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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph
2-[2-[2-CHLORO-3-[(1,3-DIHYDRO-3,3-DIMETHYL-1-PROPYL-2H-INDOL-2-YLIDENE)ETHYLIDENE]-1-CYCLOHEXEN-1-YL]ETHENYL]-3,3-DIMETHYL-1-PROPYLINDOLIUM IODIDE Basic information Product Name: 2-[2-[2-CHLORO-3-[(1,3-DIHYDRO-3,3-DIMETHYL-1-PROPYL-2H-INDOL-2-YL
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inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater
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We produce carbomer by our own factory,carbomer 940 is our best seller.It is used for cosmetic and medical.And we also become agent for lubrizol.Our carbomer 940 get high viscosity and good transparency.The price will depond on the market,surely supp
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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Molecular Formula C36H44ClN2.I Molecular Weight 667.11 CAS Registry Number 207399-07-3 IR-780 iodide …Appearance:white powder Storage:Sealed and stored in dry place Package:1kg. 2kg Transportation:Pack
World-class service, High quality, Low cost and Quick delivery. All made in our plant! Storage:To be stored in cool dry environment Package:1g,5g,10g or Bulk Application:Photonic and Optical Device > Near-Infrared(NIR) Dyes
2-(2-(2-Chloro-3-(-2-(3,3-dimethyl-1-propylindolin-2-ylidene)ethylidene)cyclohex-1-enyl)vinyl)-3,3-dimethyl-1-propyl-3H-indolium iodide
2-chloro-1-formyl-3-hydroxymethylenecyclohexene
2,3,3-trimethyl-1-propyl-3H-indolium iodide
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
Conditions | Yield |
---|---|
In butan-1-ol; benzene at 160℃; for 10h; Inert atmosphere; | 96% |
In butan-1-ol; benzene at 160℃; for 10h; Inert atmosphere; | 96% |
In butan-1-ol; benzene at 160℃; for 10h; Inert atmosphere; Dean-Stark; | 96% |
2,3,3-trimethyl-1-propyl-3H-indolium iodide
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
Conditions | Yield |
---|---|
With sodium acetate In ethanol at 50℃; for 1h; | 79% |
2,3,3-trimethylindoleniune
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetonitrile / 15 h / Reflux 2: butan-1-ol; benzene / 10 h / 160 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: acetonitrile / 15 h / Reflux 2: butan-1-ol; benzene / 10 h / 160 °C / Inert atmosphere; Dean-Stark View Scheme | |
Multi-step reaction with 2 steps 1: 5 h / Reflux 2: sodium acetate / ethanol / 1 h / 50 °C View Scheme |
cyclohexanone
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: trichlorophosphate / dichloromethane / 0.5 h / Inert atmosphere; cooling with ice 1.2: 3 h / 80 °C 2.1: butan-1-ol; benzene / 10 h / 160 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: trichlorophosphate / dichloromethane / 3 h / 80 °C / Inert atmosphere 2: butan-1-ol; benzene / 10 h / 160 °C / Inert atmosphere; Dean-Stark View Scheme | |
Multi-step reaction with 2 steps 1.1: trichlorophosphate / dichloromethane / 0.17 h / 0 °C 1.2: 3.2 h / Reflux 1.3: 1 h / 20 °C 2.1: sodium acetate / ethanol / 1 h / 50 °C View Scheme |
2,3,3-trimethyl-1-propyl-3H-indolium iodide
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
Conditions | Yield |
---|---|
With sodium acetate In ethanol at 120℃; for 0.333333h; Microwave irradiation; |
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
tert-butyl (4-hydroxybenzyl)carbamate
Conditions | Yield |
---|---|
With caesium carbonate In dichloromethane at 40℃; for 1h; Inert atmosphere; | 100% |
With caesium carbonate In dichloromethane at 40℃; for 1h; Inert atmosphere; | 100% |
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
Conditions | Yield |
---|---|
In ethanol; water | 96% |
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
Conditions | Yield |
---|---|
In ethanol; water | 94% |
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
Conditions | Yield |
---|---|
In ethanol; water | 93% |
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
4-mercaptobenzoic acid
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 20h; Inert atmosphere; | 92% |
In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 85% |
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
Conditions | Yield |
---|---|
In ethanol; water | 92% |
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
2-(4'-hydroxyphenyl)-1,2-benzoisoselenazol-3(2H)-one
Conditions | Yield |
---|---|
Stage #1: 2-(4'-hydroxyphenyl)-1,2-benzoisoselenazol-3(2H)-one With potassium tert-butylate In tetrahydrofuran at 15℃; for 0.5h; Inert atmosphere; Stage #2: 2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide In tetrahydrofuran at 60℃; for 5h; Reagent/catalyst; Temperature; Solvent; Inert atmosphere; | 92% |
piperazine
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
C40H53N4(1+)*I(1-)
Conditions | Yield |
---|---|
In acetonitrile at 82℃; for 4h; Inert atmosphere; | 90% |
In N,N-dimethyl-formamide at 85℃; for 4h; | 86% |
In N,N-dimethyl-formamide at 85℃; for 4h; Inert atmosphere; | 85% |
piperazine
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
C40H53N4(1+)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 80℃; for 4h; | 87.4% |
In N,N-dimethyl-formamide at 85℃; for 4h; Inert atmosphere; |
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
ethylamine
C38H50N3(1+)*I(1-)
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 80℃; for 0.333333h; | 87% |
With triethylamine In acetonitrile at 80℃; |
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
thiophenol
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 25℃; for 10h; Inert atmosphere; Schlenk technique; | 87% |
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
Conditions | Yield |
---|---|
With sodium hydroxide In water | 87% |
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
4-Chlororesorcinol
Conditions | Yield |
---|---|
Stage #1: 4-Chlororesorcinol With triethylamine In N,N-dimethyl-formamide at 20℃; for 0.166667h; Inert atmosphere; Stage #2: 2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide In N,N-dimethyl-formamide at 75℃; for 6h; Inert atmosphere; | 86.9% |
2-(aminoethyl)pyridine
2-[2-[2-chloro-3-[(1,3-dihydro-3,3-dimethyl-1-propyl-2H-indolyl-2-ylidenyl)ethylidenyl]-1-cyclohexen-1-yl]ethenyl]-3,3-dimethyl-1-propylindolium iodide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 80℃; for 0.333333h; | 85% |
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