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inquiry1,2,4-Triazole CAS :288-88-0 99% Hangzhou Verychem Science And Technology Co. Ltd. was set up in year 2004, it’s a young but fast growing company. In the twelve years history, it invested two pharmaceutical raw material production
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/81.html Product Name 1,2,4-Triazole CAS No.
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inquiryItems Standard Result Appearance White crystal White crystal Purity ≥99%
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inquiryProduct name 1,2,4-Triazole Synonyms 1,2,4-1H-Triazole CAS NO.: 288-88-0 EINECS 206-0
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Mainly used to produce high-efficiency and low-toxicity agricultural fungicides, plant growth regulators, and pharmaceutical intermediates. Such as tebuconazole, propiconazole, difenoconazole, fenproconazole, paclobutrazol, uniconazole, diniconazole,
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inquiryName 1,2,4-Triazole Synonyms 1,2,4-1H-Triazole Molecular Structure Molecular Formula C2H3N
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inquiryName:1,2,4-1H-Triazole CAS No:288-88-0 Grade:As an intermediate, it is widely used in the synthesis of Triadimefon, Paclobutrazol, Uniconazole and Uniconazol Product Quality 12 years of chemical raw materials Mature operation of the industry
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inquiry1,2,4-Triazole Basic information Product Name: 1,2,4-Triazole Synonyms: TA-4;PYRRODIAZOLE;TRIAZOLE;TRIAZOLE(1,2,4-);AKOS BBS-00004410;1H-1,2,4-TRIAZOLE;1-HYDRO-1,2,4-TRIAZOLE;1,2,4-1H-TR
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inquiryProName: High purity 1,2,4-Triazole 288-88-0 /m... CasNo: 288-88-0 Molecular Formula: C2H3N3 Appearance: Pale yellow acicular crystal Application: It is an important raw material and in... DeliveryTime: prompt PackAge: ac
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inquiryProduct Name: 1,2,4-Triazole Appearance: White Crystalline Powder M.F.: C2H3N3 M.W.: 69.07 CAS NO.: 288-88-0 EINECS NO.: 206-022-9 Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kg per bag or 25k
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inquiryHanways Chempharm Co., Limited, the former is Hubei Hanways Pharchem CO.,Limited, set up in 2009 in Wuhan, China. We specialize in sourcing and supplying APIs, pharmaceutical intermediates, and fine chemicals for worldwide markets. The founder has d
Product Name: 1,2,4-Triazole CAS: 288-88-0 MF: C2H3N3 MW: 69.07 EINECS: 206-022-9 Mol File: 288-88-0.mol 1,2,4-Triazole Structure 1,2,4-Triazole Chemical Properties Melting point 119-121 °C (lit.) Boiling point 260 &de
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Conditions | Yield |
---|---|
With ammonium chloride; hydrazine hydrate at 120℃; Reagent/catalyst; Temperature; Sealed tube; Large scale; | 94% |
d'hydrazide de l'acide propionique
A
1,2,4-Triazole
B
N,N-dimethyl-propanamide
Conditions | Yield |
---|---|
In methanol for 7h; Heating; | A 87% B 91% |
Conditions | Yield |
---|---|
With formamide In water | 89.9% |
Conditions | Yield |
---|---|
In methanol for 8h; Heating; | A 71% B 52% |
1-chloro-1,2,4-triazole
methyl iodide
A
1,2,4-Triazole
B
1-methyl-1H-1,2,4-triazole
Conditions | Yield |
---|---|
In dichloromethane at 42℃; for 3h; Further byproducts given; | A 19% B 6% C 56% D 17% |
In dichloromethane at 20℃; for 48h; Further byproducts given; | A 30% B 14% C 27% D 34% |
1-chloro-1,2,4-triazole
methyl iodide
A
1,2,4-Triazole
B
1-methyl-1H-1,2,4-triazole
C
1-iodo-1,2,4-triazole
Conditions | Yield |
---|---|
In chloroform at 20℃; for 48h; | A 32% B 16% C 52% |
1-chloro-1,2,4-triazole
A
