As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c
Cas:2067-33-6
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inquiryProduct description: Product name 5-Bromovaleric acid CAS number 2067-33-6 Assay ≥99% Appearance Off-white to yellowish crystal Capacity 200mt/year Application Pharmaceutical
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inquiryHigh quality 5-Bromovaleric acid CAS 2067-33-6 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed add
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Founded in 2008, East Chemsources Limited is a professional manufacturer and supplier in food and chemical field in China. Through more than ten years development, our company has developed from single product at first to provide solution to final
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inquiryAbout Product Technical Details 5-Bromovaleric acid Chemical Properties Melting point 38-40 °
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryProduct Name: 5-Bromovaleric acid Synonyms: 5-bromo-pentanoicaci;delta-Bromovaleric acid;Pentanoic acid, 5-bromo-;5-BROMOVALERIC ACID;5-BROMO-N-VALERIC ACID;5-BROMOPENTANOIC ACID;RARECHEM AL BO 0181;5-Bromo-n-pentanoic acid CAS: 2067-33-6 MF: C5H9BrO
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inquiryAppearance:Yellowish to light brown crystals or cryst. powder Storage:Room temperature Package:25kg/drum Application:Intermediate Transportation:Express/Sea/Air Port:Any port in china
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inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
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inquiry5-Bromovaleric acid CAS:2067-33-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:As
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; oxygen In acetonitrile at 30℃; for 3h; Schlenk technique; | 95% |
With N-hydroxyphthalimide; oxygen In acetonitrile at 30℃; under 760.051 Torr; for 3h; Catalytic behavior; Solvent; Schlenk technique; | 95% |
5-bromopentanoic acid
Conditions | Yield |
---|---|
With sulfuric acid; sodium bromide In water at 90 - 95℃; for 8h; Temperature; Concentration; | 88.9% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; hydrogen bromide In water for 0.166667h; Microwave irradiation; | 85% |
With sulfuric acid; water; hydrogen bromide | |
With hydrogen bromide |
1,4-dioxane
3,4,5,6-tetrahydro-2H-pyran-2-one
A
5-bromopentanoic acid
B
β-(β'-bromoethoxy)ethyl 4-bromovalerate
Conditions | Yield |
---|---|
With hydrogen bromide In water 1) room temp. 1h; 2) 80 degC, 1,5h; 3) room temp. 12h; | A 64.12% B 20.24% |
3,4,5,6-tetrahydro-2H-pyran-2-one
A
5-bromopentanoic acid
B
β-(β'-bromoethoxy)ethyl 4-bromovalerate
Conditions | Yield |
---|---|
With hydrogen bromide In 1,4-dioxane; water 1) room temp. 1 h; 2) 80 deg C, 1,5 h; 3) room temp. 12 h; | A 64.12% B 20.24% |
Conditions | Yield |
---|---|
With hydrogen bromide for 17h; Heating; | 38% |
With hydrogen bromide | |
With hydrogen bromide | |
Multi-step reaction with 2 steps 1: potassium hydroxide 2: water; hydrobromic acid View Scheme | |
Multi-step reaction with 2 steps 2: water; hydrobromic acid View Scheme |
Conditions | Yield |
---|---|
With hydrogen bromide; dibenzoyl peroxide | |
With ascaridole; hexane; hydrogen bromide |
valeric acid
5-bromopentanoic acid
Conditions | Yield |
---|---|
With sulfuric acid; hydrogen bromide | |
