Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Cas:58479-61-1
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inquiryDayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:58479-61-1
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryItems Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------
Cas:58479-61-1
Min.Order:1 Gram
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inquiryWe can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need CMO
Cas:58479-61-1
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inquiryFactory supply tert-Butylchlorodiphenylsilane CAS 58479-61-1 with fast delivery Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates,
Cas:58479-61-1
Min.Order:10 Kilogram
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Type:Trading Company
inquiryhe company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality se T rvice Appearance:Whit
Cas:58479-61-1
Min.Order:1 Kilogram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:58479-61-1
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inquiry1. made in GMP plant, commerially 2. Normal Stock: 500kgs 3. Audit accepted. Related documents are available to offer and audited by many clients, such as Lupin, MSN, Dr reddy etc 4. Chromatographic Purity (HPLC): not less than 99.0% Appearan
Cas:58479-61-1
Min.Order:1 Gram
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inquirytert-Butylchlorodiphenylsilane CAS 58479-61-1 tert-Butyldiphenylchlorosilane CAS no 58479-61-1 tert-Butyldiphenylsilyl chloride tert-Butylchlorodiphenylsilane Manufacturer High quality Best price In stock factory CAS 58479-61-1 tert-Butylchloro
Cas:58479-61-1
Min.Order:5 Kiloliter
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:58479-61-1
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:58479-61-1
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:58479-61-1
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inquiryName: tert-Butylchlorodiphenylsilane Molecular Formula:C16H19ClSi Molecular Weight:274.87 CAS No.:58479-61-1 Appearance:Colorless To Slight Brown Liquid Appearance:Colorless To Slight Brown Liquid Storage: Preserve in well-closed, light-resistant
Cas:58479-61-1
Min.Order:1 Kilogram
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inquiry1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:58479-61-1
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:58479-61-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:58479-61-1
Min.Order:1 Kilogram
FOB Price: $168.0 / 180.0
Type:Trading Company
inquirytert-Butylchlorodiphenylsilane CAS:58479-61-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or
Cas:58479-61-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryT-Butyl Diphenyl Chlorosilane CAS: 58479-61-1 Item Specification Appearance Clear Colorless Liquid Assay 98%min Density 1.057 g/mL at 25 °C(lit.) Boiling Point 90 °C0.01 mm Hg(li
Cas:58479-61-1
Min.Order:1 Kilogram
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Type:Other
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:58479-61-1
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:58479-61-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:58479-61-1
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:58479-61-1
Min.Order:0
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:58479-61-1
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:58479-61-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Cas:58479-61-1
Min.Order:1 Milligram
Negotiable
Type:Trading Company
inquirytert-Butylchlorodiphenylsilane Chemical Properties Boiling point 90 °C0.01 mm Hg(lit.) density 1.057 g/mL at 25 °C(lit.) refractive index n20/D 1.568(lit.) Fp >230 °F storage temp. Store at 5°C form Liquid c
Cas:58479-61-1
Min.Order:1 Gram
FOB Price: $66.0
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:58479-61-1