1,2,4-Triazole
B
1-methyl-1H-1,2,4-triazole
C
1-iodo-1,2,4-triazole
Conditions | Yield |
---|---|
With methyl iodide In chloroform at 20℃; for 48h; | A 32% B 16% C 52% |
1-chloro-1,2,4-triazole
methyl iodide
A
1,2,4-Triazole
B
1-methyl-1H-1,2,4-triazole
C
1-iodo-1,2,4-triazole
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 48h; | A 43% B 7% C 27% D 23% |
1-chloro-1,2,4-triazole
A
1,2,4-Triazole
B
1-methyl-1H-1,2,4-triazole
C
1-iodo-1,2,4-triazole
Conditions | Yield |
---|---|
With methyl iodide In dichloromethane at 20℃; for 48h; | A 43% B 7% C 27% D 23% |
1-chloro-1,2,4-triazole
methyl iodide
A
1,2,4-Triazole
B
2,4-dimethyl-2,4-dihydro-[1,2,4]triazol-3-one
Conditions | Yield |
---|---|
In dichloromethane at 42℃; for 3h; Product distribution; other solvent, other temperature, other time; | A 34% B 2% C 40% D 24% |
1-chloro-1,2,4-triazole
methyl iodide
A
1,2,4-Triazole
B
1-methyl-1H-1,2,4-triazole
C
4-methyl-4H-[1,2,4]triazole
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 48h; Further byproducts given; | A 30% B 14% C 5% D 27% |
Conditions | Yield |
---|---|
at 800℃; under 0.01 Torr; flash vacuum pyrolysis; | A 26% B 25% |
A
1,2,4-Triazole
B
1-(4'-chlorophenoxy)-3,3-dimethyl-butan-2-one
C
4-chloro-phenol
Conditions | Yield |
---|---|
In methanol for 24h; Product distribution; Irradiation; also in hexane and acetone; | A 5.5% B 9.5% C 15% D 10.5% E 15% F 11% |
1-benzyl-1,2,4-triazole
benzylidene phenylamine
A
1,2,4-Triazole
B
aniline
C
diphenyl acetylene
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at 75℃; for 0.5h; | A n/a B n/a C 11% |
Conditions | Yield |
---|---|
With hydrazine hydrochloride; ethanol |
Conditions | Yield |
---|---|
With hypophosphorous acid beim Diazotieren; |
Conditions | Yield |
---|---|
With diphosphorus pentasulfide at 200℃; |
Conditions | Yield |
---|---|
With ammonia at 200℃; |
Conditions | Yield |
---|---|
at 260℃; |
formamide
1,2,4-Triazole
Conditions | Yield |
---|---|
With sulfuric acid; hydrazine at 140 - 150℃; |
Conditions | Yield |
---|---|
With nitric acid; sodium nitrite |
1,1'-Carbonyl-di-(1,2,4-triazole)
1,1,1-trichloroethanol
A
1,2,4-Triazole
B
[1,2,4]Triazole-1-carboxylic acid 2,2,2-trichloro-ethyl ester
1,1'-Carbonyl-di-(1,2,4-triazole)
ethanol
A
1,2,4-Triazole
B
ethyl 1H-1,2,4-triazole-1-carboxylate
1,1'-Carbonyl-di-(1,2,4-triazole)
1,1,1,3',3',3'-hexafluoro-propanol
A
1,2,4-Triazole
B
[1,2,4]Triazole-1-carboxylic acid 2,2,2-trifluoro-1-trifluoromethyl-ethyl ester
1-acetyl-1H-[1,2,4]triazole
1,2,4-Triazole
Conditions | Yield |
---|---|
water at 25℃; Rate constant; Thermodynamic data; Mechanism; pH= 4.2; further reagent: D2O (pD= 4.2), isotope effect discussed; furth. cat.: NaOH or H2O in MeCN; |
Conditions | Yield |
---|---|
With water at 25℃; Rate constant; Thermodynamic data; ΔH (excit.), ΔS (excit.); also in the presence of var. carbohydrates; | |
With water In acetonitrile at 25℃; Rate constant; | |
With hydrogenchloride In water; tert-butyl alcohol at 25℃; Kinetics; Rate constant; Thermodynamic data; effect of hydrophobicity of the substrate; ΔH++, ΔS++; | |
With hydrogenchloride In 1,4-dioxane; water at 25℃; Kinetics; Rate constant; Thermodynamic data; effect of hydrophobicity of the substrate; ΔH++, ΔS++; | |
With hydrogenchloride at 25℃; Rate constant; other 1-acyl-1,2,4-triazoles; also in the presence of atactic poly(methacrylic acid); |
1,2,4-Triazole
sodium triazole
Conditions | Yield |
---|---|
With sodium methylate In methanol at 20℃; | 100% |
With sodium methylate In methanol for 4h; Heating / reflux; | 98% |
With sodium hydroxide In water at 20℃; for 4h; Substitution; | 67% |
1,2,4-Triazole
1-vinylthymine
1-vinyl-4-[1,2,4-(1H)-triazol-1-yl]-5-methyl-pyrimidin-2-(1H)-one
