span style="fonAppearance:Colorless transparent liquid Storage:Store in dry, dark and ventilated place. Package:200L drum Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals and Dye
Cas:80-10-4
Min.Order:1 Kilogram
FOB Price: $2.0 / 3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:80-10-4
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquirychengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
Cas:80-10-4
Min.Order:1 Metric Ton
FOB Price: $3000.0
Type:Manufacturers
inquiry1,ISO Certificate 2,Factory price 3,Free sample and Fast delivery Appearance:Colorless transparent liquid Storage:All products should be stored at a dry and ventilated location away from fire and other dangerous goods, and should avoid direct sunl
Cas:80-10-4
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:80-10-4
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Manufacturers
inquiryProduct Name: Dichlorodiphenylsilane Synonyms: CD5950;Dichlor-difenylsilan;dichlorodiphenyl-silan;Diphenyldichlorosilicane;diphenylsilyldichloride;Silane, dichlorodiphenyl-;Silane,dichlorodiphenyl-;tsl8062
Cas:80-10-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryDiphenyldichlorosilane Synonym: Dichlorodiphenylsilane;Diphenylsilyl dichloride; dichlorodiphenyl-silane; dichlor-difenylsilane CAS No.:80-10-4 Molecular Formula:C12H10Cl2Si Molecular Weight:253.2 Properties: Colorless, flammable
Cas:80-10-4
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Other
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:liquid Storage:Store in sealed containers at cool & dry plac
Cas:80-10-4
Min.Order:100 Gram
Negotiable
Type:Other
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At presen
Cas:80-10-4
Min.Order:1 Kilogram
FOB Price: $80.0 / 100.0
Type:Trading Company
inquiry80-10-4 DIPHENYLDICHLOROSILANE Diphenyldichlorosilane Molecular Formula:C12H10Cl2Si Appearance:Colorless, flammable liquid Storage:Store in dry and cool place with good seal Package:Iron drum or drum lined with Plastic,Net Weight:200kg。 A
Price, service, company and transport advantage: 1.place of origin china with super quality by reasonable price. 2. it's customers' right to choose the package (ems, dhl, fedex, ups); 3. it's custo
Cas:80-10-4
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:80-10-4
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:80-10-4
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:80-10-4
Min.Order:1 Gram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Cas:80-10-4
Min.Order:1 Gram
Negotiable
Type:Trading Company
inquiryProductName:Dichlorodiphenylsilane Synonyms:dichloro(diphenyl)silane;Silane, dichlorodiphenyl-; CAS: 80-10-4 Molecular formula: (C6H5)2SiCl2 Molecular weight: 253.2 Character: colorless flammable liquid content: ≥99% Trichloromethy
Cas:80-10-4
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers240.Safe and fa
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:80-10-4
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:80-10-4
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryAmoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
in storeAppearance:Colorless - very pale yellow transparent liquid Package:100ml Application:Organic Chemicals
1. Introduction ofDichlorodiphenylsilane The Dichl…Appearance:Colorless Transparent Liquid Storage:20℃ Package:25kg/plastic drum,200Kg/iron drum Application:silane and other products Transportation:by air or by sea Port:Donggua
Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical
Conditions | Yield |
---|---|
With tellurium tetrachloride In benzene for 3h; Heating; | 95% |
With copper(l) iodide; copper dichloride In diethyl ether at 20℃; for 4h; Inert atmosphere; | 94.1% |
With dichloromethane; eosin y at 50℃; Temperature; Reagent/catalyst; Flow reactor; Inert atmosphere; Irradiation; | 99 %Spectr. |
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole
Phenyltrichlorosilane
A
Triphenylsilyl chloride
B
diphenylsilyl dichloride
Conditions | Yield |
---|---|
Stage #1: 2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole With bis(tricyclohexylphosphine)nickel(II) dichloride; triethylaluminum; dimethylaluminum chloride In 1,4-dioxane; hexane; 1,3,5-trimethyl-benzene at 90℃; for 0.5h; Stage #2: Phenyltrichlorosilane In hexane; toluene; 1,3,5-trimethyl-benzene at 90℃; for 24h; | A n/a B 88% |
Conditions | Yield |
---|---|
Stage #1: bromobenzene With n-butyllithium In diethyl ether; hexane Stage #2: With tetrachlorosilane In diethyl ether; hexane at 0 - 5℃; | |
Stage #1: bromobenzene With n-butyllithium In diethyl ether at -78℃; Stage #2: With tetrachlorosilane In diethyl ether at 0 - 20℃; |
Phenyltrichlorosilane
chlorobenzene
A
phenylchlorosilane
B
diphenylsilyl dichloride
Conditions | Yield |
---|---|
Stage #1: Phenyltrichlorosilane With hydrogenchloride In water at 350 - 400℃; under 1500.15 Torr; for 3h; Stage #2: chlorobenzene at 350 - 480℃; under 1500.15 Torr; for 10h; Reagent/catalyst; Temperature; |
Conditions | Yield |
---|---|
With magnesium at 185℃; for 17.5h; Inert atmosphere; | 68% |
Phenyltrichlorosilane
chlorobenzene
A
Triphenylsilyl chloride
B
diphenylsilyl dichloride
Conditions | Yield |
---|---|
With magnesium at 155℃; Inert atmosphere; | A 67.2% B 31.4% |
Conditions | Yield |
---|---|
With hexachloroethane; palladium dichloride at 20℃; for 1h; | 89% |
With hydrogenchloride; ether adduct of tris(pentafluorophenyl)boron In toluene at 20℃; for 150h; Schlenk technique; Inert atmosphere; Cooling with liquid nitrogen; | 61 %Spectr. |
With dichloromethane; eosin y at 20℃; for 4h; Reagent/catalyst; Inert atmosphere; Irradiation; Green chemistry; | 99 %Spectr. |
Conditions | Yield |
---|---|
With silicon-copper at 400℃; | |
With silver; silicon at 400℃; | |
With iron; silicon at 550℃; | |
With silicon-copper at 420℃; |
chlorobenzene
silicon
A
biphenyl
B
Phenyltrichlorosilane
C
diphenylsilyl dichloride
Conditions | Yield |
---|---|
tin at 450℃; under 0.1 Torr; for 1h; Product distribution / selectivity; | |
tin; copper; zinc at 480℃; Product distribution / selectivity; | |
tin; copper at 450℃; under 0.1 Torr; for 1h; Product distribution / selectivity; |
chlorobenzene
A
biphenyl
B
Phenyltrichlorosilane
C
diphenylsilyl dichloride
Conditions | Yield |
---|---|
With silicon; tin(ll) chloride at 450 - 500℃; for 2h; Product distribution / selectivity; | |
With silicon; tin; copper; zinc at 450℃; Product distribution / selectivity; | |
With silicon; tin; zinc at 450℃; Product distribution / selectivity; | |
With silicon; tin at 450℃; Product distribution / selectivity; |
diphenylsilyl dichloride
Conditions | Yield |
---|---|
With diethyl ether; hexachlorodisilane | |
With tetrachlorosilane; diethyl ether; benzene | |
With tetrachlorosilane; diethyl ether |
Conditions | Yield |
---|---|