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryProduct name: Tert-butyl Diphenyl Chlorsilane CAS No.:58479-61-1 Molecule Formula: C16H19ClSi Molecule Weight:274.86 Purity: 98% Package: 100kg/drum Description:Colorless or brownish oily liquid Manufacture Standards:Enterprise Standa
Cas:58479-61-1
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquirytert.-butyl lithium
diphenylsilyl dichloride
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
In hexane for 4h; Reflux; | 92% |
In pentane for 12h; | 65% |
tertiary butyl chloride
diphenylsilyl dichloride
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
Stage #1: tertiary butyl chloride With magnesium In tetrahydrofuran at 60℃; for 2h; Stage #2: With lithium chloride; copper(I) bromide In tetrahydrofuran at 20℃; for 1h; Stage #3: diphenylsilyl dichloride In tetrahydrofuran at 50℃; for 6h; Reagent/catalyst; Temperature; | 87% |
With copper(l) cyanide; magnesium In tetrahydrofuran for 5h; Heating; | 80% |
With magnesium In tetrahydrofuran; hexane | 75% |
tert-butyl(methoxy)diphenylsilane
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
With iron(III) chloride; acetyl chloride In 1,2-dichloro-ethane for 72h; | 86% |
With hydrogenchloride In water |
diphenylsilyl dichloride
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
copper (II) acetylacetonate | 85% |
t-butyl diphenylsilanol
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
With thionyl chloride In chloroform for 0.5h; | 81% |
trimethylsilyldiphenylmethane
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
With SO2Cl2 In not given | 74% |
With SO2Cl2 In not given | 74% |
tert-butyldiphenylsilane
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
With iron(III) chloride; acetyl chloride In dichloromethane for 24h; | 69% |
With sulfuryl dichloride | |
With dichloromethane; eosin y at 20℃; for 24h; Reagent/catalyst; Sealed tube; Inert atmosphere; Irradiation; Green chemistry; | 99 %Spectr. |
p-toluenesulfonyl chloride
(1S,3S,5R,6S)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-bicyclo[3.1.0]hexan-3-ol
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
With pyridine; dmap In dichloromethane for 24h; Ambient temperature; | 67% |
phenyl-tert-butyldichlorosilane
phenyllithium
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
Inert atmosphere; |
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
With hydrogenchloride In water |
(diphenylmethyl)potassium
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: not given 2: SO2Cl2 / not given View Scheme |
9-(2,3-anhydro-β-D-ribofuranosyl)adenine
tert-butylchlorodiphenylsilane
9-<2,3-anhydro-5-O-<(tert-butyl)diphenylsilyl>-β-D-ribofuranosyl>adenine
Conditions | Yield |
---|---|
In pyridine at 20℃; for 12h; | 100% |
With pyridine | 100% |
In pyridine | 98% |
propargyl alcohol
tert-butylchlorodiphenylsilane
tert-butyl(diphenyl)(2-propynyloxy)silane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 5h; | 100% |
With 1H-imidazole In dichloromethane at 20℃; for 5h; | 100% |
With 1H-imidazole In dichloromethane for 16h; | 100% |
1-Hydroxy-2-butanone
tert-butylchlorodiphenylsilane
1-(tert-butyldiphenylsiloxy)-2-butanone
Conditions | Yield |
---|---|
With 1H-imidazole; dmap In N,N-dimethyl-formamide at 0℃; for 10h; | 100% |
92% |
4-methoxy-phenol
tert-butylchlorodiphenylsilane
tert-butyl-4-methoxyphenoxydiphenylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In acetonitrile for 0.166667h; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 10h; Inert atmosphere; | 90% |
With 1H-imidazole In acetonitrile for 0.166667h; |
1-phenyl-2-hydroxyethanone
tert-butylchlorodiphenylsilane
2-(tert-butylphenylsilyloxy)acetophenone
Conditions | Yield |
---|---|
With 1H-imidazole; dmap In N,N-dimethyl-formamide at 0℃; for 10h; | 100% |
With 1H-imidazole; dmap In dichloromethane at 20℃; for 12h; | 95% |
With 1H-imidazole In dichloromethane | |
With 1H-imidazole In dichloromethane at 20℃; Inert atmosphere; | |
