Puyang Huicheng Electronic Material Co., Ltd was founded in 2002, which is focus on high complex new type intermediates and fine chemical custom synthesis, LED&OLED materials and related intermediates, catalyst design and synthesis.
Cas:5122-95-2
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:5122-95-2
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inquiryHebei yanxi chemical co., LTD is a professional research, development and production 2-phenylacetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carbon environ
Cas:5122-95-2
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Cas:5122-95-2
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:5122-95-2
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Cas:5122-95-2
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/167.html Product Name Biphenyl-3-boronic acid CAS No. 5122-95-2
Cas:5122-95-2
Min.Order:1 Gram
FOB Price: $66.0
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:5122-95-2
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inquiryProduct Name 3-Biphenylboronic acid CAS No. 5122-95-2 Appearance White Crystalline Powder Molecular
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Cas:5122-95-2
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inquiryBiphenyl-3-boronic acid CAS:5122-95-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
Cas:5122-95-2
Min.Order:1 Gram
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Cas:5122-95-2
Min.Order:1 Kilogram
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inquiryAbout Product Details
Cas:5122-95-2
Min.Order:500 Kilogram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
Cas:5122-95-2
Min.Order:100 Gram
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Cas:5122-95-2
Min.Order:100 Gram
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Cas:5122-95-2
Min.Order:100 Gram
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:5122-95-2
Min.Order:1 Gram
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inquiryWe're in good position to supply OLED intermediates . In the past 25 years, we have won technical support from several well-known universities and institutes. We supply good quality Biphenyl-3-boronic acid CAS# 5122-95-2 at competitive pric
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Product Name: Biphenyl-3-boronic acid Synonyms: 3-Biphenylboronic Acid (contains varying amounts of Anhydride);Biphenyl-3-boronica;biphenyl-3-ylboronic acid(SALTDATA: FREE);2-phenylphenyl hydrogen boronate;3-Biphenylboronic Acid ;Biphenyl-3-bor
Cas:5122-95-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
Stage #1: 3-bromobiphenyl With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 2h; Stage #2: Trimethyl borate In tetrahydrofuran at -78 - 20℃; Stage #3: With hydrogenchloride In tetrahydrofuran at 20℃; for 2h; Further stages.; | 75% |
With hydrogenchloride; n-butyllithium In tetrahydrofuran soln. of n-BuLi in hexanes added dropwise to soln. of biphenyl compd. at-78°C under Ar, kept at this temp. for 2 h, soln. of borate adde d over 30 min, allowed to warm to room temp. overnight, 10% aq. HCl added, stirred for 2 h at room temp.; extd. into Et2O, washed with concd. soln. of Na2CO3 then with H2O, evapd., recrystd. twice from H2O/EtOH (95/5); | 75% |
Stage #1: 3-bromobiphenyl With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere; Stage #2: Trimethyl borate In tetrahydrofuran; hexane for 24h; | 65% |
With hydrogenchloride; n-butyllithium In tetrahydrofuran; hexane BuLi soln. (hexane) addn. to biphenylbromide soln. (THF), mixt. stirring1 h, mixt. addn. to B-compd. soln. (THF) via canula (N2) at -78° C., stirring 1 h, gradual warming to room temp., aq. HCl addn., stirringat room temp. 15 h, solvent removal; under reduced pressure, Et2O addn., org. layer sepn., drying (MgSO4), soln. concn.. oil triturating with hexane, solid repptn. from MeOH/H2O; | 43% |
With hydrogenchloride; tert.-butyl lithium In water; pentane |
Conditions | Yield |
---|---|
Stage #1: 3-bromobiphenyl With n-butyllithium In tetrahydrofuran; hexane at -80℃; for 1h; Inert atmosphere; Stage #2: With Trimethyl borate In tetrahydrofuran; hexane at -80 - 20℃; for 4h; Stage #3: With hydrogenchloride; water In tetrahydrofuran; hexane for 2h; | 55% |
Multi-step reaction with 2 steps 1.1: n-BuLi / -78 °C 1.2: -78 - 20 °C 2.1: aq. HCl View Scheme | |
Stage #1: 3-bromobiphenyl With magnesium In tetrahydrofuran Stage #2: With Trimethyl borate Stage #3: With hydrogenchloride Further stages.; |