With silicon; tin(ll) chloride at 450 - 500℃; for 3h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With silicon; tin at 450℃; for 1h; Product distribution / selectivity; | |
With silicon; copper at 450℃; for 1h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
tin at 450℃; under 0.1 Torr; for 1h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
tin at 450℃; under 0.1 Torr; for 1h; Product distribution / selectivity; | |
tin at 450℃; under 0.1 Torr; for 1h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With pyridine | |
In neat (no solvent) boiling of (C6H5)Si(OC2H5)2 and C6H5COCl in presence of some pyridine for a longer period of time;; | |
In neat (no solvent) boiling of (C6H5)Si(OC2H5)2 and C6H5COCl in presence of some pyridine for a longer period of time;; |
dichloro(o-chlorophenyl)phenylsilane
A
9,9-dichloro-9-silafluorene
B
Phenyltrichlorosilane
C
chlorobenzene
D
diphenylsilyl dichloride
Conditions | Yield |
---|---|
With hexachlorodisilane at 500℃; gas phase; Further byproducts given; | A 95% B 0.3 g C 0.8 g D 0.2 g |
chlorobenzene
silicon
A
biphenyl
B
diphenylsilyl dichloride
C
benzene
Conditions | Yield |
---|---|
tin at 450℃; under 0.1 Torr; for 1h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With aluminium trichloride |
Dichlorosilane
chlorobenzene
A
Phenyltrichlorosilane
B
diphenylsilyl dichloride
C
benzene
Conditions | Yield |
---|---|
1,1'-(1,2-ethanediyl)bisbenzene at 650℃; for 0.5h; Product distribution / selectivity; | A 10.7% B 5.11% C 8.87% |
chlorobenzene
silicon
A
biphenyl
B
Phenyltrichlorosilane
C
diphenylsilyl dichloride
D
benzene
Conditions | Yield |
---|---|
tin at 480℃; Product distribution / selectivity; | |
tin; copper; zinc at 480℃; Product distribution / selectivity; | |
tin at 480℃; Product distribution / selectivity; |
dichloro(o-chlorophenyl)phenylsilane
A
1,9,9-trichloro-9-silafluorene
B
9,9-dichloro-9-silafluorene
C
Phenyltrichlorosilane
D
diphenylsilyl dichloride
Conditions | Yield |
---|---|
With chloroform at 620℃; gas phase; | A 44% B 4.5% C 1.5 g D 4.5 g |
hexachlorodisilane
diphenylsilyl dichloride
Conditions | Yield |
---|---|
With phenylmagnesium bromide In not given | |
With C6H5MgBr In not given |
Conditions | Yield |
---|---|
With boron trichloride at 185℃; | |
With aluminium trichloride at 185℃; |
dichloro(o-chlorophenyl)phenylsilane
A
9,9-dichloro-9-silafluorene
B
Phenyltrichlorosilane
C
diphenylsilyl dichloride
D
toluene
Conditions | Yield |
---|---|
With 1,1-Dichloro-2,5-dihydro-1H-silole at 600℃; gas phase; Further byproducts given. Title compound not separated from byproducts; | A 30% B 0.5 g C 0.8 g D n/a |
dichloromethylphenylsilane
A
dimethylsilicon dichloride
B
diphenylsilyl dichloride
Conditions | Yield |
---|---|
With aluminum (III) chloride at 120℃; for 3h; | A 6% B 6% |
Conditions | Yield |
---|---|
With phosphorus pentachloride at 180 - 240℃; |
Conditions | Yield |
---|---|
With tetrachlorosilane at 840℃; in der Dampfphase; |
tetrachlorosilane
A
Triphenylsilyl chloride
B
Phenyltrichlorosilane
C
diphenylsilyl dichloride
Conditions | Yield |
---|---|
With phenylmagnesium bromide In diethyl ether SiCl4 (1 mol) and C6H5MgBr (2.25 mol) in boiling ether;; | |
With C6H5MgBr In diethyl ether SiCl4 (1 mol) and C6H5MgBr (2.25 mol) in boiling ether;; |
Conditions | Yield |
---|---|
With benzene In neat (no solvent) H2SiCl2 and C6H6 with a Zn-halide as catalyst at 400°C;; |
diphenylsilyl dichloride
