Products

Refine

Country

Business Type

Certificate

Display

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

Dimethyl chlorothiophosphate 2524-03-0

Cas:2524-03-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Pure Chemistry Scientific Inc.

Dimethyl chlorothiophosphate Application:823863

Dimethyl chlorothiophosphate

Cas:2524-03-0

Min.Order:1 Gram

FOB Price: $500.0

Type:Trading Company

inquiry

Synthetic route

Dimethyl phosphite
868-85-9

Dimethyl phosphite

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

Conditions
ConditionsYield
With chlorine at 20 - 740℃; Reagent/catalyst; Temperature;98.6%
O,O-dimethyl phosphorodithioic acid
756-80-9

O,O-dimethyl phosphorodithioic acid

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

Conditions
ConditionsYield
With chlorine; iron In water at 50℃; for 6h;94.3%
With chlorine at 30 - 40℃; for 3h; Temperature; Green chemistry;92.1%
With chlorine; benzene
With chlorine In tetrachloromethane at 0℃; Inert atmosphere;
With chlorine; benzene
dimethylthiophosphoric acid
1112-38-5

dimethylthiophosphoric acid

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

Conditions
ConditionsYield
With trichlorophosphate at 0 - 5℃; for 1h;93%
methanol
67-56-1

methanol

methyl phosphorodichloridothionate
2523-94-6

methyl phosphorodichloridothionate

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane; water at -5 - 5℃; for 1h; Inert atmosphere;88%
dimethyl thiophosphite
5930-72-3

dimethyl thiophosphite

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

Conditions
ConditionsYield
With sulfuryl dichloride In benzene for 0.5h;45%
methanol
67-56-1

methanol

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

Conditions
ConditionsYield
With phosphorous (V) sulfide; benzene und anschliessendes Behandeln mit Chlor;
With trichlorothiophosphine; sodium hydroxide at -10℃;
O,O,O-trimethylthiophosphate
152-18-1

O,O,O-trimethylthiophosphate

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

Conditions
ConditionsYield
With phosphorus pentachloride
dimethyl S-methyl phosphorodithioate
2953-29-9

dimethyl S-methyl phosphorodithioate

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

Conditions
ConditionsYield
With dichloromethane Irradiation;
methanol
67-56-1

methanol

A

methyl phosphorodichloridothionate
2523-94-6

methyl phosphorodichloridothionate

B

O,O,O-trimethylthiophosphate
152-18-1

O,O,O-trimethylthiophosphate

C

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

Conditions
ConditionsYield
With trichlorophosphate at 20℃; Product distribution; multistep reaction; varying of molar ratio of components; time taken in the addition of alcohol; consumption time of reactants; alcoholysis of PSCl3 (estimation of rel. rates);
sodium methylate
124-41-4

sodium methylate

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

Conditions
ConditionsYield
With trichlorothiophosphine In methanol; benzene for 3h; Ambient temperature;
O,O-dimethyl-O-(2,5-dichloro-4-cyano-phenyl)-thionophosphate
64582-42-9

O,O-dimethyl-O-(2,5-dichloro-4-cyano-phenyl)-thionophosphate

A

potassium 2,5-dichloro-4-cyano-phenolate

potassium 2,5-dichloro-4-cyano-phenolate

B

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

O,O-dimethyl phosphoramidothioate
17321-47-0

O,O-dimethyl phosphoramidothioate

Conditions
ConditionsYield
With ammonium hydroxide In dichloromethane at 0 - 44℃;99%
With ammonium hydroxide In dichloromethane at 0 - 44℃; pH=8.4 - 9.1;99%
With ammonia In dichloromethane at 5 - 10℃; for 10h; Solvent; Temperature;99.8%
dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

2-diethylamino-4-hydroxy-6-methyl-pyrimidine
42487-72-9

2-diethylamino-4-hydroxy-6-methyl-pyrimidine

Pirimiphos-methyl
29232-93-7

Pirimiphos-methyl

Conditions
ConditionsYield
Stage #1: 2-diethylamino-4-hydroxy-6-methyl-pyrimidine With potassium carbonate In water; toluene at 78 - 93℃; for 0.5h; Green chemistry;
Stage #2: dimethyl chlorothiophosphate at 20℃; Solvent; Temperature; Green chemistry;
98.6%
Stage #1: 2-diethylamino-4-hydroxy-6-methyl-pyrimidine With potassium carbonate In benzene for 3h; Reflux;
Stage #2: dimethyl chlorothiophosphate In butanone; benzene at 60 - 95℃; for 2h; Reflux;
methylamine hydrochloride
593-51-1