Conditions | Yield |
---|---|
With hydrogenchloride; n-butyllithium In tetrahydrofuran; hexane BuLi soln. (hexane) addn. to biphenylbromide soln. (THF), mixt. stirring1 h, mixt. addn. to B-compd. soln. (THF) via canula (N2) at -78° C., stirring 1 h, gradual warming to room temp., aq. HCl addn., stirringat room temp. 15 h, solvent removal; under reduced pressure, Et2O addn., org. layer sepn., drying (MgSO4), soln. concn.. oil triturating with hexane, solid repptn. from MeOH/H2O; | 40% |
boric acid tributyl ester
[(1,1'-biphenyl)-3-yl]magnesium bromide
3-Biphenylboronic acid
Conditions | Yield |
---|---|
With diethyl ether at -70℃; und anschliessenden Hydrolyse; |
3-Biphenylboronic acid
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: Pd(PPh3)4; Na2CO3 / 1,2-dimethoxy-ethane / 80 °C 2.1: n-BuLi / -78 °C 2.2: -78 - 20 °C 3.1: aq. HCl View Scheme | |
Multi-step reaction with 2 steps 1.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; ethanol / 3 h / 90 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere 2.2: 24 h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: Pd(PPh3)4; Na2CO3 / 1,2-dimethoxy-ethane / 80 °C 2.1: n-BuLi / -78 °C 2.2: -78 - 20 °C 3.1: aq. HCl View Scheme |
Conditions | Yield |
---|---|
Stage #1: 3-bromobiphenyl With n-butyllithium In diethyl ether; hexane; toluene at -30 - 0℃; for 1h; Stage #2: Triisopropyl borate In diethyl ether; hexane; toluene at -70 - 20℃; for 1h; Stage #3: With hydrogenchloride; water In diethyl ether; hexane; toluene | |
With tert.-butyl lithium In diethyl ether; pentane |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene; ethanol / 3 h / 90 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere 2.2: 24 h View Scheme |
9-bromo-N-(tert-butyl)-3,4-dihydro-2H,6H-pyrimido[1,2-c][1,3]benzothiazin-6-imine
3-Biphenylboronic acid
9-[(1-1’-biphenyl)-3-yl]-N-(tert-butyl)-3,4-dihydro-2H,6H-pyrimido[1,2-c][1,3]benzothiazin-6-imine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium carbonate In ethanol; water; toluene for 1h; Suzuki-Miyaura Coupling; Reflux; | 100% |
2-chloro-4,5-dimethoxypyrimidine
3-Biphenylboronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,4-dioxane; water for 8h; Suzuki Coupling; Reflux; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: C25H27N3O3 With trichlorophosphate In toluene at 100℃; for 0.5h; Microwave irradiation; Stage #2: 3-Biphenylboronic acid With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In 1,4-dioxane at 90℃; for 16h; Stage #3: With hydrogenchloride In tetrahydrofuran; water at 20℃; | 100% |
methyl o-formylbenzoate
3-Biphenylboronic acid
3-(biphenyl-3-yl)-3H-isobenzofuran-1-one
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); C27H30N2S(1+)*Cl(1-); cesium fluoride In toluene at 80℃; for 1h; Inert atmosphere; | 99% |
3-Biphenylboronic acid
2,4,6-tris(biphenyl-3-yl)boroxine
Conditions | Yield |
---|---|
In toluene for 2h; Reflux; Dean-Stark; Inert atmosphere; | 99% |
In toluene for 1h; Reflux; Molecular sieve; |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 70℃; for 8h; Inert atmosphere; | 99% |
Stage #1: bromochlorobenzene; 3-Biphenylboronic acid In ethanol; toluene Inert atmosphere; Stage #2: With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene at 70℃; for 8h; Inert atmosphere; | 99% |
With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate In 1,2-dimethoxyethane; water for 4h; Inert atmosphere; Reflux; | 4.11 g |
but-3-enoic acid
3-Biphenylboronic acid
4-([1,1'-biphenyl]-3-yl)butanoic acid
Conditions | Yield |
---|---|
With propan-1-ol; bis(1,5-cyclooctadiene)nickel (0); potassium tert-butylate; 4,4-dibenzyl-2-(pyridin-2-yl)-4,5-dihydrooxazole at 60℃; Sealed tube; regioselective reaction; | 99% |
3-Biphenylboronic acid
3-bromo-4-chloropyrazolo<3,4-d>pyrimidine
3-chloro-aniline
Conditions | Yield |
---|---|
Stage #1: 3-bromo-4-chloropyrazolo<3,4-d>pyrimidine; 3-chloro-aniline With acetic acid In 1,4-dioxane at 150℃; for 0.166667h; microwave irradiation; Stage #2: 3-Biphenylboronic acid With potassium phosphate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In 1,4-dioxane at 180℃; for 0.166667h; Suzuki coupling; microwave irradiation; | 98% |
Conditions | Yield |
---|---|
With pyridine; oxygen; copper diacetate In α,α,α-trifluorotoluene at 20℃; for 48h; | 98% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In water; toluene at 120℃; for 5h; | 98% |
2-(4-fluorophenyl)-3-iodo-6-phenylimidazo[1,2-a]pyridine
3-Biphenylboronic acid