With triethylamine In dichloromethane at 0 - 10℃; |
allyl alcohol
tert-butylchlorodiphenylsilane
3-(tert-butyldiphenylsilyloxy)prop-1-ene
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 23℃; for 2h; | 100% |
With 1H-imidazole In dichloromethane at 0 - 20℃; for 8h; | 100% |
With ammonium nitrate In N,N-dimethyl-formamide for 0.25h; | 99% |
hydroxy-2-propanone
tert-butylchlorodiphenylsilane
1-(tert-butyldiphenylsilyloxy)-2-propanone
Conditions | Yield |
---|---|
With 1H-imidazole; dmap In N,N-dimethyl-formamide at 0℃; for 10h; | 100% |
With 1H-imidazole; dmap In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 100% |
With 1H-imidazole; dmap In N,N-dimethyl-formamide at 0 - 25℃; for 18.25h; Inert atmosphere; | 100% |
1,6-anhydro-3,4-dideoxy-β-D-erythro-hex-3-enopyranose
tert-butylchlorodiphenylsilane
1,6-anhydro-2-O-(tert-butyldiphenylsilyl)-3,4-dideoxy-β-D-erythro-hex-3-enopyranose
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 3h; Ambient temperature; | 100% |
(1S,5R,6S,7R)-7-benzoyloxy-6-hydroxymethyl-2-oxabicyclo[3.3.0]octan-3-one
tert-butylchlorodiphenylsilane
(3aR,4S,5R,6aS)-5-benzoyloxy-4-[(t-butyldiphenylsiloxy)methyl]hexahydro-2H-cyclopenta[b]furan-2-one
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide | 100% |
With 1H-imidazole; dmap In dichloromethane | 83% |
With 1H-imidazole; dmap In dichloromethane |
2,3-O-isopropylidene-D-ribofuranose
tert-butylchlorodiphenylsilane
5-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-ribofuranose
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; for 3h; | 100% |
With dmap; triethylamine In dichloromethane at 20℃; for 3h; | 100% |
With dmap; triethylamine In dichloromethane at 20℃; for 3h; | 99% |
n-Pent-4-enyl alcohol
tert-butylchlorodiphenylsilane
tert-butyl(pent-4-en-1-yloxy)diphenylsilane
Conditions | Yield |
---|---|
With 1H-imidazole; dmap In N,N-dimethyl-formamide for 19h; Ambient temperature; | 100% |
With 1H-imidazole; dmap In N,N-dimethyl-formamide for 19h; Ambient temperature; | 100% |
With dmap; triethylamine In dichloromethane at 0 - 20℃; | 100% |
(1S,5R,6R,7R,15S)-7-(tetrahydro-2-pyranyloxy)-6-<(E)-3-hydroxy-1-octenyl>-2-oxabicyclo<3.3.0>octan-3-one
tert-butylchlorodiphenylsilane
3α,5α-dihydroxy-2β-<3α-((tert-butyldiphenylsilyl)oxy)-trans-1-octenyl>-1α-cyclopentaneacetic acid γ-lactone 3-(tetrahydropyranyl ether)
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 1.5h; Ambient temperature; | 100% |
Butane-1,4-diol
tert-butylchlorodiphenylsilane
4-(tret-butyldiphenylsilyloxy)butan-1-ol
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane; N,N-dimethyl-formamide at 0 - 25℃; | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h; Inert atmosphere; | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 18℃; for 20h; Inert atmosphere; | 100% |
tert-butylchlorodiphenylsilane
3-methyl-2-buten-1-ol
1-((tert-butyldiphenylsilyl)oxy)-3-methyl-2-butene
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; | 100% |
With 1H-imidazole In dichloromethane at 0 - 20℃; for 0.5h; | 98% |
With dmap; triethylamine In dichloromethane for 2h; Ambient temperature; | 82% |
homoalylic alcohol
tert-butylchlorodiphenylsilane
4-tert-butyldiphenylsilyloxy-1-butene
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 0 - 20℃; for 3h; Inert atmosphere; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide for 17h; Ambient temperature; | 99% |
1,4-butenediol
tert-butylchlorodiphenylsilane
(Z)-2,2,11,11-tetramethyl-3,3,10,10-tetraphenyl-4,9-dioxa-3,10-disiladodec-6-ene
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 2h; Inert atmosphere; | 100% |
With 1H-imidazole In dichloromethane at 0 - 20℃; for 2.83333h; | 99% |
With dmap; triethylamine In dichloromethane at 0 - 20℃; | 97% |
hex-1-en-5-yn-3-ol
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide | 100% |
glycolic acid methyl ester
tert-butylchlorodiphenylsilane
methyl 2-((tert-butyl(diphenyl)silyl)oxy)acetate
