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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryCAS Number 2675-89-0 Product Name 2-chloro-n,n-dimethylacetamide Synonyms 2-chloro-n,n-dimethyl Butylamine; N,n-dimethylchlo
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inquiry2-Chloro-N,N-dimethylacetamide CAS:2675-89-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality org
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Factory direct sales, accept customization. 2-Chloro-N,N-dimethylacetamide is N,M-dialkyl amide used as an organic catalyst in the preparation of phosphorylated thiosemicarbazide. Kind Pharma has its own laboratory, we can do analytical testing for
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryProduct name: 2-Chloro-N,N-Dimethyl Acetamide CAS No.: 2675-89-0 Molecule Formula:C4H8ClNO Molecule Weight:121.57 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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inquiry2-Chloro-N,N-dimethylacetamide Basic information Product Name: 2-Chloro-N,N-dimethylacetamide Synonyms: N,N-DIMETHYL-2-CHLOROACETAMIDE;N,N-DIMETHYLCHLOROACETAMIDE;N,N-DIMETHYLCHOROACETAMIDE;CHLOROACETYLDIMETHYLAMINE;AKOS BBS-00000943;2-CHLORO-N,N-DI
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Shanghai Massive Chemical Technology Co., Ltd. is engaged in development, production and marketing Specialty Chemicals to satisfy the changing needs of the chemical industry. We specialize in manufacturing high quality of Advanced Intermediates, Sp
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inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
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inquiryJinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
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inquiryR & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In toluene at -2 - 5℃; for 1h; Reagent/catalyst; Solvent; Temperature; | 93.1% |
With triethylamine In dichloromethane at -5 - 20℃; for 13h; Inert atmosphere; | 93.09% |
In diethyl ether at 20℃; Cooling; | 81% |
N,N-dimethylammonium chloride
chloroacetyl chloride
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 15℃; | 77% |
With triethylamine In dichloromethane at 0℃; for 3h; | 62% |
With sodium hydroxide In 1,2-dichloro-ethane at -5℃; for 0.5h; | 33% |
diethyl 2-amino-6-[(hydroxycarbamoyl)-methyl]-azulene-1,3-dicarboxylate sodium
B
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
A 27% B n/a |
Ketene
diethyl ether
dimethylchloroamine
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
at -60℃; |
Conditions | Yield |
---|---|
With diethyl ether at -60℃; |
bis-(dimethylamino)methane
Chloroacetic anhydride
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
In chloroform |
Dimethyl-(6-methyl-2-oxo-2λ5-[1,3,2]oxathiaphosphinan-2-yl)-amine
A
2-Chloro-6-methyl-[1,3,2]oxathiaphosphinane 2-oxide
B
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With chloroacetyl chloride Heating; |
Dimethyl-(6-methyl-2-oxo-2λ5-[1,3,2]oxathiaphosphinan-2-yl)-amine
chloroacetyl chloride
A
2-Chloro-6-methyl-[1,3,2]oxathiaphosphinane 2-oxide
B
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
Heating; |
Conditions | Yield |
---|---|
Stage #1: chloroacetic acid With dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 0.5h; Stage #2: dimethyl amine With dmap In dichloromethane at 20℃; |
Conditions | Yield |
---|---|
In tetrahydrofuran; dichloromethane at -40℃; for 1h; |
Conditions | Yield |
---|---|
With copper dichloride at 150℃; for 24h; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl acetamide With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere; Stage #2: With methyl chlorosulfate In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere; Overall yield = 99 %; Overall yield = 87 mg; |
1-benzyloxy-5-(4-methoxy-benzyloxy)-9-(tetrahydro-pyran-2-yloxy)-non-7-en-4-ol
2-chloro-N,N-dimethylacetamide
