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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry4-Methoxyphenacyl chloride CAS:2196-99-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiry4-Methoxyphenacyl chloride Basic information Product Name: 4-Methoxyphenacyl chloride Synonyms: 2-CHLORO-1-(4-METHOXYPHENYL)ETHANONE;2-CHLORO-4'-METHOXYACETOPHENONE;2-CHLORO-4'-METHOXYLPHACETONE;4-METHOXYPHENACYL CHLORIDE;ALPHA-CHLORO-4-METH
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryProduct name: 2-chloro-4-methoxyacetophenone. Synonym:2-CHLORO-1-(4-METHOXYPHENYL)ETHANONE;2-CHLORO-4'-METHOXYACETOPHENONE;2-CHLORO-4'-METHOXYLPHACETONE;4-METHOXYPHENACYLCHLORIDE;ALPHA-CHLORO-4-METHOXYACETChemicalbookOPHENONE;Ethanone,2-c
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
N-methyl-N-nitrosotoluene-p-sulfonamide
4-methoxy-benzoyl chloride
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
Stage #1: N-methyl-N-nitrosotoluene-p-sulfonamide With potassium hydroxide In methanol; water; N,N-dimethyl-formamide Flow reactor; Stage #2: 4-methoxy-benzoyl chloride In methanol; diethyl ether; water; N,N-dimethyl-formamide at 0 - 30℃; for 1.5h; Sonication; Stage #3: With hydrogenchloride In methanol; diethyl ether; water; N,N-dimethyl-formamide for 1h; | 99% |
Conditions | Yield |
---|---|
With hydrogenchloride; ammonium nitrate; iodine; oxygen In water; acetonitrile at 60℃; for 72h; Solvent; Green chemistry; Large scale; chemoselective reaction; | 98% |
With N,N,N-trimethylbenzenemethanaminium dichloroiodate In methanol; 1,2-dichloro-ethane for 5h; Heating; | 97% |
With 1,3-dichloro-5,5-dimethylhydantoin; toluene-4-sulfonic acid In methanol at 30 - 35℃; for 8h; | 94% |
4-(2-chloroethynyl)anisole
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With tetrafluoroboric acid; water In 2,2,2-trifluoroethanol at 80℃; for 10h; | 95% |
2,2,2-trichloro-1-(4-methoxyphenyl)ethan-1-ol
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; copper(l) chloride In 1,2-dichloro-ethane for 3h; Heating; | 90% |
Multi-step reaction with 4 steps 1: 90 percent / NaH / tetrahydrofuran / 1 h / 0 °C 2: 0.2M ammonium nitrate / methanol; H2O / cathodic reduction 3: 5M KOH / ethanol / Heating 4: cond. H2SO4 / H2O; dioxane / 3 h / Ambient temperature View Scheme |
4-methoxyphenylboronic acid
chloroacetyl chloride
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With potassium carbonate In toluene at 20℃; for 2h; Suzuki-Miyaura Coupling; Inert atmosphere; | 88% |
With mono(1-benzyl-3-(1-benzyl-1-methylpyrrolidin-1-ium-2-yl)pyridin-1-ium)monopalladium(II) tetrachloride; potassium carbonate In chloroform at 20℃; for 0.75h; | 91 %Chromat. |
[1-(4-methoxyphenyl)vinyloxy]trimethylsilane
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With tris(triphenylphosphine)ruthenium(II) chloride; trifluoromethane sulfonyl chloride In benzene at 120℃; for 7h; | 85% |
Trichloromethanesulfonyl chloride
[1-(4-methoxyphenyl)vinyloxy]trimethylsilane
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With ruthenium(II) In benzene at 120℃; for 7h; sealed; | 80% |
methoxybenzene
chloroacetyl chloride
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane for 2h; Ambient temperature; | 78.5% |
With carbon disulfide; aluminium trichloride | |
With carbon disulfide; aluminium trichloride |
Conditions | Yield |
---|---|
With hydrogenchloride; iodine In dimethyl sulfoxide at 20℃; for 16h; | 76% |
