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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
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inquiryglycolaldehyde dimer
methanol
2,2-dimethoxyethanol
Conditions | Yield |
---|---|
aminopropylated Silica-Gel hydrochloride (APSG*HCl) resin for 15h; Ambient temperature; | 92% |
With hydrogenchloride at 89.84℃; for 1h; Reagent/catalyst; Time; | 72 %Chromat. |
Conditions | Yield |
---|---|
With titanium tetrachloride for 3h; Irradiation; | 68% |
methanol
D-Xylose
A
methyl xyloside
B
2,2-dimethoxyethanol
C
methyl lactate
Conditions | Yield |
---|---|
With Ti-beta zeolite at 160℃; for 2h; Microwave irradiation; | A 48% B 7% C 11% |
With Zr-beta zeolite at 160℃; for 2h; Microwave irradiation; | A 39% B 12% C 10% |
Conditions | Yield |
---|---|
With titanium tetrachloride for 3h; Irradiation; | 37% |
methanol
Glycolaldehyde
A
2,2-dimethoxyethanol
B
glycolic acid methyl ester
C
ethylene glycol
Conditions | Yield |
---|---|
tris(triphenylphosphine)ruthenium(II) chloride In 1,4-dioxane at 70℃; for 2 - 5h; Product distribution / selectivity; | A n/a B n/a C 35% |
With triethylamine; tris(triphenylphosphine)ruthenium(II) chloride In 1,4-dioxane at 70℃; for 2 - 5h; Product distribution / selectivity; | A n/a B n/a C 35% |
With potassium carbonate; tris(triphenylphosphine)ruthenium(II) chloride In 1,4-dioxane at 20℃; for 2 - 5h; Product distribution / selectivity; | A n/a B n/a C 27% |
With caesium carbonate; tris(triphenylphosphine)ruthenium(II) chloride In 1,4-dioxane at 20℃; for 2 - 5h; Product distribution / selectivity; | A n/a B n/a C 27% |
With potassium hydroxide; dichloro(pentamethylcyclopentadienyl) iridium In 1,4-dioxane at 70℃; for 2 - 5h; Product distribution / selectivity; | A n/a B n/a C 20% |
methanol
D-Xylose
A
furfural
B
2-furaldehyde dimethyl acetal
C
methyl xyloside
D
2,2-dimethoxyethanol
E
methyl lactate
Conditions | Yield |
---|---|
With Sn-beta zeolite at 160℃; for 2h; Microwave irradiation; | A n/a B n/a C 32% D 6% E 11% F 12% |
methanol
D-Xylose
A
methyl xyloside
B
2,2-dimethoxyethanol
C
methyl lactate
Conditions | Yield |
---|---|
With Sn-beta zeolite at 160℃; for 2h; Microwave irradiation; | A 30% B 6% C 17% D 11% |
2-benzyloxy-1,1-dimethoxyethane
2,2-dimethoxyethanol
Conditions | Yield |
---|---|
With diethyl ether; ammonia; sodium |
Conditions | Yield |
---|---|
With hydrogenchloride | |
With S2O82-/silicon MCM-41 at 100℃; for 3h; |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid |
Conditions | Yield |
---|---|
(i) Br2, Et2O, (ii) /BRN= 3592982/; Multistep reaction; |
Conditions | Yield |
---|---|
With tetraethylammonium tosylate anodic oxidation; |
methanol
2,2-dimethoxyethanol
Conditions | Yield |
---|---|
With titanium tetrachloride for 15h; Irradiation; Yield given; |
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid; sulfuric acid 1a) MeOH, 0 deg C, 1.5h, 1b) RT, overnight, 2) 1h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With dihydrogen peroxide; potassium hydrogencarbonate; acetonitrile; sulfuric acid 1a) MeOH, 0 deg C, 1.5h, 2) 12h, reflux, 2) MeOH, 1h, reflux; Yield given. Multistep reaction; |
methanol
Glycolaldehyde
A