2-[1-(3-benzyloxy-propyl)-2-(4-methoxy-benzyloxy)-6-(tetrahydro-pyran-2-yloxy)-hex-4-enyloxy]-N,N-dimethyl-acetamide
Conditions | Yield |
---|---|
Stage #1: 1-benzyloxy-5-(4-methoxy-benzyloxy)-9-(tetrahydro-pyran-2-yloxy)-non-7-en-4-ol With sodium hydride In tetrahydrofuran at 0℃; for 0.166667h; Stage #2: 2-chloro-N,N-dimethylacetamide In tetrahydrofuran at 20℃; for 4h; | 100% |
1,3-dihydro-1-(1-tert-butyloxycarbonylpiperidin-4-yl)-2H-benzimidazol-2-one
2-chloro-N,N-dimethylacetamide
4-(3-dimethylcarbamoylmethyl-2-oxo-2,3-dihydro-benzimidazol-1-yl)-piperidine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide | 100% |
(4S)-3-oxo-8-[2-(8-tert-butoxycarbonyl-5,6,7,8-tetrahydroimidazo[1,2-a]-pyrimidin-2-yl)ethoxy]-2-(2,2,2-trifluoroethyl)-2,3,4,5-tetrahydro-1H-2-benzazepin-4-acetic acid
2-chloro-N,N-dimethylacetamide
(N,N-dimethylaminocarbonyl)methyl (4S)-3-oxo-8-[2-(8-tert-butoxycarbonyt-5,6,7,8-tetrahydroimidazo[1,2-a]pyrimidin-2-yl)ethoxy]-2-(2,2,2-trifluooroethyl)-2,3,4,5-tetrahydro-1H-2-benzazep in-4-acetate
Conditions | Yield |
---|---|
With potassium carbonate In water; N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 8h; Inert atmosphere; |
(6-{(pyridin-2-ylsulfonyl)[4-(thiazol-2-yl)benzyl]aminomethyl}pyridin-2-ylamino)-acetic acid
2-chloro-N,N-dimethylacetamide
[2-(dimethylamino)-2-oxoethyl] (6-{(pyridin-2-ylsulfonyl)[4-(thiazol-2-yl)benzyl]-aminomethyl} pyridin-2-ylamino)acetate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 4h; | 100% |
methyl 6-(2,6-difluoro-4-hydroxyphenyl)-5-fluoropyridine-2-carboxylate
2-chloro-N,N-dimethylacetamide
methyl 6-(4-(2-(dimethylamino)-2-oxoethoxy)-2,6-difluorophenyl)-5-fluoropicolinate
Conditions | Yield |
---|---|
Stage #1: methyl 6-(2,6-difluoro-4-hydroxyphenyl)-5-fluoropyridine-2-carboxylate With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.5h; Stage #2: 2-chloro-N,N-dimethylacetamide In N,N-dimethyl-formamide; mineral oil at 20℃; | 100% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 0.5h; | 99% |
3-[(R)-1-(4-bromo-phenyl)-1-cyclopropyl-ethyl]-5-(1H-pyrazol-4-yl)-[1,2,4]oxadiazole
2-chloro-N,N-dimethylacetamide
2-(4-{3-[(R)-1-(4-bromophenyl)-1-cyclopropylethyl]-[1,2,4]oxadiazol-5-yl}pyrazol-1-yl)-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 99% |
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine In dichloromethane at 50℃; for 12h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: (2S,3S)-(+)-1,2-epoxy-3-octanol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.166667h; Inert atmosphere; Stage #2: 2-chloro-N,N-dimethylacetamide In tetrahydrofuran; mineral oil at 0 - 20℃; for 7h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
Stage #1: C21H26N2O2 With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 0.25h; Stage #2: 2-chloro-N,N-dimethylacetamide In N,N-dimethyl-formamide; mineral oil for 1h; | 98% |
2-phenyl-6H-pyrrolo<3,2-e>benzoxazole
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With trichlorophosphate In 1,4-dioxane at 80℃; for 1h; | 97% |
(S)-(4-Methylphenyl)phenylmethanol
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 25℃; for 4h; enantioselective reaction; | 97% |
With sodium hydride In tetrahydrofuran at 0 - 20℃; for 5h; | 91% |
With sodium hydride In diethyl ether |
2-chloro-N,N-dimethylacetamide
C16H23NO4
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In N,N-dimethyl-formamide at 40℃; for 4h; | 97% |
Conditions | Yield |
---|---|
With (1-2H)-D-glucose; nicotinamide adenine dinucleotide phosphate; GDH-105 lysate; MPTLFDPIDFGPIHAKNRIVMSPLTRGRADKEAVPAPIMAEYYAQRASAGLIITEATGISREGLGWPFAPGIWSDAQVEAWKPIVAGVHAKGGKIVCQLWHMGRMVHSSVTGTQPVSSSATTAPGEVHTYEGKKPFEQARAIDAADISRILNDYENAARNAIRAGFDGVQIHAANGYLIDEFLRNGTNHRTDEYGGVPENRIRFLKEVTERVIAAIGADRTGVRLSPNGDTQGCIDSAPETVFVPAAKLLQDLGVAWLELREPGPNGTFGKTDQPKLSPQIRKVFLRPLVLNQDYTFEAAQTALAEGKADAIAFGRKFISNPDLPERFARGIALQPDDMKTWYSQGPEGYTDYPSATSGPNN In dimethyl sulfoxide for 24h; pH=9; Reagent/catalyst; Irradiation; Sealed tube; Enzymatic reaction; enantioselective reaction; | 97% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; | 96.1% |