Conditions | Yield |
---|---|
With magnesium(II) chloride hexahydrate; oxygen; lithium perchlorate; manganese(ll) chloride In dichloromethane; acetone at 40℃; for 40h; Electrochemical reaction; | 71% |
With magnesium(II) chloride hexahydrate; cobalt(II) chloride hexahydrate; sulfuric acid; oxygen; lithium perchlorate In dichloromethane; acetone at 40℃; for 12h; Electrolysis; Sealed tube; chemoselective reaction; | 65% |
With iron(III) chloride; potassium chloride; oxygen; toluene-4-sulfonic acid In tert-butyl methyl ether at 20℃; Irradiation; Green chemistry; | 43% |
Multi-step reaction with 3 steps 1: thionyl chloride / chloroform / 20 °C 2: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / water / 24 h / 70 °C 3: iron(III) trifluoromethanesulfonate; 2-((4R,5R)-1-((4-(tert-butyl)phenyl)sulfonyl)-4,5-diphenylimidazolidin-2-yl)-6-((4R,5R)-1-((4-(tert-butyl)phenyl)sulfonyl)-4,5-diphenylimidazolidin-2-yl)pyridine; oxygen / 1,2-dichloro-ethane / 16 h / 75 °C / 760.05 Torr / Green chemistry View Scheme |
methoxybenzene
chloroacetic acid
A
2-chloro-1-(2-methoxy-phenyl)-ethanone
B
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With P2O5/silica gel In 1,2-dichloro-ethane for 3h; Friedel Crafts acylation; Reflux; | A 12 %Spectr. B 70% |
1-(1-chloroethenyl)-4-methoxybenzene
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With iron(III) trifluoromethanesulfonate; 2-((4R,5R)-1-((4-(tert-butyl)phenyl)sulfonyl)-4,5-diphenylimidazolidin-2-yl)-6-((4R,5R)-1-((4-(tert-butyl)phenyl)sulfonyl)-4,5-diphenylimidazolidin-2-yl)pyridine; oxygen In 1,2-dichloro-ethane at 75℃; under 760.051 Torr; for 16h; Solvent; Green chemistry; chemoselective reaction; | 70% |
Conditions | Yield |
---|---|
With iron(III) chloride; silica gel In dichloromethane at 20℃; for 0.166667h; | 65% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid for 264h; Ambient temperature; | 63% |
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With hydrogenchloride; ethanol In 1,2-dichloro-ethane at 20℃; | 62% |
2-chloro-1-(4-methoxyphenyl)-2-(phenylsulfinyl)-1-ethanone
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With ethylmagnesium bromide In tetrahydrofuran at -70 - -40℃; for 2h; | 60% |
2,2,2-trichloro-1-(4-methoxyphenyl)ethan-1-one
B
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; copper(l) chloride In 1,2-dichloro-ethane; benzene for 1h; Inert atmosphere; Schlenk technique; Reflux; diastereoselective reaction; | A 60% B 18% |
Conditions | Yield |
---|---|
Stage #1: 4-Methoxystyrene; N-chloro-N-fluoro-benzenesulfonamide In dichloromethane at 35℃; for 12h; Stage #2: With triethylamine In dichloromethane at 35℃; for 1h; | A 48% B 38% |
1-(4-methoxyphenyl)ethanone
A
2-chloro-1-(3-chloro-4-methoxyphenyl)-ethanone
B
4-acetyl-2-chloroanisole
C
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With aluminum oxide; sodium chlorite; manganese(III) acetylacetonate In dichloromethane at 20℃; for 3.16667h; | A 25% B 22% C 30% |
With chlorine In acetic acid for 0.5h; Ambient temperature; | A 14% B 19% C 29% |
1-(4-methoxyphenyl)ethanone
A
2,2-dichloro-4'-methoxyacetophenone
B
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With hydrogenchloride; potassium permanganate In acetonitrile at 60℃; | A 16% B 28% |
With aluminum (III) chloride; oxygen; vanadium(V) oxytriisopropoxide; tetra-(n-butyl)ammonium iodide In acetonitrile at 80℃; for 24h; | A 13 %Spectr. B 44 %Spectr. |
