DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:51-24-1
Min.Order:1 Kilogram
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Min.Order:1 Kilogram
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Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Min.Order:1 Gram
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Min.Order:1 Kilogram
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inquiry3,3',5-TRIIODOTHYROACETIC ACID Basic information Product Name: 3,3',5-TRIIODOTHYROACETIC ACID Synonyms: TIRATRICOL;TRIAC;3,3',5-TRIIO
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inquiryProduct name: Tiratricol CAS No.:51-24-1 Molecule Formula:C14H9I3O4 Molecule Weight:621.93 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS SPECIFIC
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inquiry2-(4-(4-hydroxyphenoxy)-3,5-diiodophenyl)acetic acid
3,3',5-triiodothyroacetic acid
Conditions | Yield |
---|---|
With ammonia anschliessendes Behandeln mit wss. Jod-KI-Loesung; |
3,3',5-triiodothyroacetic acid ethyl ester
A
3,3',5-triiodothyroacetic acid
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; dibromodifluoromethane; copper(I) bromide; cadmium Multistep reaction. Further byproducts given. Title compound not separated from byproducts; |
[3,5-diiodo-4-(4-methoxy-phenoxy)-phenyl]-acetic acid ethyl ester
3,3',5-triiodothyroacetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aqueous HI; red phosphorus; acetic acid 2: aqueous methanol. NH3 / anschliessendes Behandeln mit wss. Jod-KI-Loesung View Scheme |
3,3',5-triiodothyroacetic acid
methylamine
2-(4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl)-N-methylacetamide
Conditions | Yield |
---|---|
Stage #1: 3,3',5-triiodothyroacetic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran at 50℃; for 2h; Sealed tube; Inert atmosphere; Stage #2: methylamine In tetrahydrofuran at 20 - 50℃; for 16h; Inert atmosphere; | 87% |
Stage #1: 3,3',5-triiodothyroacetic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran at 50℃; for 2h; Inert atmosphere; Sealed tube; Stage #2: methylamine In tetrahydrofuran at 20 - 50℃; for 16h; Inert atmosphere; | 87% |
Stage #1: 3,3',5-triiodothyroacetic acid With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide for 0.5h; Stage #2: methylamine In N,N-dimethyl-formamide | 40% |
3,3',5-triiodothyroacetic acid
dimethyl amine
2-(4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl)-N,N-dimethylacetamide
Conditions | Yield |
---|---|
Stage #1: 3,3',5-triiodothyroacetic acid With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide for 0.5h; Stage #2: dimethyl amine In N,N-dimethyl-formamide | 60% |
morpholine
3,3',5-triiodothyroacetic acid
2-(4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl)-1-morpholinoethanone
Conditions | Yield |
---|---|
Stage #1: 3,3',5-triiodothyroacetic acid With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide for 0.5h; Stage #2: morpholine In N,N-dimethyl-formamide | 43% |
3,3',5-triiodothyroacetic acid
2-(4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl)acetamide
Conditions | Yield |
---|---|
Stage #1: 3,3',5-triiodothyroacetic acid With thionyl chloride for 2h; Reflux; Stage #2: With ammonium hydroxide In water; toluene for 0.0833333h; | 40% |
3,3',5-triiodothyroacetic acid
1-pentanamine
2-(4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl)-N-pentylacetamide
Conditions | Yield |
---|---|
Stage #1: 3,3',5-triiodothyroacetic acid With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide for 0.5h; Stage #2: n-Pentylamine In N,N-dimethyl-formamide | 36% |
piperidine
3,3',5-triiodothyroacetic acid
2-(4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl)-1-(piperidin-1-yl)ethanone
Conditions | Yield |
---|---|
Stage #1: 3,3',5-triiodothyroacetic acid With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide for 0.5h; Stage #2: piperidine In N,N-dimethyl-formamide | 31% |
methanesulfonamide
3,3',5-triiodothyroacetic acid
2-(4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl)-N-(methylsulfonyl)acetamide
Conditions | Yield |
---|---|
Stage #1: 3,3',5-triiodothyroacetic acid With 1,1'-carbonyldiimidazole In dichloromethane at 0 - 20℃; for 1h; Stage #2: methanesulfonamide With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane | 21% |
benzenesulfonamide
3,3',5-triiodothyroacetic acid
2-(4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl)-N-(phenylsulfonyl)acetamide
Conditions | Yield |
---|---|
Stage #1: 3,3',5-triiodothyroacetic acid With 1,1'-carbonyldiimidazole In dichloromethane at 0 - 20℃; Stage #2: benzenesulfonamide With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane | 16% |
Stage #1: 3,3',5-triiodothyroacetic acid With 1,1'-carbonyldiimidazole In dichloromethane at 0 - 20℃; for 1h; Stage #2: benzenesulfonamide With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane | 16% |
3,3',5-triiodothyroacetic acid
aniline
2-(4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl)-N-phenylacetamide
Conditions | Yield |
---|---|
Stage #1: 3,3',5-triiodothyroacetic acid With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide for 0.5h; Stage #2: aniline In N,N-dimethyl-formamide | 16% |
Stage #1: 3,3',5-triiodothyroacetic acid With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide for 0.5h; Stage #2: aniline In N,N-dimethyl-formamide | 16% |
3,3',5-triiodothyroacetic acid
diethylamine
N,N-diethyl-2-(4-(4-hydroxy-3-iodophenoxy)-3,5-diiodophenyl)acetamide
Conditions | Yield |
---|---|
Stage #1: 3,3',5-triiodothyroacetic acid With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide for 0.5h; Stage #2: diethylamine In N,N-dimethyl-formamide | 8% |
3,3',5-triiodothyroacetic acid
4-(4-Hydroxy-3-iod-phenoxy)-3,5-diiod-phenethylalkohol
Conditions | Yield |
---|---|
With diborane In tetrahydrofuran |
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