With sulfuric acid; hydrogen bromide Cooling with ice; Heating; |
Conditions | Yield |
---|---|
With water; hydrogen bromide |
Conditions | Yield |
---|---|
With water; hydrogen bromide |
Conditions | Yield |
---|---|
With hydrogen bromide | |
(hydrolysis); |
ethyl 2-hydroxyethylpropionate
5-bromopentanoic acid
Conditions | Yield |
---|---|
With sulfuric acid; hydrogen bromide zuletzt auf dem Wasserbad; |
(4-cyano)butyl acetate
5-bromopentanoic acid
Conditions | Yield |
---|---|
With water; hydrogen bromide |
diethyl 2-(3-bromopropane)malonate
5-bromopentanoic acid
Conditions | Yield |
---|---|
With hydrogen bromide |
Conditions | Yield |
---|---|
With hydrogen bromide |
Conditions | Yield |
---|---|
With hydrogen bromide |
Conditions | Yield |
---|---|
With dihydrogen peroxide Behandeln des Reaktionsprodukts in Aether mit einer aus Kupfer(I)-chlorid (oder Eisen(II)-sulfat) und wss.Bromwasserstoffsaeure bereiteten Loesung; | |
Multi-step reaction with 2 steps 1: 3-chloro-benzenecarboperoxoic acid / chloroform / Reflux 2: hydrogen bromide; sodium bromide; sulfuric acid / 85 - 90 °C View Scheme |
ethyl 5-bromovalerate
5-bromopentanoic acid
Conditions | Yield |
---|---|
(hydrolysis); | |
With water; lithium hydroxide In methanol at 20℃; for 0.5h; |
cyclopentanone hydroperoxide
A
5-bromopentanoic acid
C
2-bromocyclopentanone
Conditions | Yield |
---|---|
With hydrogen bromide; sodium bromide; copper(ll) bromide In water at 25℃; | A 15.0 g B 0.4 g C 0.6 g |
C17H34O2Sn
5-bromopentanoic acid
Conditions | Yield |
---|---|
With hydrogen bromide Irradiation; |
5-bromopentanoic acid
Conditions | Yield |
---|---|
With silver(I) bromide; hydrogen bromide |
5-bromopentanoic acid
Conditions | Yield |
---|---|
With hydrogen bromide at 145℃; im geschlossenen Rohr; |
pent-4-enoic acid
hexane
hydrogen bromide
5-bromopentanoic acid
ascaridole
pent-4-enoic acid
hexane
hydrogen bromide
5-bromopentanoic acid
pent-4-enoic acid
hydrogen bromide
diphenylamine
5-bromopentanoic acid
5-bromopentanoic acid
Conditions | Yield |
---|---|
With hydrogen bromide; acetic acid |
pent-4-enoic acid
hydrogen bromide
hydroquinone
5-bromopentanoic acid
pent-4-enoic acid
hydrogen bromide
toluene
5-bromopentanoic acid
pent-4-enoic acid
hydrogen bromide
dibenzoyl peroxide
5-bromopentanoic acid
5-bromopentanoic acid
5-iodopentanoic acid
Conditions | Yield |
---|---|
With potassium iodide In acetone for 6h; Heating; | 100% |
With acetone; sodium iodide | |
Multi-step reaction with 2 steps 1: KHS 2: hydriodic acid View Scheme |
Conditions | Yield |
---|---|
With thionyl chloride | 100% |
With oxalyl dichloride In benzene at 20 - 50℃; Inert atmosphere; | 98% |
With oxalyl dichloride In benzene at 50℃; for 3h; | 97% |
1-[5-(aminomethyl)-2-nitrophenyl]ethanol
5-bromopentanoic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 0.166667h; | 100% |
Conditions | Yield |
---|---|
With acetyl chloride for 5h; Reflux; | 99% |
With hydroxy-substituted sulfonic acid-functionalized silica (HO-SAS) at 110℃; Fischer-Speier Esterification; Flow reactor; | 99% |
With acetyl chloride for 5h; Reflux; | 99% |
5-bromopentanoic acid
(3R,5R)-1-benzyl-5-(hydroxydiphenylmethyl)pyrrolidin-3-yl 5-bromopentanoate
Conditions | Yield |
---|---|
Stage #1: 5-bromopentanoic acid With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 0.166667h; Stage #2: (3R,5R)-1-benzyl-5-(hydroxydiphenylmethyl)pyrrolidin-3-ol In dichloromethane at 0℃; for 1.5h; Reflux; | 99% |