2-chloro-1,3-bis(4′-methoxy-phenyl)-1,3-propanedione
A
1,3-bis(4'-methoxyphenyl)propane-1,3-dione
B
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
Stage #1: 2-chloro-1,3-bis(4′-methoxy-phenyl)-1,3-propanedione With [Cu(tris(2-pyridylmethyl)amine)(CH3CN)](ClO4)2; lithium hexamethyldisilazane In diethyl ether; acetonitrile for 48h; Inert atmosphere; Glovebox; Stage #2: With water In diethyl ether; acetonitrile | A n/a B 28% |
diazomethane
p-hydroxyphenacyl chloride
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With methanol; diethyl ether |
diazomethane
4-methoxy-benzoyl chloride
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With diethyl ether |
methoxybenzene
chloroacetyl chloride
A
2-chloro-1,1-bis-(4-methoxy-phenyl)-ethene
B
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With aluminium trichloride at 20℃; |
methoxybenzene
chloroacetyl chloride
A
2-chloro-1-(2-methoxy-phenyl)-ethanone
B
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With carbon disulfide; aluminium trichloride in der Kaelte; | |
With iron(III) oxide at 20℃; for 0.25h; Friedel Crafts acylation; regioselective reaction; |
triphenylacetic acid
methoxybenzene
Chloroacetic anhydride
A
(4-methoxyphenyl)triphenylmethane
B
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
at 150 - 155℃; |
4-Methoxystyrene
A
Z-1-(2-chloroethenyl)phenyl methyl ether
B
1-[(E)-2-chlorovinyl]-4-methoxybenzene
C
4-methoxy-benzaldehyde
D
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With chlorine dioxide In tetrachloromethane at 52 - 54℃; for 1.16667h; Further byproducts given. Title compound not separated from byproducts; | A 4.2 % Chromat. B 14.1 % Chromat. C 1.5 % Chromat. D 33.7 % Chromat. |
With chlorine dioxide In tetrachloromethane at 52 - 54℃; for 1.16667h; Further byproducts given; | A 4.2 % Chromat. B 14.1 % Chromat. C 1.5 % Chromat. D 33.7 % Chromat. |
4-Methoxystyrene
A
Z-1-(2-chloroethenyl)phenyl methyl ether
B
1-[(E)-2-chlorovinyl]-4-methoxybenzene
C
4-methoxybenzoic acid
D
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With chlorine dioxide In tetrachloromethane at 52 - 54℃; for 1.16667h; Further byproducts given; | A 4.2 % Chromat. B 14.1 % Chromat. C 1.2 % Chromat. D 33.7 % Chromat. |
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With sulfuric acid In 1,4-dioxane; water for 3h; Ambient temperature; Yield given; |
2-nitro-benzaldehyde
2-chloro-1-(4-methoxyphenyl)ethanone
trans-(4-methoxyphenyl)(3-(2-nitrophenyl)oxiran-2-yl)methanone
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 20℃; for 0.5h; Darzens Condensation; stereoselective reaction; | 100% |
With methanol; sodium at 20℃; for 0.25h; Darzens Condensation; |
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; f-amphox; hydrogen; potassium carbonate In ethanol; hexane at 25 - 30℃; under 60804.1 Torr; for 48h; Pressure; Inert atmosphere; Glovebox; Autoclave; enantioselective reaction; | 99% |
With potassium tert-butylate; isopropyl alcohol; chloro[(1R,2R)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine] (pentamethylcyclopentadienyl) rhodium at 25℃; | 96% |
With borane-THF; potassium hydroxide; (S)-Corey-Bakshi-Shibata oxazaborolidine In diethyl ether; water at -30℃; | |
With (R)-alcohol dehydrogenase from Lactobacillus kefir DSM 20587 In aq. buffer at 30℃; for 12h; pH=7; Enzymatic reaction; stereoselective reaction; | n/a |