2,2-dimethoxyethanol
B
glycolic acid methyl ester
Conditions | Yield |
---|---|
dichloro(pentamethylcyclopentadienyl) iridium In 1,4-dioxane at 70℃; for 2 - 5h; Product distribution / selectivity; | |
With potassium carbonate; tris(triphenylphosphine)ruthenium(II) chloride In 1,4-dioxane at 70℃; for 2 - 5h; Product distribution / selectivity; | |
With caesium carbonate; tris(triphenylphosphine)ruthenium(II) chloride In 1,4-dioxane at 70℃; for 2 - 5h; Product distribution / selectivity; | |
With potassium hydroxide; tris(triphenylphosphine)ruthenium(II) chloride In 1,4-dioxane at 70℃; for 2 - 5h; Product distribution / selectivity; | |
With sodium hydroxide; tris(triphenylphosphine)ruthenium(II) chloride In 1,4-dioxane at 70℃; for 2 - 5h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With zeotype catalyst Sn-Beta (Si/Sn = 400) In methanol at 120℃; under 15001.5 Torr; for 16h; Autoclave; Inert atmosphere; | A 5 %Chromat. B 31 %Chromat. |
D-xylose
A
2,2-dimethoxyethanol
B
methyl lactate
C
methyl 2-hydroxybut-3-enoate
Conditions | Yield |
---|---|
With zeotype catalyst Sn-Beta (Si/Sn = 400) In methanol at 160℃; under 15001.5 Torr; for 16h; Autoclave; Inert atmosphere; | A 5 %Chromat. B 42 %Chromat. C 7 %Chromat. |
D-Arabinose
A
2,2-dimethoxyethanol
B
methyl lactate
C
methyl 2-hydroxybut-3-enoate
Conditions | Yield |
---|---|
With zeotype catalyst Sn-Beta (Si/Sn = 400) In methanol at 160℃; under 15001.5 Torr; for 16h; Autoclave; Inert atmosphere; | A 6 %Chromat. B 39 %Chromat. C 8 %Chromat. |
D-ribose
A
2,2-dimethoxyethanol
B
methyl lactate
C
methyl 2-hydroxybut-3-enoate
Conditions | Yield |
---|---|
With zeotype catalyst Sn-Beta (Si/Sn = 400) In methanol at 160℃; under 15001.5 Torr; for 16h; Autoclave; Inert atmosphere; | A 5 %Chromat. B 38 %Chromat. C 8 %Chromat. |
D-lyxose
A
2,2-dimethoxyethanol
B
methyl lactate
C
methyl 2-hydroxybut-3-enoate
Conditions | Yield |
---|---|
With zeotype catalyst Sn-Beta (Si/Sn = 400) In methanol at 160℃; under 15001.5 Torr; for 16h; Autoclave; Inert atmosphere; | A 6 %Chromat. B 39 %Chromat. C 7 %Chromat. |
Glycolaldehyde
A
2,2-dimethoxyethanol
B
methyl lactate
C
methyl 2-hydroxybut-3-enoate
D
methyl 2-hydroxy-4-methoxybutanoate
Conditions | Yield |
---|---|
With zeotype catalyst Sn-Beta (Si/Sn = 400) In methanol at 120℃; under 15001.5 Torr; for 16h; Autoclave; Inert atmosphere; | A 7 %Chromat. B 10 %Chromat. C 25 %Chromat. D 19 %Chromat. |
With zeotype catalyst Sn-Beta (Si/Sn = 400) In methanol at 140℃; under 15001.5 Torr; for 16h; Autoclave; Inert atmosphere; | A 8 %Chromat. B 14 %Chromat. C 30 %Chromat. D 12 %Chromat. |
With zeotype catalyst Sn-Beta (Si/Sn = 400) In methanol at 160℃; under 15001.5 Torr; for 16h; Autoclave; Inert atmosphere; | A 7 %Chromat. B 16 %Chromat. C 27 %Chromat. D 6 %Chromat. |
Glycolaldehyde
A
2,2-dimethoxyethanol
B
methyl 2-hydroxybut-3-enoate
C
methyl 2-hydroxy-4-methoxybutanoate
Conditions | Yield |
---|---|
With zeotype catalyst Sn-Beta (Si/Sn = 400) In methanol at 100℃; under 15001.5 Torr; for 16h; Autoclave; Inert atmosphere; | A 8 %Chromat. B 13 %Chromat. C 26 %Chromat. |
glycolaldehyde dimer
methanol
A
2,2-dimethoxyethanol
B
methyl 2-hydroxy-4-methoxybutanoate
Conditions | Yield |
