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Cas:461-82-5
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inquiryItems Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------
Cas:461-82-5
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 4-(Trifluoromethoxy)aniline CAS No. 461-82-5
Cas:461-82-5
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inquiryFor the synthesis of fluorinated pharmaceutical, pesticide intermediates. Appearance:white powder Storage:Store below +30°C Package: according to customers' requirements Application:For the synthesis of fluorinated pharmaceutical, pesticide interm
Cas:461-82-5
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Cas:461-82-5
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Appearance:white or yellowish white flaky crystal Storage:Keep the sun from direct sunlight ;prevention against high temperature Package:As customer request Application:Used for research and industrial manufacture. Transportatio
Cas:461-82-5
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryConditions | Yield |
---|---|
Stage #1: 1-trifluoromethoxybenzene With sodium ferrate(VI); sodium bromide In dimethyl sulfoxide at 95℃; for 4h; Inert atmosphere; Stage #2: With sodium amide In dimethyl sulfoxide at 155℃; under 3040.2 Torr; for 10h; Solvent; Temperature; Reagent/catalyst; Pressure; Inert atmosphere; | 98.2% |
Multi-step reaction with 2 steps 1: sulfuric acid; nitric acid / dichloromethane / 2 h / 0 - 30 °C 2: iron; hydrogenchloride / methanol / 2 h / 60 - 65 °C View Scheme |
Conditions | Yield |
---|---|
With C36H56Cl3CrN2O; magnesium; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; | 92% |
With hydrogen; ShPAK-0.5 In methanol at 44 - 46℃; under 29420.3 - 30891.3 Torr; | 89% |
With hydrogenchloride; iron In methanol at 60 - 65℃; for 2h; |
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
With formic acid; potassium hydroxide In ethanol at 70℃; for 1h; | 91% |
1‐azido‐4‐(trifluoromethoxy)benzene
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
Stage #1: 1‐azido‐4‐(trifluoromethoxy)benzene With hydrazine hydrate for 0.166667h; Inert atmosphere; Stage #2: for 7h; Irradiation; chemoselective reaction; | 85% |
Conditions | Yield |
---|---|
With sodium methylate In methanol at 60℃; under 2250.23 Torr; for 4h; Autoclave; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
With dicyclohexyl(2',4',6'-triisopropyl-5-methoxy-3,4,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; C50H70NO4PPdS; C50H70NO4PPdS; dicyclohexyl(2',4',6'-triisopropyl-4-methoxy-3,5,6-trimethyl-[1,1'-biphenyl]-2-yl)phosphine; ammonia; sodium t-butanolate In 1,4-dioxane at 60℃; for 24h; Inert atmosphere; | 82% |
Stage #1: 1-bromo-4-(trifluoromethoxy)benzene With magnesium In tetrahydrofuran Inert atmosphere; Stage #2: With C10H17NO In tetrahydrofuran; toluene at -20℃; for 2h; Inert atmosphere; Stage #3: With ammonium chloride In tetrahydrofuran; water; toluene Inert atmosphere; | 62% |
Stage #1: 1-bromo-4-(trifluoromethoxy)benzene With magnesium; ethylene dibromide In tetrahydrofuran Inert atmosphere; Stage #2: With C10H17NO In tetrahydrofuran; toluene at -20℃; for 2h; Inert atmosphere; | 62% |
N-methyl-4-(trifluoromethoxy)aniline
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
With piperidine; dichloro(dimethylglyoxime)(dimethylglyoximato)cobalt(III); (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate In acetonitrile at -78℃; for 24h; Reagent/catalyst; Sealed tube; Inert atmosphere; Irradiation; | 73% |
N-2-propynyl-4-(trifluoromethoxy)benzenamine
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
With palladium on activated charcoal; ethanolamine In water at 80℃; Inert atmosphere; | 61% |
Conditions | Yield |
---|---|
With potassium hydroxide; bromine |
4-(Trichloromethoxy)benzoyl chloride
