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Product Name: 2-Pyridinemethanethiol Synonyms: PYRIDINE-2-METHANETHIOL;2-pyridylmethylmercaptan;pyridine-2-thiocarbinol;2-MERCAPTOMETHYL PYRIDINE;2-PYRIDINE METHANETHIOL;FEMA 3232;FEMA NUMBER 3232;2-PYRIDINE METHANETHIOL 10% IN ETHANOL CAS: 2044-
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inquirythioacetic acid S‐pyridine‐2‐ylmethyl ester
2-(sulfanylmethyl)pyridine
Conditions | Yield |
---|---|
With water; potassium carbonate In methanol at 85℃; for 2.5h; Inert atmosphere; | 94% |
With potassium carbonate In methanol for 0.5h; Heating; | 82% |
With sodium hydroxide In methanol |
Conditions | Yield |
---|---|
With sodium hydrogensulfide In ethanol for 4h; Substitution; | 88% |
2-chloromethylpyridine hydrochloride
thiourea
2-(sulfanylmethyl)pyridine
Conditions | Yield |
---|---|
Stage #1: 2-chloromethylpyridine hydrochloride; thiourea In water at 85 - 89℃; for 1h; Inert atmosphere; Stage #2: With sodium hydroxide In water at 5 - 22℃; for 16h; Inert atmosphere; | 86% |
Stage #1: 2-chloromethylpyridine hydrochloride; thiourea In water at 85 - 89℃; for 1h; Inert atmosphere; Stage #2: With sodium hydroxide In water at 5 - 22℃; for 16h; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With thiourea; sodium hydroxide In water | 85% |
With sodium hydroxide; thiourea In ethanol for 1h; Heating; | 65% |
Stage #1: 2-chloromethylpyridine hydrochloride With thiourea In water at 80 - 85℃; for 1h; Schlenk technique; Inert atmosphere; Stage #2: With sodium hydroxide at 0 - 20℃; for 12.5h; Schlenk technique; Inert atmosphere; | 63% |
3-Phenyl-5-pyridin-2-yl-2-thioxo-thiazolidin-4-one
A
2-(sulfanylmethyl)pyridine
B
aniline
Conditions | Yield |
---|---|
With hydrogen bromide for 8h; Heating; | A n/a B 51% |
2-<2>Pyridylmethyl-isothioharnstoff
2-(sulfanylmethyl)pyridine
Conditions | Yield |
---|---|
With sodium hydroxide at 70℃; for 0.333333h; |
Conditions | Yield |
---|---|
With sodium hydroxide at 70℃; for 0.333333h; |
2-((pyridin-2-yl)methyl)isothiourea hydrobromide
2-(sulfanylmethyl)pyridine
Conditions | Yield |
---|---|
With sodium hydroxide In water for 1h; Heating; | 0.7 g |
2-(sulfanylmethyl)pyridine
Conditions | Yield |
---|---|
With sodium hydroxide |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 80 percent / p-toluenesulphonylchloride / benzene / 4 h / Heating 2: 88 percent / sodium hydrogen sulfide / ethanol / 4 h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: DEAD, PPh3 / tetrahydrofuran / Ambient temperature 2: NaOH / methanol View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ethanol / 3 h / Heating 2: 10 N aq. NaOH / 0.33 h / 70 °C View Scheme |
2-(Bromomethyl)pyridine
2-(sulfanylmethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 3.12 g / ethanol / 6 h / Heating 2: 0.7 g / NaOH / H2O / 1 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 72 percent / acetic anhydride / dimethylformamide / 5 h / 90 °C 2: 48percent hydrobromic acid / 8 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 80 °C / Inert atmosphere 2: triethylamine / methanol / 2 h / 20 °C / Inert atmosphere 3: water; potassium carbonate / methanol / 2.5 h / 85 °C / Inert atmosphere View Scheme |
2-(bromomethyl)pyridine hydrochloride
2-(sulfanylmethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / methanol / 2 h / 20 °C / Inert atmosphere 2: water; potassium carbonate / methanol / 2.5 h / 85 °C / Inert atmosphere View Scheme |
2-(sulfanylmethyl)pyridine
1-<(4-methoxyphenyl)amino>-2-methylpropane-2-thiol
(N-(2-mercapto-2-methylpropyl)-N-(4'-methoxyphenyl)aminato)(2-mercaptomethylpyridinato)oxorhenium(V)
Conditions | Yield |
---|---|
With sodium acetate In methanol ratio propanethiol:C5H4NCH2SH = 1:1, heated at 75°C for 20 min; cooled to ambient temp., recrystd. (MeOH/CHCl3); | 99% |
With sodium acetate In methanol ratio propanethiol:C5H4NCH2SH = 1:2, heated at 75°C for 20 min; cooled to ambient temp., recrystd. (MeOH/CHCl3); | 85% |
With sodium acetate In methanol ratio propanethiol:C5H4NCH2SH = 1:4, heated at 75°C for 20 min; cooled to ambient temp., recrystd. (MeOH/CHCl3); | 50% |
Conditions | Yield |
---|---|
at 20℃; Inert atmosphere; Schlenk technique; | 98% |
2-(sulfanylmethyl)pyridine
1-<(4-methoxyphenyl)amino>-2-methylpropane-2-thiol
(N-(2-mercapto-2-methylpropyl)-N-(4'-methoxyphenyl)aminato)(2-mercaptomethylpyridinato)oxorhenium(V)
Conditions | Yield |