With nicotinamide adenine dinucleotide phosphate; isopropyl alcohol In dimethyl sulfoxide at 30℃; for 24h; pH=7.5; Enzymatic reaction; enantioselective reaction; | n/a |
5-(4-methylphenyl)-4-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione
2-chloro-1-(4-methoxyphenyl)ethanone
1-(4-methoxyphenyl)-2-{[5-(4-methylphenyl)-4-phenyl-4H-1,2,4-triazol-3-yl]thio}ethanone
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 2h; Heating / reflux; | 99% |
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With formic acid; C31H33N2O3RuS; potassium formate In water; ethyl acetate at 60℃; for 4h; Inert atmosphere; enantioselective reaction; | 98% |
With sodium perchlorate; hydrogen; chloro[(1S,2S)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine]-(mesitylene) ruthenium (II) In methanol at 30℃; under 76005.1 Torr; for 24h; Product distribution / selectivity; | 93% |
With nicotinamide adenine dinucleotide phosphate; isopropyl alcohol In dimethyl sulfoxide at 30℃; for 24h; pH=7.5; Reagent/catalyst; Enzymatic reaction; enantioselective reaction; | 90% |
With glucose; glucose dehydrogenase from Bacillus subtilis CGMCC 1.1398; medium-chain dehydrogenase from Kuraishia capsulate CBS1993; NAD In aq. phosphate buffer for 16h; pH=7.0; Enzymatic reaction; enantioselective reaction; | n/a |
2-chloro-1-(4-methoxyphenyl)ethanone
(4-methoxyphenyl)(4-(4-methoxyphenyl)-1H-imidazol-2-yl)methanone
Conditions | Yield |
---|---|
With sodium azide; choline chloride; glycerol at 80℃; for 4h; Green chemistry; | 98% |
3-methoxybenzenethiol
2-chloro-1-(4-methoxyphenyl)ethanone
α-(3-methoxyphenyl-thio)-4-methoxyacetophenone
Conditions | Yield |
---|---|
Stage #1: 3-methoxybenzenethiol With sodium methylate In methanol at 35℃; Stage #2: 2-chloro-1-(4-methoxyphenyl)ethanone In methanol at 0 - 35℃; for 1.16667h; | 97.4% |
4-phenyl-5-(pyridin-4-yl)-2,4-dihydro-3H-1,2,4-triazole-3-thione
2-chloro-1-(4-methoxyphenyl)ethanone
1-(4-methoxyphenyl)-2-[(4-phenyl-5-pyridin-4-yl-4H-1,2,4-triazol-3-yl)thio]ethanone
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 3h; Heating / reflux; | 97% |
2-chloro-1-(4-methoxyphenyl)ethanone
(+/-)-1-chloro-2-hydroxy-2-(p-methoxyphenyl)ethane
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol at 2℃; | 96.2% |
95.9% | |
With formic acid; 4-methoxy-N-(1-(naphthalen-2-yl)ethylidene)aniline; sodium formate In water at 80℃; for 18h; pH=4.5; Inert atmosphere; chemoselective reaction; | 92% |
potassium acetate
2-chloro-1-(4-methoxyphenyl)ethanone
p-methoxyphenacyl acetate
Conditions | Yield |
---|---|
With [bmim]Br at 20℃; for 0.666667h; | 96% |
Conditions | Yield |
---|---|
With sodium methylate In methanol at 15℃; for 0.25h; Darzens Condensation; | 96% |
salicylaldehyde
2-chloro-1-(4-methoxyphenyl)ethanone
(1-benzofuran-2-yl)(4-methoxyphenyl)methanone
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In tetrahydrofuran at 20℃; for 0.0666667h; Rap-Stoermer reaction; | 95% |
With potassium carbonate at 100℃; for 0.416667h; Rapp-Stoermer Benzofuran Synthesis; Inert atmosphere; | 86% |
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With formic acid*triethylamine; Ru/(S,S)-DPEN/MCF In dichloromethane at 20℃; for 12h; | A 94% B n/a |
With Geotrichum sp. 38 in 5percent glucose In dimethyl sulfoxide at 30℃; for 17h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With dimethylsulfide borane complex; (S)-chiral pyrrolidine-based ionic liquid In toluene Heating; Title compound not separated from byproducts; |