methylamine hydrochloride

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

N-methyl O,O-dimethyl phosphoramidothioate
31464-99-0

N-methyl O,O-dimethyl phosphoramidothioate

Conditions
ConditionsYield
In dichloromethane at 0 - 35℃; for 1h; pH=8.4 - 9.1;96%
methyl 3-hydroxybenzoate, sodium salt
51114-02-4

methyl 3-hydroxybenzoate, sodium salt

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

carbomethoxydenitrofenitrothion
142827-30-3

carbomethoxydenitrofenitrothion

Conditions
ConditionsYield
95%
dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

sodium salt of meta-hydroxybenzaldehyde
38697-17-5

sodium salt of meta-hydroxybenzaldehyde

formyldenitrofenitrothion
153174-74-4

formyldenitrofenitrothion

Conditions
ConditionsYield
95%
cefotaxime
65872-41-5

cefotaxime

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

C8H12N3O5PS2

C8H12N3O5PS2

Conditions
ConditionsYield
With tributyl-amine; triethylamine In dichloromethane at 0 - 5℃; for 3h; Inert atmosphere;95%
C8H11N2O2(1-)*Na(1+)
1445137-34-7

C8H11N2O2(1-)*Na(1+)

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

etrimfos
38260-54-7

etrimfos

Conditions
ConditionsYield
With dmap; N-benzyl-N,N,N-triethylammonium chloride; sodium dodecyl sulfate; potassium carbonate In water at 50℃; for 2.5h; pH=9.5 - 10;94.1%
dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

sodium salt of 3,5,6-trichloropyridine-2-ol

sodium salt of 3,5,6-trichloropyridine-2-ol

O,O-dimethyl O-3,5,6-trichloro-2-pyridyl phosphorothioate
5598-13-0

O,O-dimethyl O-3,5,6-trichloro-2-pyridyl phosphorothioate

Conditions
ConditionsYield
With dmap; N-benzyl-N,N,N-triethylammonium chloride; sodium dodecyl sulfate; potassium carbonate In water at 50℃; for 2.5h; pH=9.5 - 10;93.4%
dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

5-hydroxy-2-nitrobenzaldehyde, sodium salt

5-hydroxy-2-nitrobenzaldehyde, sodium salt

O,O-dimethyl O-(3-formyl-4-nitro)phenyl phosphorothioate
59417-72-0

O,O-dimethyl O-(3-formyl-4-nitro)phenyl phosphorothioate

Conditions
ConditionsYield
92%
sodium 3-methylphenoxide
3019-89-4

sodium 3-methylphenoxide

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

denitrofenitrothion
4829-03-2

denitrofenitrothion

Conditions
ConditionsYield
91%
With pyridine In toluene
N,N-dimethylammonium chloride
506-59-2

N,N-dimethylammonium chloride

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

N,N-dimethyl O,O-dimethyl phosphoramidothioate
28167-51-3

N,N-dimethyl O,O-dimethyl phosphoramidothioate

Conditions
ConditionsYield
In dichloromethane at 0 - 35℃; for 1h; pH=8.4 - 9.1;91%
With triethylamine In tetrahydrofuran 0 deg C to RT;
benzamide
55-21-0

benzamide

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

N-[dimethoxy(thio)phosphoryl]benzamide
123269-08-9

N-[dimethoxy(thio)phosphoryl]benzamide

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran90%
dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

methylamine
74-89-5

methylamine

N-methyl O,O-dimethyl phosphoramidothioate
31464-99-0

N-methyl O,O-dimethyl phosphoramidothioate

Conditions
ConditionsYield
In diethyl ether for 0.5h;87%
With triethylamine In diethyl ether
With triethylamine In benzene
dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

1-amino-2-propene
107-11-9

1-amino-2-propene

O,O-dimethyl-N-allylaminothiophosphate
36592-38-8

O,O-dimethyl-N-allylaminothiophosphate

Conditions
ConditionsYield
With triethylamine In dichloromethane Ambient temperature;87%
cyclooctylamine
5452-37-9

cyclooctylamine

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

cyclooctyl-thiophosphoramidic acid O,O'-dimethyl ester

cyclooctyl-thiophosphoramidic acid O,O'-dimethyl ester

Conditions
ConditionsYield
With aluminum oxide at 20℃;87%
dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

