-acetamide

Conditions

Conditions	Yield
Multistep reaction;	95%

...Expand

: 76-05-1
trifluoroacetic acid

: 207908-96-1
4-[5-(4-aminobutyl)thien-2-yl]butylamine

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

trityl chloride resin: trityl chloride resin

: [3-(4-[5-(4-ammoniobutyl)-2-thienyl]butylamino)-3-oxo-1-phenylpropyl]ammonium ditrifluoroacetate

Conditions

Conditions	Yield
Multistep reaction.;	73%

...Expand

: 31575-35-6
2-fluoropyrimidine

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: 852632-28-1
C13H14N4O

Conditions

Conditions	Yield
Stage #1: (±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine solid phase reaction; Stage #2: With piperidine In N,N-dimethyl-formamide solid phase reaction; Stage #3: 2-fluoropyrimidine Further stages;	23%

: 123622-48-0
5-(9H-fluoren-9-ylmethoxycarbonyl)aminopentanoic acid

: 250280-31-0
5-(9H-fluoren-9-ylmethoxy)-1,3,4-oxadiazol-2(3H)-one

: N,N'-bis-Boc-1-guanylpyrazole

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: C16H24N6O4

Conditions

Conditions	Yield
Multistep reaction.;	22 mg

...Expand

: 185116-42-1
3-(9-fluorenylmethyloxycarbonyl)aminobenzoic acid

: 250280-31-0
5-(9H-fluoren-9-ylmethoxy)-1,3,4-oxadiazol-2(3H)-one

: N,N'-bis-Boc-1-guanylpyrazole

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: C18H20N6O4

Conditions

Conditions	Yield
Multistep reaction.;	6 mg

...Expand

: 250280-31-0
5-(9H-fluoren-9-ylmethoxy)-1,3,4-oxadiazol-2(3H)-one

: 287959-61-9
5-[N-(4-methylpyridin-2-yl)amino]pentanoic acid

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: 3-{N-[N'-(5-(4-methylpyridin-2-ylamino)pentanoyl)hydrazino]carbonyl}amino-3-phenylpropionic acid

Conditions

Conditions	Yield
Multistep reaction.;	17 mg

...Expand

: 77128-70-2
N-(9-fluorenylmethoxycarbonyl)sarcosine

: 175452-89-8
α-methyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)glutamate ester

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: 368443-82-7
α-methyl (2R)-N-(fluoren-9-ylmethoxycarbonyl)aspartate

Fmoc-(2S)-Phe: Fmoc-(2S)-Phe

: 1053615-12-5
(2S)-phenylalanyl-[(3R/S)-3-amino-3-phenylpropanoyl]-[α-methyl (2R)-glutamyl]-sarcosyl-[α-methyl (2R)-aspartate] diester

Conditions

Conditions	Yield
Multistep reaction.;	150 mg

...Expand

: 71989-33-8
Fmoc-Ser(tBu)-OH

: 1074-59-5
3-(imidazol-4-yl)propionic acid

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: (S)-2-amino-3-(8-hydroxy-5-(N,N-dimethyl)sulfonamidoquinoline-2-yl)propionic acid hydrochloride

Fmoc-Pro: Fmoc-Pro

: [3-(imidazol-4-yl)propionic acid]-Pro-β-dimethylcysteine-[(S)-2-amino-3-(8-hydroxy-5-(N,N-dimethyl)sulfonamidoquinoline-2-yl)propionic acid]-Ser-Ser-NH2

Conditions

Conditions	Yield
Multistep reaction;

...Expand

trityl chloride polystyrene resin: trityl chloride polystyrene resin

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: C24H20NO4Pol

Conditions

Conditions	Yield
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 2h;

: 2-chlorotrityl chloride polystyrene resin

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: C43H33ClNO4Pol

Conditions

Conditions	Yield
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 0.5h; not specified;

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: 200642-62-2
[3-[(4,5-dihydro-5-thioxo-1,3,4-thiadiazol-2-yl)amino]-3-oxo-1-phenylpropyl]carbamic acid 9H-fluoren-9-yl methyl ester

Conditions

Conditions	Yield

: 4548-45-2
2-chloro-5-nitropyridine

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: 1235447-27-4
C14H14N4O3

Conditions

Conditions	Yield
Stage #1: (±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine solid phase reaction; Stage #2: With piperidine In N,N-dimethyl-formamide solid phase reaction; Stage #3: 2-chloro-5-nitropyridine Further stages;

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: C24H20ClNO3

Conditions

Conditions	Yield
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 1h; Inert atmosphere;
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 1h; Inert atmosphere;

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: C39H45NO6

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: magnesium chloride; pyridine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 2 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: ethyl 4,16-dioxo-2-phenyl-1-azacyclohexadecane-5-carboxylate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: magnesium chloride; pyridine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 2 h / 20 °C / Inert atmosphere 3.1: piperidine / dichloromethane / 2 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: ethyl-4,9-dioxo-2-phenylazonane-5-carboxylate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: pyridine; magnesium chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 2 h / 20 °C / Inert atmosphere 3.1: piperidine / dichloromethane / 1 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: C38H35NO6

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: pyridine; magnesium chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 1 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: C33H33NO7

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: pyridine; magnesium chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 1 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: ethyl 4, 10-dioxo-2-phenylazecane-5-carboxylate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: pyridine; magnesium chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 2 h / 20 °C / Inert atmosphere 3.1: piperidine / dichloromethane / 1 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: ethyl 1,5-dioxo-3-phenyl-1,2,3,4,5,6,7,8-octahydrobenzo[c]azecine-6-carboxylate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: pyridine; magnesium chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 1 h / 20 °C / Inert atmosphere 3.1: piperidine / dichloromethane / 1 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: ethyl-4,11-dioxo-2-phenyl-1-azacycloundecane-5-carboxylate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: pyridine; magnesium chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 2 h / 20 °C / Inert atmosphere 3.1: piperidine / dichloromethane / 2 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: ethyl 1,5-dioxo-3-phenyl-2,3,4,5,6,7,8,9-octahydro-1H-benzo[c][1]azacycloundecine-6-carboxylate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: pyridine; magnesium chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 1 h / 20 °C / Inert atmosphere 3.1: piperidine / dichloromethane / 1 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: ethyl 4,8-dioxo-6-phenyl-1-oxa-5-azacycloundecane-9-carboxylate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: pyridine; magnesium chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 1 h / 20 °C / Inert atmosphere 3.1: piperidine / dichloromethane / 1 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: C32H31NO6

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: pyridine; magnesium chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 2 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: C33H33NO6

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: pyridine; magnesium chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 2 h / 20 °C / Inert atmosphere View Scheme

: 180181-93-5
(±)-3-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-phenylpropanoic acid

: C37H33NO6

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C / Inert atmosphere 2.1: pyridine; magnesium chloride / dichloromethane / 0.5 h / 20 °C / Inert atmosphere 2.2: 1 h / 20 °C / Inert atmosphere View Scheme

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Henan Allgreen Chemical Co.,Ltd

Antimex Chemical Limied

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Hunan Russell Chemicals Technology Co.,Ltd

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