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In 1,4-dioxane at 0 - 20℃; for 0.666667h; | 100% |
1,2,4-Triazole
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In acetonitrile at 20℃; for 0.75h; | 100% |
1,2,4-Triazole
5'-O-(4,4'-dimethoxytrityl)-3'-O-[(2-cyanoethoxy)(N,N-diisopropylamino)phosphino]-3'-deuterouridine
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In acetonitrile at 0 - 20℃; | 100% |
1,2,4-Triazole
5'-O-(4,4'-dimethoxytrityl)-3'-O-[(2-cyanoethoxy)(N,N-diisopropylamino)phosphino]-3'-deuterothymidine
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In acetonitrile at 0 - 20℃; | 100% |
1,2,4-Triazole
(4-bromomethyl-benzyl)-(2-chloro-pyrimidin-4-yl)-(2,2-dimethyl-propyl)-amine
(2-chloro-pyrimidin-4-yl)-(2,2-dimethyl-propyl)-(4-[1,2,4]triazol-1-ylmethyl-benzyl)-amine
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 16h; | 100% |
In N,N-dimethyl-formamide at 20℃; for 18h; | 85% |
1,2,4-Triazole
5'-O-levulinyl-3'-O-tert-butyldimethylsilylthymidine
4-(1,2,4-triazol-1-yl)-5'-O-levulinyl-3'-O-tert-butyldimethylsilylthymidine
Conditions | Yield |
---|---|
Stage #1: 1,2,4-Triazole With triethylamine; trichlorophosphate In acetonitrile at 0℃; for 0.75h; Stage #2: 5'-O-levulinyl-3'-O-tert-butyldimethylsilylthymidine In acetonitrile at 20℃; for 1h; Further stages.; | 100% |
1,2,4-Triazole
2-[3-bromomethyl-5-(cyanodimethylmethyl)phenyl]-2-methylpropanenitrile
anastrozol
Conditions | Yield |
---|---|
With potassium tert-butylate In toluene at 9 - 21℃; for 4.5h; | 100% |
With tetrabutylammomium bromide; potassium hydroxide In water; toluene at 75 - 80℃; for 2h; Solvent; Temperature; Reagent/catalyst; | 82% |
With tetrabutylammomium bromide; potassium carbonate; potassium hydroxide In toluene at 85 - 90℃; for 5h; | 47% |
1,2,4-Triazole
2-[4-(chloromethyl)-2-methoxyphenoxy]-6-fluoro pyridine
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 40℃; | 100% |
With sodium hydride In N,N-dimethyl-formamide at 40℃; Inert atmosphere; |
1,2,4-Triazole
cyclohexenone
3-(1H-1,2,4-triazol-1-yl)cyclohexan-1-one
Conditions | Yield |
---|---|
In water at 60℃; under 4500450 Torr; for 20h; Aza-Michael reaction; | 100% |
In water at 60℃; under 4500450 Torr; for 20h; Solvent; Pressure; Reagent/catalyst; Concentration; Time; | 100% |
With toluene-4-sulfonic acid In neat (no solvent) at 60℃; for 0.5h; Michael Addition; Irradiation; Green chemistry; | 99% |
With poly(N-vinylimidazole) In water at 20 - 25℃; for 24h; aza-Michael reaction; Inert atmosphere; | 92% |
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In acetonitrile at 23℃; for 6h; Michael Addition; | 91% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 60℃; for 20h; | 100% |
With sodium hydrogencarbonate In toluene at 110 - 120℃; for 3h; Inert atmosphere; | 22.2% |
1,2,4-Triazole
5-bromo-3',5'-diacetyl-2'-fluoro-2'-deoxyuridine
C15H15BrFN5O6
Conditions | Yield |
---|---|
Stage #1: 1,2,4-Triazole With trichlorophosphate In acetonitrile at 0℃; for 0.333333h; Stage #2: 5-bromo-3',5'-diacetyl-2'-fluoro-2'-deoxyuridine In acetonitrile at 0 - 20℃; Stage #3: With triethylamine In water; acetonitrile for 0.5h; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In methanol; acetonitrile at 40℃; for 72h; | 100% |
1,2,4-Triazole
ethyl 2-(5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)acetate
1-(ethoxycarbonylmethyl)-4-(1,2,4-triazolyl)thymine
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In acetonitrile at 20℃; for 3h; | 100% |
With triethylamine; trichlorophosphate In dichloromethane; acetonitrile at 0 - 23℃; for 21h; Inert atmosphere; | 89% |
1,2,4-Triazole
N1-tert-butyloxycarbonylmethylthymine
1-(tert-butoxycarbonylmethyl)-4-(1,2,4-triazolyl)thymine
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In acetonitrile at 20℃; for 3h; | 100% |