3-(hydroxymethyl)phenol, sodium salt
40599-33-5

3-(hydroxymethyl)phenol, sodium salt

O,O-dimethyl O-(3-hydroxymethyl)phenyl phosphorothioate

O,O-dimethyl O-(3-hydroxymethyl)phenyl phosphorothioate

Conditions
ConditionsYield
85%
dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

methylhydrazine
60-34-4

methylhydrazine

N1-dimethoxythiophosphoro-N1-methylhydrazide
80254-53-1

N1-dimethoxythiophosphoro-N1-methylhydrazide

Conditions
ConditionsYield
In chloroform for 6h; Ambient temperature;85%
cyclohexylamine
108-91-8

cyclohexylamine

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

O,o'-dimethyl-N-cyclohexyl phosphoramido thionate
941-39-9

O,o'-dimethyl-N-cyclohexyl phosphoramido thionate

Conditions
ConditionsYield
With aluminum oxide at 20℃;85%
dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

benzylamine
100-46-9

benzylamine

dimethyl N-benzylphosphoramidothionate
130012-35-0

dimethyl N-benzylphosphoramidothionate

Conditions
ConditionsYield
With triethylamine In dichloromethane for 20h; Ambient temperature;84%
With triethylamine In tetrahydrofuran 0 deg C to RT;
dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

Cyclopentamine
1003-03-8

Cyclopentamine

C7H16NO2PS

C7H16NO2PS

Conditions
ConditionsYield
With aluminum oxide at 20℃;83%
In acetonitrile for 4h;
dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

methylhydrazine
60-34-4

methylhydrazine

C5H16N2O4P2S2

C5H16N2O4P2S2

Conditions
ConditionsYield
With triethylamine In chloroform for 2h; Ambient temperature;82%
cycloheptanamine
5452-35-7

cycloheptanamine

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

C9H20NO2PS

C9H20NO2PS

Conditions
ConditionsYield
With aluminum oxide at 20℃;82%
1-bromo-3,5-di-tert-butylbenzene
22385-77-9

1-bromo-3,5-di-tert-butylbenzene

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

3, 5-di-tert-butyltoluene
15181-11-0

3, 5-di-tert-butyltoluene

Conditions
ConditionsYield
Stage #1: 1-bromo-3,5-di-tert-butylbenzene With tert.-butyl lithium In tetrahydrofuran; pentane at -78℃; for 1h;
Stage #2: dimethyl chlorothiophosphate In tetrahydrofuran; pentane at -78 - 20℃; for 4h; Further stages.;
80%
diethyl amine hydrochloride
660-68-4

diethyl amine hydrochloride

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

N,N-diethyl O,O-dimethyl phosphoramidothioate
31599-85-6

N,N-diethyl O,O-dimethyl phosphoramidothioate

Conditions
ConditionsYield
In dichloromethane at 0 - 35℃; for 1h; pH=8.4 - 9.1;80%
4-amino-5-fluoro-pyrimidin-2-ol
2022-85-7

4-amino-5-fluoro-pyrimidin-2-ol

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

O-(4-amino-5-fluoropyrimidin-2-yl) O,O-dimethyl phosphorothioate

O-(4-amino-5-fluoropyrimidin-2-yl) O,O-dimethyl phosphorothioate

Conditions
ConditionsYield
Stage #1: 4-amino-5-fluoro-pyrimidin-2-ol With sodium In N,N-dimethyl-formamide at 20℃; for 2h;
Stage #2: dimethyl chlorothiophosphate In N,N-dimethyl-formamide at 20℃; for 48h;
80%
6-(4-(trifluoromethoxy)phenylthio)-2,3,7-trimethylquinolin-4-ol

6-(4-(trifluoromethoxy)phenylthio)-2,3,7-trimethylquinolin-4-ol

dimethyl chlorothiophosphate
2524-03-0

dimethyl chlorothiophosphate

O,O-dimethyl O-2,3,7-trimethyl-6-(4-(trifluoromethoxy)phenylthio)quinolin-4-yl phosphorothioate

O,O-dimethyl O-2,3,7-trimethyl-6-(4-(trifluoromethoxy)phenylthio)quinolin-4-yl phosphorothioate

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane at 10℃; for 4h; Reflux;80%

Hot Products

Post buying leads

About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia

Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog

©2008 LookChem.com,License: ICP

NO.:Zhejiang16009103

complaints:service@lookchem.com Desktop View