Conditions | Yield |
---|---|
With sulfuric acid at 20℃; for 5h; Addition; | 98% |
With sulfuric acid In dichloromethane for 48h; Ambient temperature; | 96% |
With sulfuric acid at 20℃; for 120h; autoclave; | 72% |
5-bromopentanoic acid
5-bromopentanamide
Conditions | Yield |
---|---|
Stage #1: 5-bromopentanoic acid With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide at 0 - 40℃; for 2h; Stage #2: With ammonium hydroxide In tetrahydrofuran at 20℃; for 2h; | 98% |
Multi-step reaction with 2 steps 1: SOCl2 / 4 h / Heating 2: 28percent NH4OH / H2O / 0.75 h / 0 °C View Scheme |
Conditions | Yield |
---|---|
Stage #1: 5-bromopentanoic acid; (3Z,13Z)-7-[(3Z)-hex-3-en-1-yl]-10-[(3Z)-non-3-en-1-yl]nonadeca-3,13-dien-9-ol With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 30℃; for 18h; Stage #2: 2-(N,N-dimethylamino)ethanol In dichloromethane at 80℃; for 5h; Sealed tube; | 98% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; Schlenk technique; Inert atmosphere; | 98% |
5-bromopentanoic acid
(3R,5S)-1-benzyl-5-[bis(3,5-dimethylphenyl)(hydroxy)methyl]pyrrolidin-3-ol
{(3R,5S)-1-benzyl-5-[bis(3,5-dimethylphenyl)(hydroxy)methyl]pyrrolidin-3-yl} 5-bromopentanoate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 1.66667h; Reflux; | 97% |
5-bromopentanoic acid
5-(nitrooxy)pentanoic acid
Conditions | Yield |
---|---|
With silver nitrate In acetonitrile at 70℃; for 16h; | 96.18% |
With silver nitrate In acetonitrile at 20℃; for 48h; | 89% |
With silver nitrate In acetonitrile at 70℃; for 2h; Darkness; Inert atmosphere; | 77% |
Conditions | Yield |
---|---|
With potassium fluoride; tetra(n-butyl)ammonium hydrogensulfate In tetrahydrofuran at 20℃; for 5h; | 96% |
With Amberlyst A26 (hydrogen carbonate form) 1.) aq. MeOH, 20 deg C, 18 h, 2.) THF, reflux, 18 h; Yield given. Multistep reaction; | |
With potassium carbonate In water; dimethyl sulfoxide at 50℃; Rate constant; | |
With 2,3,3-trimethylbenzo[e]indole; potassium iodide In acetonitrile at 80 - 85℃; for 96h; |
5-bromopentanoic acid
triphenylphosphine
(4-carboxybutyl)triphenylphosphonium bromide
Conditions | Yield |
---|---|
In acetonitrile at 80℃; for 24h; | 96% |
In acetonitrile for 24h; Heating; | 92% |
In toluene for 48h; Inert atmosphere; Reflux; | 88% |
diazomethane
5-bromopentanoic acid
5-bromovaleric acid methyl ester
Conditions | Yield |
---|---|
In diethyl ether for 3h; | 96% |
In diethyl ether |
5-bromopentanoic acid
5-bromopentan-1-ol
Conditions | Yield |
---|---|
With dimethylsulfide borane complex | 96% |
With lithium aluminium tetrahydride; sulfuric acid In tetrahydrofuran for 0.25h; T < 2 deg C; Yield given; | |
With dimethylsulfide; borane | |
With diphenylsilane; triphenylphosphine; chloro(1,5-cyclooctadiene)rhodium(I) dimer In tetrahydrofuran at 20℃; for 48h; | 63 % Spectr. |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Reflux; Dean-Stark; | 96% |
With 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide | 95% |
Stage #1: 5-bromopentanoic acid With 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide In dichloromethane at 20℃; for 2h; Stage #2: benzyl alcohol In dichloromethane | 95% |
5-bromopentanoic acid
(2S,4R)-4-hydroxy-2-(1-hydroxy-1,1-diphenylmethyl)pyrroline-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 1.5h; Reflux; | 96% |