---|---|
With tin (IV) chloride pentahydrate at 89.84℃; for 1h; Kinetics; Reagent/catalyst; Time; | A 54 %Chromat. B 10 %Chromat. |
methanol
D-xylofuranose
A
2,2-dimethoxyethanol
B
glycolic acid methyl ester
C
methyl lactate
Conditions | Yield |
---|---|
at 240℃; under 20686.5 Torr; for 1h; Inert atmosphere; |
Conditions | Yield |
---|---|
at 240℃; under 20686.5 Torr; for 1h; Inert atmosphere; |
methanol
Glycolaldehyde
A
2,2-dimethoxyethanol
B
methyl lactate
Conditions | Yield |
---|---|
With mesoporous Zr-SBA-15 at 240℃; under 20686.5 Torr; for 1h; Inert atmosphere; |
Methyl dimethoxyacetate
2,2-dimethoxyethanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 3h; | 5.45 g |
Conditions | Yield |
---|---|
With 1H-imidazole In tetrahydrofuran at 0 - 20℃; for 4h; | 100% |
2,2-dimethoxyethanol
isobutyryl chloride
isobutyric acid 2,2-dimethoxy-ethyl ester
Conditions | Yield |
---|---|
With dmap; triethylamine at 20℃; for 16h; | 99% |
With dmap; triethylamine In ethyl acetate at 0 - 20℃; for 16h; | 99% |
With dmap; triethylamine In tert-butyl methyl ether at 0 - 20℃; for 16h; | 99% |
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 12h; | 98% |
Conditions | Yield |
---|---|
With sodium hydroxide In DMF (N,N-dimethyl-formamide) at 0 - 20℃; | 93% |
With sodium hydroxide In N,N-dimethyl-formamide at 0 - 20℃; for 16h; | 60% |
2,2-dimethoxyethanol
carbon monoxide
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; palladium diacetate; (S)-(-)-(6,6’-dimethoxybiphenyl-2,2’-diyl)bis(diphenylphosphine) In chlorobenzene; acetone at 20 - 80℃; for 30h; Schlenk technique; enantioselective reaction; | 93% |
2,2-dimethoxyethanol
2-Nitrobenzenesulfonyl chloride
Conditions | Yield |
---|---|
With TEA In dichloromethane at 20℃; for 3h; | 92% |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol for 24h; Heating; | 91% |
With hydrogenchloride In ethanol; water at -5℃; for 24h; Reflux; | 91% |
3-thienyl iodide
2,2-dimethoxyethanol
3-(2,2-dimethoxyethoxy)thiophene
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In toluene at 110℃; for 36h; | 91% |
Conditions | Yield |
---|---|
With Montmorillonite K10 at 20℃; for 1.5h; | 88% |
2,2-dimethoxyethanol
2-Fluoro-4-iodo-3-methylpyridine
Conditions | Yield |
---|---|
Stage #1: 2,2-dimethoxyethanol With sodium hydride In tetrahydrofuran Stage #2: 2-Fluoro-4-iodo-3-methylpyridine In tetrahydrofuran at 20℃; Further stages.; | 86% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane at 20℃; for 120h; | 85% |
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran -78 deg C -> r.t.; | 82% |
With 2-chloro-1-methyl-pyridinium iodide; triethylamine In dichloromethane for 24h; Ambient temperature; | 81% |
2,2-dimethoxyethanol
sorbinyl chloride
2,2-dimethoxyethyl (2E,4E)-2,4-hexadienoate
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran for 9h; Ambient temperature; | 82% |
Conditions | Yield |
---|---|
Stage #1: 2,2-dimethoxyethanol With sodium hydride In N,N-dimethyl-formamide for 0.5h; Stage #2: 2-Chloroquinoline In N,N-dimethyl-formamide at 20℃; for 24h; | 81% |
2,6-dichloroquinoline
2,2-dimethoxyethanol
Conditions | Yield |
---|---|