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SbCl5; SbF3 2: aqueous NH3 3: bromine; aqueous KOH View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq.-ethanolic NaOH; aqueous H2O2 2: bromine; aqueous KOH View Scheme |
4-cyanophenyl trichloromethyl ether
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SbF3; SbCl5 2: aq.-ethanolic NaOH; aqueous H2O2 3: bromine; aqueous KOH View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aqueous NH3 2: bromine; aqueous KOH View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: PCl5; chlorine 2: SbCl5; SbF3 3: aqueous NH3 4: bromine; aqueous KOH View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: PCl5; chlorine 2: SbF3; SbCl5 3: aq.-ethanolic NaOH; aqueous H2O2 4: bromine; aqueous KOH View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: chlorine; 4-chlorobenzotrifluoride / 90 - 100 °C / UV-irradiation 2: hydrogen fluoride / 80 °C / 22502.3 - 26252.6 Torr / Inert atmosphere; Autoclave 3: sulfuric acid; nitric acid / dichloromethane / 2 h / 0 - 30 °C 4: iron; hydrogenchloride / methanol / 2 h / 60 - 65 °C View Scheme |
(trichloromethoxy)benzene
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrogen fluoride / 80 °C / 22502.3 - 26252.6 Torr / Inert atmosphere; Autoclave 2: sulfuric acid; nitric acid / dichloromethane / 2 h / 0 - 30 °C 3: iron; hydrogenchloride / methanol / 2 h / 60 - 65 °C View Scheme |
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / methanol / 5 °C 2: formic acid; potassium hydroxide; / ethanol / 1 h / 70 °C View Scheme |
4-(trifluoromethoxy)aniline
N-tert-butyloxycarbonylpiperidin-4-one
4-(4-trifluoromethoxyaniline)piperidin-1-yl-formic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride; acetic acid In dichloromethane at 20℃; for 18h; Inert atmosphere; | 100% |
4-(trifluoromethoxy)aniline
5-carboethoxypyridine-2-carboxylic acid
ethyl 6-((4-(trifluoromethoxy)phenyl)carbamoyl)nicotinate
Conditions | Yield |
---|---|
With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide at 20℃; | 100% |
4-(trifluoromethoxy)aniline
1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-4-chloro-6-(methylthio)-1H-pyrazolo[3,4-d]pyrimidine
1-((1-benzyl-1H-1,2,3-triazol-4-yl)methyl)-6-(methylthio)-N-(4-(trifluoromethoxy)phenyl)-1H-pyrazolo[3,4-d]pyrimidin-4-amine
Conditions | Yield |
---|---|
In ethanol for 12h; Reflux; Inert atmosphere; | 100% |
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
In toluene at 80℃; for 24h; Inert atmosphere; | 100% |
4-(trifluoromethoxy)aniline
5-fluoro-2H-benzo[d][1,3]-oxazine-2,4(1H)-dione
Conditions | Yield |
---|---|
In toluene for 4h; Reflux; | 100% |
Conditions | Yield |
---|---|
In toluene for 4h; Reflux; | 100% |
5-bromo-3-pyridinecarboxylic acid
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 6h; | 100% |
Conditions | Yield |
---|---|
With acetic anhydride In acetic acid | 99.9% |
4-(trifluoromethoxy)aniline
2,6-dibromo-4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
With sulfuric acid; dihydrogen peroxide; sodium bromide at 30 - 55℃; for 3h; Reagent/catalyst; | 99.2% |
With bromine chloride; triethylamine In chloroform at 35℃; for 12h; Solvent; Reagent/catalyst; Temperature; | 90% |
With N-Bromosuccinimide In acetonitrile at 20℃; for 12h; | 89% |
With bromine; acetic acid at 20℃; for 4.5h; Molecular sieve; |
4-(trifluoromethoxy)aniline
trichloromethyl chloroformate
1-isocyanato-4-trifluoromethoxy-benzene
Conditions | Yield |
---|---|
In tetrahydrofuran for 0.75h; Reflux; | 99% |
In tetrahydrofuran for 0.75h; Reflux; | 99% |
With pyrographite In ethyl acetate Heating; | |
Stage #1: 4-(trifluoromethoxy)aniline With hydrogenchloride In ethyl acetate Stage #2: trichloromethyl chloroformate In toluene for 2.5h; Reflux; Inert atmosphere; |
di-tert-butyl dicarbonate
4-(trifluoromethoxy)aniline
tert-butyl N-(4-trifluoromethoxyphenyl)carbamate
Conditions | Yield |
---|---|
In toluene at 100℃; | 99% |