5-bromopentanoic acid
Conditions | Yield |
---|---|
With dmap; copper diacetate In acetonitrile at 80℃; for 0.416667h; Schlenk technique; Sealed tube; | 96% |
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane at 20 - 22℃; for 45h; | 95% |
sulfuric acid In toluene for 1.5h; Heating; | 88.5% |
With sulfuric acid | 87% |
endo-N-hydroxy-5-norbornene-2,3-dicarboxyimide
5-bromopentanoic acid
N-hydroxy-5-norbornene-2,3-dicarboximide bromopentanoate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide | 95% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 16h; |
5-bromopentanoic acid
(3R,5S)-1-benzyl-5-[bis(3,5-bis(trifluoromethyl)phenyl)(hydroxy)methyl]pyrrolidin-3-ol
{(3R,5S)-1-benzyl-5-[bis(3,5-bis(trifluoromethyl)phenyl)(hydroxy)methyl]pyrrolidin-3-yl} 5-bromopentanoate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 1.66667h; Reflux; | 95% |
Conditions | Yield |
---|---|
Stage #1: 5-bromopentanoic acid With 1-methyl-pyrrolidin-2-one; tert-butylmagnesium chloride In tetrahydrofuran at -78℃; for 0.166667h; Inert atmosphere; Stage #2: n-octylmagnesium chloride With buta-1,3-diene; nickel dichloride In tetrahydrofuran under 760.051 Torr; for 1h; Inert atmosphere; Cooling with ice; | 95% |
Conditions | Yield |
---|---|
With trifluoroacetic anhydride; Duolite ES 467 H+ phosphonic resin In nitromethane at 25℃; for 0.5h; | 94% |
5-bromopentanoic acid
5-mercaptopentanoic acid
Conditions | Yield |
---|---|
Stage #1: 5-bromopentanoic acid With thiourea In ethanol at 80℃; for 20h; Stage #2: With sodium hydroxide at 90℃; for 16h; | 94% |
Stage #1: 5-bromopentanoic acid With thiourea In ethanol for 20h; Reflux; Stage #2: With sodium hydroxide In water at 90℃; for 16h; Inert atmosphere; Stage #3: With sulfuric acid In water Cooling with ice; Inert atmosphere; | 87% |
Stage #1: 5-bromopentanoic acid With thiourea In ethanol for 16h; Heating; Stage #2: With sodium hydroxide for 6h; Heating; | 82% |
5-bromopentanoic acid
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 1.16667h; | 94% |
5-bromopentanoic acid
(2R)-(-)-2-phenyl-2-(piperidin-1-yl)ethanol
Conditions | Yield |
---|---|
Stage #1: (2R)-(-)-2-phenyl-2-(piperidin-1-yl)ethanol With methanesulfonyl chloride; triethylamine In chloroform at 0 - 5℃; for 0.5h; Stage #2: 5-bromopentanoic acid With triethylamine In chloroform at 5 - 20℃; for 16h; enantiospecific reaction; | 94% |
5-bromopentanoic acid
dibenzyl 5,5'-((1,4-phenylenebis(azanediyl))bis(carbonyl))bis(3-hydroxypyrrolidine-1-carboxylate)
dibenzyl 5,5'-((1,4-phenylenebis(azanediyl))bis(carbonyl))bis(3-((5-bromopentanoyl)oxy)-pyrrolidine-1-carboxylate)
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 25℃; for 4h; | 93% |
5-bromopentanoic acid
N,0-dimethylhydroxylamine
5-bromo-N-methoxy-N-methylpentanamide
Conditions | Yield |
---|---|
Stage #1: 5-bromopentanoic acid; N,0-dimethylhydroxylamine In toluene at 0℃; for 0.166667h; Stage #2: With phosphorus trichloride In toluene at 20 - 60℃; for 0.5h; | 93% |
5-bromopentanoic acid
dibenzyl 5,5'-((ethane-1,2-diylbis(azanediyl))bis(carbonyl))bis(3-hydroxypyrrolidine-1-carboxylate)
dibenzyl 5,5'-((ethane-1,2-diylbis(azanediyl))bis(carbonyl))bis(3-((5-bromopentanoyl)oxy)pyrrolidine-1-carboxylate)
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 25℃; for 4h; | 92% |
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