Stage #1: 2,2-dimethoxyethanol With sodium hydride In N,N-dimethyl-formamide for 0.5h; Stage #2: 2,6-dichloroquinoline In N,N-dimethyl-formamide at 20℃; for 24h; | 81% |
2,2-dimethoxyethanol
ethyl-2-O-benzyl-6-O-isobutyl-3,4-di-O-methyl-1-thio-α-D-mannopyranoside
Conditions | Yield |
---|---|
With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate In dichloromethane; toluene at 0℃; | 80% |
2,2-dimethoxyethanol
ethyl-2-O-benzyl-6-O-isopropyl-3,4-di-O-methyl-1-thio-α-D-mannopyranoside
Conditions | Yield |
---|---|
With N-iodo-succinimide; 4 A molecular sieve; silver trifluoromethanesulfonate In dichloromethane; toluene at 0℃; | 80% |
2,2-dimethoxyethanol
N-(2-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)-4-nitrobenzenesulfonamide
N-[2-(tert-butyldimethylsilanyloxymethyl)phenyl]-N-(2,2-dimethoxyethyl)-4-nitrobenzenesulfonamide
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at -20 - 30℃; for 21h; Mitsunobu reaction; | 80% |
3,3-Dimethylacryloyl chloride
2,2-dimethoxyethanol
2,2-dimethoxyethyl 3-methyl-2-butenoate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0℃; | 78% |
2,2-dimethoxyethanol
methyl 2-(bromomethyl)propenoate
2-(2,2-dimethoxy-ethoxymethyl)-acrylic acid methyl ester
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 0 - 20℃; | 78% |
indole
2,2-dimethoxyethanol
acetic anhydride
2,2-di-(1H-indol-3-yl)ethyl acetate
Conditions | Yield |
---|---|
Stage #1: indole; 2,2-dimethoxyethanol at 20℃; for 1.5h; Stage #2: acetic anhydride With sodium acetate at 20℃; for 17h; | 76% |
2,2-dimethoxyethanol
Conditions | Yield |
---|---|
With silver carbonate In dichloromethane at 0℃; | 75% |
2,2-dimethoxyethanol
Conditions | Yield |
---|---|
With 4 A molecular sieve; silver carbonate In dichloromethane at 0℃; | 75% |
2,2-dimethoxyethanol
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Fmoc-Ser(tBu)-OH
4-Nitrobenzenesulfonyl chloride
(3S,6S,8aS)-6-methyl-7-((4-nitrophenyl)sulfonyl)-5-oxohexahydro-2H-oxazolo[3,2-a]pyrazine-3-carboxamide
Conditions | Yield |
---|---|
Stage #1: Fmoc-Ser(tBu)-OH With benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 16h; Rink amide resin; Stage #2: With piperidine In N,N-dimethyl-formamide at 20℃; for 0.333333h; Rink amide resin; Stage #3: 2,2-dimethoxyethanol; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; 4-Nitrobenzenesulfonyl chloride stereoselective reaction; Further stages; | 75% |
2,2-dimethoxyethanol
6-chloro-2-(chloromethyl)-1-isopropyl-imidazo [4,5-c]pyridine
Conditions | Yield |
---|---|
Stage #1: 2,2-dimethoxyethanol With sodium hydride In N,N-dimethyl-formamide at 50℃; for 1h; Stage #2: 6-chloro-2-chloromethyl-1-isopropyl-1H-imidazo[4,5-c]pyridine In N,N-dimethyl-formamide at 50℃; for 2h; | 75% |
2,2-dimethoxyethanol
monoallyl malonate
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride
Conditions | Yield |
---|---|
With triethylamine In ethyl acetate | 73% |
2,2-dimethoxyethanol
4-phenylbutyronitrile
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane at 20℃; for 120h; | 73% |
veratronitrile
2,2-dimethoxyethanol
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In 1,2-dichloro-ethane at 20℃; for 24h; Concentration; Solvent; Temperature; | 68% |
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