4-methoxybenzoic acid hydrazide
2-chloro-1-(4-methoxyphenyl)ethanone
3,6-bis(4-methoxyphenyl)-1,2,4-triazine
Conditions | Yield |
---|---|
With ammonium propionate; propionic acid In 1-methyl-pyrrolidin-2-one at 190℃; for 36h; | 94% |
Conditions | Yield |
---|---|
With bismuth(III) chloride; sodium tetrahydroborate; sodium iodide In acetone Ambient temperature; | 93.3% |
With triphenyl phosphite; sodium hydrogencarbonate; (BrBu2Te)2O In water; N,N-dimethyl-formamide at 80℃; for 5h; | 89% |
With diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; acetic acid for 1.5h; Irradiation; Inert atmosphere; | 88% |
With tris(2,2'-bipyridyl)ruthenium dichloride; 1,5-dimethoxynaphthalene; ascorbic acid In methanol; water for 15h; Inert atmosphere; Irradiation; | 81% |
5-acetyl-2,4-dimethylthiazole
thiosemicarbazide
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
at 20℃; for 0.5h; Solvent; | 93% |
5-acetyl-4-methyl-2-phenylthiazole
thiosemicarbazide
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
at 20℃; for 0.5h; Solvent; | 93% |
2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
2-chloro-1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With methanol; (S)-2-((2-hydroxy-3-(triphenylsilyl)benzyl)amino)-3-methyl-1-(pyrrolidin-1-yl)butan-1-one; zinc dimethoxide In toluene at 22℃; for 4h; Inert atmosphere; enantioselective reaction; | 93% |
1-(2-hydroxy-5-nitrophenyl)ethanone
2-chloro-1-(4-methoxyphenyl)ethanone
2-(4-methoxy benzoyl) 3-methyl 5-nitro benzofuran
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 20℃; for 4h; Solvent; Molecular sieve; Inert atmosphere; | 92.15% |
cyclohexene
2-chloro-1-(4-methoxyphenyl)ethanone
A
6-Methoxy-2,3,4,4a,10,10a-hexahydro-1H-phenanthren-9-one
B
1-(4-methoxyphenyl)ethanone
Conditions | Yield |
---|---|
With silver trifluoromethanesulfonate In benzene for 4h; Irradiation; | A 92% B n/a |
methyl magnesium iodide
2-chloro-1-(4-methoxyphenyl)ethanone
1-chloro-2-(4-methoxyphenyl)propan-2-ol
Conditions | Yield |
---|---|
In tetrahydrofuran at -78℃; for 1.5h; | 92% |
1-methyl-1,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one
2-chloro-1-(4-methoxyphenyl)ethanone
5-[2-(4-methoxyphenyl)-2-oxoethyl]-1-methyl-1H-pyrazolo[3,4-d]pyrimidin-4(5H)-one
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide; acetonitrile for 7h; Reflux; | 92% |
2-amino-phenol
2-chloro-1-(4-methoxyphenyl)ethanone
3-(4-methoxyphenyl)-2H-benzo[b][1,4]oxazine
Conditions | Yield |
---|---|
With iodine; potassium carbonate In tetrahydrofuran; water at 20℃; for 7.5h; Inert atmosphere; Green chemistry; | 92% |
2-(phenylamino)pyridine
2-chloro-1-(4-methoxyphenyl)ethanone
2-(4-methoxyphenyl)-1-(pyridin-2-yl)-1H-indole
Conditions | Yield |
---|---|
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; sodium fluoride In methanol at 90℃; for 24h; | 92% |
Conditions | Yield |
---|---|
In tetrahydrofuran at -78℃; for 2.5h; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
With sodium azide In water at 20℃; for 2h; Green chemistry; | 91% |
o-hydroxyacetophenone
2-chloro-1-(4-methoxyphenyl)ethanone
(4-methoxyphenyl)-(3-methylbenzofuran-2-yl)methanone
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 20℃; for 2.5h; Solvent; Molecular sieve; Inert atmosphere; | 90.2% |
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