1,2,4-Triazole
Conditions | Yield |
---|---|
Stage #1: 1,2,4-Triazole With triethylamine; trichlorophosphate In acetonitrile at 0 - 20℃; for 0.416667h; Stage #2: 5-(2-fluorophenyl)-7-methylimidazo[5,1-f][1,2,4]triazin-4(3H)-one In acetonitrile at 20℃; for 2h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 1,2,4-Triazole; phosgene With dmap In dichloromethane; toluene at 25℃; for 1h; Inert atmosphere; Stage #2: piperidine In dichloromethane; toluene at 25℃; for 12h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With pyridine at 90℃; | 100% |
1,2,4-Triazole
2-amino-4-chloro-5,6,7,8-tetrahydro<1>benzothieno<2,3-d>pyrimidine
Conditions | Yield |
---|---|
With pyridine at 90℃; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetone at 80℃; for 72h; | 100% |
1,2,4-Triazole
Conditions | Yield |
---|---|
Stage #1: 1,2,4-Triazole With triethylamine In dichloromethane; acetonitrile at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: With trichlorophosphate In dichloromethane; acetonitrile at 0℃; for 0.5h; Inert atmosphere; Stage #3: 1-(3-O-acetyl-2,5,6-trideoxy-β-D-erythro-hex-5-ynofuranosyl)-5-methyluraciI In dichloromethane; acetonitrile at 20℃; for 1h; | 100% |
Stage #1: 1,2,4-Triazole With triethylamine; trichlorophosphate In dichloromethane; acetonitrile at 0℃; for 0.5h; Stage #2: 1-(3-O-acetyl-2,5,6-trideoxy-β-D-erythro-hex-5-ynofuranosyl)-5-methyluraciI In dichloromethane; acetonitrile at 20℃; for 1h; |
Conditions | Yield |
---|---|
With triethylamine for 2.5h; Heating; | 99% |
With triethylamine for 2h; Heating; | 98.5% |
In tetrahydrofuran; water at 20℃; | 96% |
1,2,4-Triazole
1-((6aR,8R,9aS)-2,2,4,4-tetraisopropyl-9-methylenetetrahydro-6H-furo[3,2-f][1,3,5,2,4]trioxadisilocin-8-yl)-pyrimidine-2,4(1H,3H)-dione
1-<3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-2-deoxy-2-methylidene-β-D-ribofuranosyl>-4-(1,2,4-triazol-1-yl)-1H-pyrimidin-2-one
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In acetonitrile for 2h; Ambient temperature; | 99% |
With pyridine; 4-chlorophenylphosphorodichloridate for 48h; Ambient temperature; | 77% |
1,2,4-Triazole
1-((2R,5R)-4-((tert-butyldimethylsilyl)oxy)-5-((tert-butyldimethylsilyl)oxy)tetrahydrofuran-2-yl)pyrimidine-2,4 (1H,3H)-dione
1-[(2R,4S,5R)-4-(tert-Butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-3-methylene-tetrahydro-furan-2-yl]-4-[1,2,4]triazol-1-yl-1H-pyrimidin-2-one
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In acetonitrile for 2h; Ambient temperature; | 99% |
1,2,4-Triazole
1-<2,5-bis-O-(tert-butyldimethylsilyl)-3-deoxy-3-methylene-β-D-erythro-pentofuranosyl>uracil
1-<2,5-bis-O-(tert-butyldimethylsilyl)-3-deoxy-3-methylene-β-D-erythro-pentofuranosyl>-4-(1,2,4-triazol-1-yl)pyrimidin-2(1H)-one
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In acetonitrile for 2h; Ambient temperature; | 99% |
1,2,4-Triazole
Ethylchlor<4-(3-chlorphenyl)-piperazin-1-ylamido>phosphat
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 40℃; | 99% |
1,2,4-Triazole
Ethylchlor<4-(2-chlorphenyl)-piperazin-1-ylamido>phosphat
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 40℃; | 99% |
1,2,4-Triazole
Ethylchlor<<2-(2,6-dichlorphenoxy)-ethyl>-propylamido>phosphat
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 40℃; | 99% |
1,2,4-Triazole
1-[3,5-di-O-acetyl-2-deoxy-4-thio-β-D-ribofuranosyl]uracil
4-(1,2,4-triazol-1-yl)-1-(3,5-di-O-acetyl-2-deoxy-4-thio-β-D-erythro-pentofuranosyl)pyrimidin-2(1H)-one
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In acetonitrile | 99% |
1,2,4-Triazole
N,N-tert-butoxycarbonyldehydroalanine
Boc-Ala[N-Boc-β-(1,2,4-triazol-1-yl)]-OMe
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile Ambient temperature; | 99% |
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