3-(biphenyl-3-yl)-2-(4-fluorophenyl)-6-phenylimidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water at 100℃; for 4h; Suzuki Coupling; Inert atmosphere; | 98% |
3-Biphenylboronic acid
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate In 1,4-dioxane; water at 100℃; for 6h; | 98% |
3-Biphenylboronic acid
diphenyl(2,2,2-trifluoroethyl)sulfonium trifluoromethanesulfonate
1,3-diphenylbenzene
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); sodium hydrogencarbonate In N,N-dimethyl-formamide at 60℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere; Glovebox; Sealed tube; | 98% |
(5-bromothiazol-2-yl)methylcarbamic acid tert-butyl ester
3-Biphenylboronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,2-dimethoxyethane; water at 100℃; for 18h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; sodium carbonate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl In 1,4-dioxane; water at 80℃; for 2h; enantioselective reaction; | 98% |
3-Biphenylboronic acid
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In water; toluene at 110℃; for 24h; Inert atmosphere; | 98% |
3-Biphenylboronic acid
sodium methansulfinate
3-(methanesulfonyl)-1,1'-biphenyl
Conditions | Yield |
---|---|
With copper diacetate; 4 Angstroem MS; potassium carbonate In dimethyl sulfoxide at 20℃; for 16h; | 97% |
3-Biphenylboronic acid
Conditions | Yield |
---|---|
With potassium phosphate; bis(dibenzylideneacetone)-palladium(0); tricyclohexylphosphine In water; toluene for 7h; Suzuki Coupling; Inert atmosphere; Reflux; | 97% |
Conditions | Yield |
---|---|
With C35H40N4O9(2+)*2Cl(1-); palladium diacetate; potassium hydroxide In ethanol at 100℃; for 1.5h; Suzuki Coupling; Green chemistry; | 97% |
3-Biphenylboronic acid
1-iodo-2-((2-methylallyl)oxy)benzene
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); (R)-N-((S)-(3,5-di-tert-butyl-4-methoxyphenyl)(2-(dicyclohexylphosphanyl)phenyl)methyl)-N,2-dimethylpropane-2-sulfinamide; potassium hydroxide In toluene at 20 - 85℃; Inert atmosphere; Sealed tube; enantioselective reaction; | 97% |
1-Bromo-3-iodobenzene
3-Biphenylboronic acid
3-bromo-1,1′: 3′1″-terphenyl
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In water; toluene for 8h; Suzuki Coupling; Heating / reflux; | 96% |
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; water; toluene for 10h; Inert atmosphere; Reflux; | 93% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 6h; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 12h; Inert atmosphere; | 96% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran at 80℃; for 12h; Inert atmosphere; | 96% |
3-Biphenylboronic acid
Conditions | Yield |
---|---|
With [(dppe)Pd(H2O)2](OTf)2 In 1,4-dioxane; water at 30 - 35℃; for 6h; | 96% |
3-Biphenylboronic acid
2-(acetylamino)-5-benzyl-3-bromopyridine N-oxide
2-(acetylamino)-5-benzyl-3-(3-biphenylyl)pyridine N-oxide
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; water; toluene at 90 - 95℃; for 17h; | 95% |
3-Biphenylboronic acid
5-Bromo-2,2-dimethoxyindane-1,3-dione
5-Biphenyl-3-yl-2,2-dimethoxy-indan-1,3-dione
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol; benzene for 6h; Heating; | 95% |
Conditions | Yield |
---|---|
With caesium carbonate; bis(η3-allyl-μ-chloropalladium(II)) In 1,4-dioxane at 90℃; for 20h; Suzuki-Miyaura cross-coupling reaction; | 95% |
3-(4-bromophenyl)-1-(pyridin-2-yl)-1H-pyrazol-5-yl t-butyl carbonate
3-Biphenylboronic acid
tert-butyl 1-(2-pyridinyl)-3-[4-(3'-phenyl)biphenyl]-5-pyrazolyl carbonate
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate In 1,4-dioxane at 100℃; for 1h; Suzuki-Miyaura cross-coupling; | 95% |
1,4-bromoiodobenzene
3-Biphenylboronic acid
4-bromo-[1,1′;3′,1′′]-terphenyl
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 8h; Inert atmosphere; | 95% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 60℃; for 3h; | 93% |
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; toluene at 120℃; for 24h; | 90% |
2-(4-fluorophenyl)-3-iodo-6-(thien-3-yl)imidazo[1,2-a]pyridine
3-Biphenylboronic acid
3-(biphenyl-3-yl)-2-(4-fluorophenyl)-6-(thien-3-yl)imidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water at 100℃; for 4h; Suzuki Coupling; Inert atmosphere; | 95% |
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water Suzuki Coupling; |
3-Biphenylboronic acid
N-(tert-butoxycarbonyl)-4-iodo-L-phenylalanine methyl ester
C27H29NO4
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0) Suzuki Coupling; | 95% |
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