With sodium hydride In tetrahydrofuran at 25℃; for 4h; Substitution; | 89% |
1'-[(5-chloro-1H-indol-2-yl)carbonyl]-5-fluoro-3H-spiro[2-benzofuran-1,4'-piperidin]-3-one
2-chloro-N,N-dimethylacetamide
2-{5-chloro-2-[(5-fluoro-3-oxo-1'H,3H-spiro[2-benzofuran-1,4'-piperidin]-1'-yl)carbonyl]-1H-indol-1-yl}-N,N-dimethylacetamide
Conditions | Yield |
---|---|
Stage #1: 1'-[(5-chloro-1H-indol-2-yl)carbonyl]-5-fluoro-3H-spiro[2-benzofuran-1,4'-piperidin]-3-one With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.333333h; Stage #2: 2-chloro-N,N-dimethylacetamide In N,N-dimethyl-formamide; mineral oil at 20℃; | 96% |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 3h; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran; N,N-dimethyl-formamide at 0 - 20℃; for 15h; Williamson etherification; | 96% |
5-(4-{(R)-1-cyclopropyl-1-[5-(1H-pyrazol-4-yl)-[1,2,4]oxadiazol-3-yl]ethyl}phenyl)pyrimidin-2-ylamine
2-chloro-N,N-dimethylacetamide
2-[4-(3-{(1R)-1-[4-(2-aminopyrimidin-5-yl)phenyl]-1-cyclopropylethyl}-1,2,4-oxadiazol-5-yl)-1H-pyrazol-1-yl]-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 48 - 50℃; for 0.5h; Large scale; | 95.6% |
With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 50℃; for 1h; Inert atmosphere; | 94.4% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2h; | |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2h; | 10 g |
25,26-Bis<(ethoxycarbonyl)methoxy>-27,28-dihydroxycalix<4>arene
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With caesium carbonate; sodium iodide In acetonitrile at 60℃; | 95% |
(4R,5R)-7-benzyloxy-5-(4-methoxybenzyloxy)hept-1-en-4-ol
2-chloro-N,N-dimethylacetamide
(1'R,1R)-2-{1-[3'-benzyloxy-1'-(4-methoxybenzyloxy)propyl]but-3-enyloxy}-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 3h; | 95% |
(1,4,8,11-tetraazacyclotetradec-1-yl)acetic acid ethyl ester
2-chloro-N,N-dimethylacetamide
C26H51N7O5
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 30 - 45℃; for 48h; | 95% |
2-chloro-9-cyclohexyl-7,9-dihydro-8H-purin-8-one
2-chloro-N,N-dimethylacetamide
2-(2-chloro-9-cyclohexyl-8-oxo-8,9-dihydro-7H-purin-7-yl)-N,N-dimethyl acetamide
Conditions | Yield |
---|---|
Stage #1: 2-chloro-9-cyclohexyl-7,9-dihydro-8H-purin-8-one; 2-chloro-N,N-dimethylacetamide With sodium hydride In N,N-dimethyl-formamide; mineral oil for 3.25h; Cooling with ice; Stage #2: for 3h; | 95% |
1-(benzyloxymethyl)-4-(cyanomethyl)-2-methyl-5-nitroindole
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 60℃; for 24h; | 95% |
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In N,N-dimethyl-formamide at 56℃; | 94.6% |
ephedrine
2-chloro-N,N-dimethylacetamide
(1R,2S)-2-<(β-hydroxy-α-methylphenethyl)methylamino>-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With triethylamine In benzene for 8h; Heating; | 94% |
(1R,2R)-pseudoephedrine
2-chloro-N,N-dimethylacetamide
(1R,2R)-2-<(β-hydroxy-α-methylphenethyl)methylamino>-N,N-dimethylacetamide
Conditions | Yield |
---|---|
With triethylamine In benzene for 8h; Heating; | 94% |
n-Pent-4-enyl alcohol
2-chloro-N,N-dimethylacetamide
N,N-dimethyl-2-(pent-4-enyloxy)acetamide
Conditions | Yield |
---|---|
Stage #1: n-Pent-4-enyl alcohol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; Williamson ether synthesis; Stage #2: 2-chloro-N,N-dimethylacetamide In tetrahydrofuran; mineral oil at 0 - 20℃; Williamson ether synthesis; | 94% |
Stage #1: n-Pent-4-enyl alcohol With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 1h; Williamson synthesis; Inert atmosphere; Stage #2: 2-chloro-N,N-dimethylacetamide In tetrahydrofuran; mineral oil at 20℃; for 24h; Inert atmosphere; | 94% |
4,4'-bis[5-heptafluoropropyl-4-(4-pyridyl)oxazol-2-yl]biphenyl
2-chloro-N,N-dimethylacetamide
Conditions | Yield |
---|---|
at 110℃; for 48h; Inert atmosphere; | 94% |
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