---|---|
With sodium acetate In methanol ratio propanethiol:C5H4NCH2SH = 2:1, heated at 75°C for 20 min; cooled to ambient temp., recrystd. (MeOH/CHCl3); | A 97% B 2% |
With sodium acetate In methanol ratio propanethiol:C5H4NCH2SH = 4:1, heated at 75°C for 20 min; cooled to ambient temp., recrystd. (MeOH/CHCl3); | A 4% B 86% |
2-(sulfanylmethyl)pyridine
acrylonitrile
3-<<(2-pyridyl)methyl>thio>propionitrile
Conditions | Yield |
---|---|
With sodium methylate at 40 - 50℃; | 95.5% |
With sodium methylate; acetic acid In water | |
With sodium methylate; acetic acid In water |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 3h; Inert atmosphere; | 88% |
2-(sulfanylmethyl)pyridine
(3R,4R)-3-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-4-acetoxyazetidin-2-one
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 2h; Ambient temperature; | 87.3% |
Conditions | Yield |
---|---|
With NaOCH3 In methanol mixing equimolar amts. of pyridine derivative and NaOMe, addn. of 0.5 equiv. of Zn-salt (pptn.); filtration, washing (cold MeOH), drying (vac.), recrystn. (MeOH); elem. anal.; | 87% |
Conditions | Yield |
---|---|
With potassium hydroxide In acetonitrile for 12h; Reflux; | 86% |
Conditions | Yield |
---|---|
With potassium hydroxide In acetonitrile for 12h; Reflux; | 85% |
1,2,4-Triazole
2-(sulfanylmethyl)pyridine
2-picolylthiophosphoro-bis-triazolide
Conditions | Yield |
---|---|
Stage #1: 2-(sulfanylmethyl)pyridine With phosphorus trichloride for 0.5h; Substitution; Stage #2: 1,2,4-Triazole In tetrahydrofuran for 0.5h; Substitution; | 81% |
2-(sulfanylmethyl)pyridine
Conditions | Yield |
---|---|
81% |
2,3-Dichloro-1,4-naphthoquinone
2-(sulfanylmethyl)pyridine
2,3-di-α-pyridylmethylmercapto-1,4-naphthoquinone
Conditions | Yield |
---|---|
With tributyl-amine In ethanol for 3h; stirring in the cold; | 74% |
2-(sulfanylmethyl)pyridine
hydridotetakis(triphenylphosphine)rhodium(I)
RhH2(2-pyridylmethanethiolate)(PPh3)2
Conditions | Yield |
---|---|
In diethyl ether (N2); addn. of excess of thiol to suspn. of Rh-complex in Et2O, stirring (30 min); filtration, washing (Et2O); | 73% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 2.5h; Reflux; Inert atmosphere; | 71% |
2-(sulfanylmethyl)pyridine
methyl iodide
2-[(methylsulfanyl)methyl]pyridine
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 0 - 20℃; | 70% |
With sodium hydroxide at 0℃; for 2h; |
2-(sulfanylmethyl)pyridine
1-(2-butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine
Conditions | Yield |
---|---|
64.8% |
2-(sulfanylmethyl)pyridine
Conditions | Yield |
---|---|
With diimidazolylsulfide at 0 - 25℃; | 60% |
2-(sulfanylmethyl)pyridine
potassium trifluoro(3-oxo-3-phenylprop-1-yn-1-yl)borate
Conditions | Yield |
---|---|
With potassium tert-butylate; tert-butyl alcohol In acetonitrile at 0 - 20℃; Fiesselmann Thiophene Synthesis; regioselective reaction; | 60% |
2-(sulfanylmethyl)pyridine
potassium trifluoro(3-oxo-3-phenylprop-1-yn-1-yl)borate
Conditions | Yield |
---|---|
With methanol; potassium carbonate In acetonitrile at 0 - 20℃; Fiesselmann Thiophene Synthesis; regioselective reaction; | 60% |
2-(sulfanylmethyl)pyridine
Conditions | Yield |
---|---|
In acetonitrile to refluxing soln. of Re-complex in MeCN soln. of ligand in MeCN was added dropwise, refluxed for 15 min; evapd. to dryness, dissolved in EtOH, layered with Et2O; elem. anal.; | 56.8% |
2-(sulfanylmethyl)pyridine
[1,4]naphthoquinone
A
naphtho<2,3-b>indolizine-6,11-dione
B
2-α-pyridylmethylmercapto-1,4-naphthoquinone
C
2,3-di-α-pyridylmethylmercapto-1,4-naphthoquinone
Conditions | Yield |
---|---|
In dichloromethane for 24h; ice-bath; | A n/a B 45% C n/a |
2-(sulfanylmethyl)pyridine
ethyl iodide
2-[(ethylsulfanyl)methyl]pyridine
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 0 - 20℃; | 42.8% |
Conditions | Yield |
---|---|
With Et3N In chloroform to soln. of Re-complex in CHCl3 soln. of ligand and diol in CHCl3 was added, Et3N was added, stirred and refluxed for 30 min; evapd. to dryness; elem. anal.; | 42.1% |
2-(sulfanylmethyl)pyridine
dichlorotetrakis(dimethyl sulfoxide)ruthenium(II)
water
Conditions | Yield |
---|---|
Stage #1: 2-(sulfanylmethyl)pyridine; dichlorotetrakis(dimethyl sulfoxide)ruthenium(II) With silver nitrate In ethanol at 20℃; for 48h; Stage #2: sodium perchlorate; water In water | 42.1% |
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