1,3-diallyl-4-(trimethylsilyloxy)-2,6-dioxo-1,3,5-triazine
Conditions | Yield |
---|---|
at 120 - 160℃; | 99.6% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 40℃; for 6h; | 99.5% |
Conditions | Yield |
---|---|
In 5,5-dimethyl-1,3-cyclohexadiene at 120℃; for 10h; | 99.3% |
(S)-4-trimethylsilyl-3-butyn-2-ol
diphenylsilyl dichloride
C26H36O2Si3
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at 0 - 23℃; for 4h; | 99% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 1h; | 99% |
Conditions | Yield |
---|---|
Stage #1: allyl bromide With indium In N,N-dimethyl-formamide at 20℃; for 1h; Stage #2: diphenylsilyl dichloride In N,N-dimethyl-formamide at 20℃; for 3h; | 99% |
With zinc In tetrahydrofuran for 0.166667h; Inert atmosphere; Sonication; | 88% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 99% |
diphenylsilyl dichloride
Conditions | Yield |
---|---|
In tetrahydrofuran at -25 - 20℃; | 99% |
tetrakis(trimethylsilyl)silane
diphenylsilyl dichloride
1-chloro-1,1-diphenyl-2,2-bis(trimethylsilyl)trimethyltrisilane
Conditions | Yield |
---|---|
Stage #1: tetrakis(trimethylsilyl)silane With potassium tert-butylate In 1,2-dimethoxyethane for 6h; Stage #2: diphenylsilyl dichloride In 1,2-dimethoxyethane; toluene for 14h; | 99% |
Conditions | Yield |
---|---|
With sodium; 1,2-dibromomethane In xylene Ar; to suspension of Na were added at 138°C during 1.5 h silane and borane (4:1) and CH2Br2; 30 min reflux; filtration; evapn. of solvent and drying at 100°C for 20 h (vacuo); elem. anal.; | 98.8% |
silver trifluoromethanesulfonate
diphenylsilyl dichloride
Diphenylsilicium-bis(trifluormethansulfonat)
Conditions | Yield |
---|---|
In dichloromethane at -25 - 20℃; | 98% |
96 h,25°C; | 80% |
1,2-dimethyl-4,5-di(mercaptomethyl)benzene
diphenylsilyl dichloride
9,10-Dimethyl-2,2-diphenyl-5,6-benzo-1,3,2-dithiasilepine
Conditions | Yield |
---|---|
With triethylamine In benzene for 5h; Heating; | 98% |
vinyl magnesium bromide
diphenylsilyl dichloride
diphenyl-divinyl-silane
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 12h; Grignard reaction; | 98% |
In tetrahydrofuran; pentane for 12h; Heating; | 80% |
sodium tri-tert-butylsilanide
diphenylsilyl dichloride
Conditions | Yield |
---|---|
In tetrahydrofuran Substitution; supersilanidation; | 98% |
diphenylsilyl dichloride
allylsamarium bromide
allyl(chloro)diphenylsilane
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 1h; | 98% |
Conditions | Yield |
---|---|
Stage #1: propargyl bromide With indium In N,N-dimethyl-formamide at 20℃; for 1h; Stage #2: diphenylsilyl dichloride In N,N-dimethyl-formamide at 20℃; for 3h; | 98% |
phenylacetylene
diphenylsilyl dichloride
1,1-diphenylbis(phenylethynyl)silane
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran at -70℃; | 97% |
With [{Ir(μ-Cl)(CO)2}2]; N-ethyl-N,N-diisopropylamine; lithium iodide at 100℃; for 72h; Schlenk technique; Inert atmosphere; | 90% |
With n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃; for 1h; Inert atmosphere; | 90% |
ethynylmagnesium chloride
diphenylsilyl dichloride
diethynyldiphenylsilane
Conditions | Yield |
---|---|
In tetrahydrofuran at 30 - 40℃; for 3h; | 97% |
Stage #1: ethynylmagnesium chloride; diphenylsilyl dichloride In tetrahydrofuran for 1h; Inert atmosphere; Stage #2: With ammonium chloride In tetrahydrofuran; water Inert atmosphere; | 70% |
In tetrahydrofuran |
Conditions | Yield |
---|---|