Conditions | Yield |
---|---|
With 1H-imidazole; dmap In N,N-dimethyl-formamide for 10h; Ambient temperature; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 3h; | 99% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 3h; Inert atmosphere; | 98% |
(E)-2-penten-4-yn-1-ol
tert-butylchlorodiphenylsilane
(E)-tert-butyl(pent-2-en-4-yn-1-yloxy)diphenylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 25℃; | 100% |
With 1H-imidazole In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 88% |
With 1H-imidazole In dichloromethane at 0℃; for 2h; | 85% |
3-hydroxy-(2S)-methylpropionate
tert-butylchlorodiphenylsilane
(S)-3-(tert-butyl-diphenyl-silanyloxy)-2-methyl-propionic acid methyl ester
Conditions | Yield |
---|---|
With Imd | 100% |
With N-ethyl-N,N-diisopropylamine In dichloromethane | 100% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; | 100% |
(S)-Ethyl lactate
tert-butylchlorodiphenylsilane
ethyl (S)-2-(tert-butyldiphenylsilyloxy)propanoate
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane at 20℃; | 100% |
With 1H-imidazole In dichloromethane at 20℃; for 1h; | 100% |
With 1H-imidazole In dichloromethane at 20℃; for 4.5h; | 100% |
Nerol
tert-butylchlorodiphenylsilane
(Z)-1-[(tert-butyldiphenylsilyl)oxy]-3,7-dimethyl-2,6-octadiene
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 0.25h; Ambient temperature; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide | 99% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 16h; | 98% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 16h; | 98% |
With 1H-imidazole In dichloromethane; N,N-dimethyl-formamide for 3h; Ambient temperature; | 95% |
Geraniol
tert-butylchlorodiphenylsilane
tert-butyl ({[(2E)-3,7-dimethylocta-2,6-dien-1-yl]oxy})diphenylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 0.25h; Ambient temperature; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 1h; Silylation; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 1h; | 100% |
(S)-2-hydroxy-3-(methoxycarbonyl)propionamide
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In tetrahydrofuran at 36℃; for 10h; | 100% |
3,3-dimetylbutan-1,2-diol
tert-butylchlorodiphenylsilane
1-(tert-Butyl-diphenyl-silanyloxy)-3,3-dimethyl-butan-2-ol
Conditions | Yield |
---|---|
100% |
pent-1-yn-5-ol
tert-butylchlorodiphenylsilane
tert-butyl-pent-4-ynyloxy-diphenyl-silane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide | 100% |
With 1H-imidazole In dichloromethane at 25℃; | 100% |
With 1H-imidazole In dichloromethane at 0℃; for 1h; Inert atmosphere; | 100% |
3-bromobut-3-en-1-ol
tert-butylchlorodiphenylsilane
((3-bromobut-3-en-1-yl)oxy)(tert-butyl)diphenylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane at 20℃; for 3h; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide at 22℃; for 18h; | 96% |
With dmap; triethylamine In dichloromethane at 23℃; for 2h; | 93% |
With 1H-imidazole In dichloromethane at 0 - 20℃; for 10h; Inert atmosphere; | 90% |
With 1H-imidazole; dmap |
3-cyclohexen-1-ol
tert-butylchlorodiphenylsilane
4-<(tert-Butyldiphenylsilyl)oxy>cyclohexene
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 24h; | 100% |
(2R*,3Z)-4-Iodo-3-buten-2-ol
tert-butylchlorodiphenylsilane
(1Z,3R*)-3-(tert-Butyldiphenylsilyloxy)-1-iodo-1-butene
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at -10℃; for 40h; | 100% |
N-benzyloxycarbonyl-L-serine methyl ester
tert-butylchlorodiphenylsilane
methyl (2S)-3-(2,2-dimethyl-1,1-diphenyl-1-silapropoxy)-2-[(phenylmethoxy)carbonylamino]propanoate
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide for 0.75h; Ambient temperature; | 100% |
With 1H-imidazole In N,N-dimethyl-formamide | 90% |
With 1H-imidazole; dmap In N,N-dimethyl-formamide at 45℃; for 7h; | 90% |
With 1H-imidazole In dichloromethane at 0 - 20℃; for 8h; Inert atmosphere; | 64% |
With 1H-imidazole | 61% |
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