In toluene for 2h; Reflux; | 99% |
With Amberlyst A21 In neat (no solvent) at 20℃; for 0.416667h; Green chemistry; | 92% |
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane at -75℃; | 99% |
thiophosgene
4-(trifluoromethoxy)aniline
1-isothiocyanato-4-(trifluoromethoxy)benzene
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane; water at 23℃; for 1h; | 99% |
With sodium hydroxide In chloroform; water at 0℃; for 24h; | 72% |
With triethylamine In dichloromethane at 20℃; for 1h; |
4-(trifluoromethoxy)aniline
cis-1,2-diphenyloxirane
(1S,2S)-1,2-diphenyl-2-(4-(trifluoromethoxy)phenylamino)ethanol
Conditions | Yield |
---|---|
With indium(III) triflate; C28H48N4O4 In tetrahydrofuran at 0℃; for 69h; Molecular sieve; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 99% |
1,3,5-trichloro-2,4,6-triazine
4-(trifluoromethoxy)aniline
4,6-dichloro-N-(4-trifluoromethoxyphenyl)-1,3,5-triazin-2-amine
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran at 0 - 20℃; for 17h; | 99% |
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
With pyridine; oxygen; copper; ammonium bromide In toluene at 100℃; under 760.051 Torr; | 99% |
With copper-manganese spinel oxide In ethyl acetate at 80℃; for 3h; | 94% |
With Ag/C; potassium hydroxide In dimethyl sulfoxide at 60℃; under 760.051 Torr; for 24h; Catalytic behavior; Green chemistry; | 67% |
4-(trifluoromethoxy)aniline
2,3,6-trifluorobenzaldehyde
Conditions | Yield |
---|---|
In toluene at 110℃; for 96h; Dean-Stark; | 99% |
Conditions | Yield |
---|---|
In toluene at 110℃; for 96h; Dean-Stark; | 99% |
In toluene for 96h; Dean-Stark; Reflux; |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 18h; Schlenk technique; Inert atmosphere; Darkness; | 99% |
Conditions | Yield |
---|---|
Stage #1: 3-bromo-3-methyl-2-indolinone With nickel(II) tetrafluoroborate hexahydrate; C42H66N4O8 In ethyl acetate at 35℃; for 0.583333h; Stage #2: With N-ethyl-N,N-diisopropylamine In ethyl acetate at 0℃; for 0.166667h; Stage #3: 4-(trifluoromethoxy)aniline In ethyl acetate at 0℃; for 24h; enantioselective reaction; | 99% |
4-(trifluoromethoxy)aniline
t-butyl 2-diazopropanoate
Conditions | Yield |
---|---|
With C32H30N4O4; copper(l) chloride In dichloromethane at 0℃; for 18h; Inert atmosphere; Molecular sieve; optical yield given as %ee; enantioselective reaction; | 98% |
4-(trifluoromethoxy)aniline
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate In water at 100℃; for 0.166667h; Microwave irradiation; Green chemistry; | 98% |
With sodium t-butanolate In neat (no solvent) at 20℃; for 3h; Inert atmosphere; Glovebox; | 97% |
Conditions | Yield |
---|---|
In ethanol at 120℃; for 1h; | 98% |
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 20℃; for 2h; | 97.79% |
With triethylamine In dichloromethane at 0℃; for 4h; | |
With triethylamine In acetone at 0 - 20℃; |
Conditions | Yield |
---|---|
With dmap; triethylamine In 1,2-dichloro-ethane at 0 - 15℃; for 2h; | 97.4% |
With sodium hydrogencarbonate In dichloromethane; water at 10 - 25℃; for 3h; | 95.7% |
Stage #1: 4-(trifluoromethoxy)aniline With triethylamine In 1,2-dichloro-ethane at 0℃; for 0.166667h; Stage #2: methyl chloroformate In 1,2-dichloro-ethane at 0 - 20℃; | 92.8% |
Conditions | Yield |
---|---|
In acetic acid | 97% |
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; trifuran-2-yl-phosphane In dichloromethane at 20℃; for 12h; | 97% |
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
With N,N-diisopropyl-2,4,8,10-tetra(naphthalen-2-yl)dibenzo[d,f][1,3,2]dioxaphosphepin-6-amine; bis(dibenzylideneacetone)-palladium(0) In tetrahydrofuran at 25℃; for 36h; Schlenk technique; Inert atmosphere; regioselective reaction; | 97% |
6-bromo-4-chloroquinozoline
4-(trifluoromethoxy)aniline
Conditions | Yield |
---|---|
In isopropyl alcohol at 90℃; for 4h; | 96.1% |
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