With air; sodium fluoride; rhodium(I)-bis(1,5-cyclooctadiene) tetrafluoroborate at 100℃; for 12h; | 97% |
diphenylsilyl dichloride
Conditions | Yield |
---|---|
Stage #1: 1,2-bis(1H-indol-2-yl)benzene With potassium hexamethylsilazane In tetrahydrofuran; toluene at 0℃; for 0.25h; Stage #2: diphenylsilyl dichloride In tetrahydrofuran; toluene at 0 - 20℃; for 12h; | 97% |
Conditions | Yield |
---|---|
With polyaniline at 40 - 50℃; for 8h; | 96% |
In diethyl ether at 40℃; for 3h; Inert atmosphere; | 76.92% |
Conditions | Yield |
---|---|
With sodium tetrafluoroborate In various solvent(s) for 0.75h; Heating; | 96% |
With hydrogen fluoride In ethanol at 20℃; | 90% |
With ammonium hexafluorosilicate In 1,2-dimethoxyethane at 0℃; for 0.333333h; Product distribution; var. react.: Na2SiF6, var. solv., temp and time; | 82% |
Conditions | Yield |
---|---|
In benzene for 12h; Heating; | 96% |
diphenylsilyl dichloride
Conditions | Yield |
---|---|
With ammonium fluoride; 18-crown-6 ether In hexane; toluene for 10h; Heating; | 96% |
diphenylsilyl dichloride
Conditions | Yield |
---|---|
In chloroform for 6h; Heating; | 96% |
diphenylsilyl dichloride
1,4-diphenylbut-2-ene-1,4-dione
1,2,4-triphenylbutane-1,4-dione
Conditions | Yield |
---|---|
With air; sodium fluoride; rhodium(I)-bis(1,5-cyclooctadiene) tetrafluoroborate at 100℃; for 12h; | 96% |
Conditions | Yield |
---|---|
Stage #1: 2,6-diisopropylbenzenamine With n-butyllithium In diethyl ether; hexane at -78 - 20℃; Inert atmosphere; Stage #2: diphenylsilyl dichloride In diethyl ether; hexane at -78℃; Inert atmosphere; | 96% |
Stage #1: 2,6-diisopropylbenzenamine With n-butyllithium In diethyl ether; hexane; Petroleum ether at -78 - 20℃; Stage #2: diphenylsilyl dichloride In Petroleum ether at -78℃; for 8h; | 66% |
With n-butyllithium In diethyl ether; hexane; Petroleum ether at -78 - 20℃; for 8h; |
diphenylsilyl dichloride
trimethylsilylacetylene
bis((trimethylsilyl)ethynyl)diphenylsilane
Conditions | Yield |
---|---|
With [{Ir(μ-Cl)(CO)2}2]; N-ethyl-N,N-diisopropylamine; lithium iodide at 100℃; for 72h; Schlenk technique; Inert atmosphere; | 96% |
Stage #1: trimethylsilylacetylene With n-butyllithium In diethyl ether; hexane at -78 - 0℃; for 1h; Stage #2: diphenylsilyl dichloride In diethyl ether; hexane at 0 - 20℃; | 87% |
With n-butyllithium In diethyl ether; hexane at -78 - 20℃; | 72% |
1.4-dibromobenzene
diphenylsilyl dichloride
bis(4-bromophenyl)(diphenyl)silane
Conditions | Yield |
---|---|
Stage #1: 1.4-dibromobenzene With n-butyllithium In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; Stage #2: diphenylsilyl dichloride In tetrahydrofuran at -78 - 20℃; for 14h; Inert atmosphere; | 96% |
Stage #1: 1.4-dibromobenzene With n-butyllithium In diethyl ether at 0℃; for 3h; Inert atmosphere; Stage #2: diphenylsilyl dichloride In diethyl ether at 20℃; for 48h; Inert atmosphere; | 85% |
Stage #1: 1.4-dibromobenzene With n-butyllithium In diethyl ether at -78℃; for 2.5h; Inert atmosphere; Stage #2: diphenylsilyl dichloride In diethyl ether at -78 - 20℃; Inert atmosphere; | 82.9% |
allyl bromide
diphenylsilyl dichloride
A
diallyldiphenylsilane
B
allyl(chloro)diphenylsilane
Conditions | Yield |
---|---|
Stage #1: allyl bromide With indium In 1,3-dimethylimidazolidine at 20℃; for 1h; Stage #2: diphenylsilyl dichloride In 1,3-dimethylimidazolidine at 70℃; for 3h; | A 3% B 96% |
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