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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti

High purity 3-Methoxypropylamine TOP1 supplier in China

Cas:5332-73-0

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Hangzhou Ocean Chemical Co., Ltd.

★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support ★.Shortest delivery time . Appearance:Colorless transparent liquid Storage:Store in dry, cool and ventilated

3-Methoxypropylamine

Cas:5332-73-0

Min.Order:170 Kilogram

FOB Price: $3.0 / 3.2

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 3-Methoxy-Propylamine supplier in China

Cas:5332-73-0

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com Product Name 3-Methoxypropylamine CAS No.

3-Methoxypropylamine

Cas:5332-73-0

Min.Order:1 Gram

FOB Price: $8.0

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 3-Methoxy-Propylamine

Cas:5332-73-0

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Large Stock 99.0% γ-Methoxy propyl amine 5332-73-0 Producer

Cas:5332-73-0

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

Methoxy Propyl Amine

Cas:5332-73-0

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

3-Methoxypropylamine

Cas:5332-73-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

3-Methoxypropylamine

Cas:5332-73-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu

3-Methoxypropylamine CAS 5332-73-0

Cas:5332-73-0

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 5332-73-0 with best quality

Cas:5332-73-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

3-Methoxypropylamine CAS5332-73-0

Cas:5332-73-0

Min.Order:1 Kilogram

FOB Price: $7.0 / 9.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

English name: 3-Methoxypropylamine English synonyms: 3-METHOXYPROPYLAMINE FOR SYNTHESIS;3-MethoxypropylaMine, 99+%, 99+%;.gamma.-Methoxypropaneamine;1-Propanamine,3-methoxy-;3-methoxy-1-propanamin;3-Methoxy

3-Methoxypropylamine CAS:5332-73-0

Cas:5332-73-0

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in t

Favorable price 5332-73-0 FENTAMINE MOPA 99.5% 5332-73-0 FENTAMINE MOPA for sale

Cas:5332-73-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

3-Methoxypropylamine 5332-73-0

Cas:5332-73-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Xi'an Faithful Biotech Co., Ltd.

We are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

3-Methoxypropylamine with CAS:5332-73-0

Cas:5332-73-0

Min.Order:1 Kilogram

FOB Price: $21.0 / 31.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

Beluga chemical professional supply High quality 3-Methoxypropylamine CAS 5332-73-0 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in

High quality 3-Methoxypropylamine CAS 5332-73-0

Cas:5332-73-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS 5332-73-0 3-Methoxypropylamine

Cas:5332-73-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Lonwin Chemical Group Limited

3-Methoxypropylamine CAS:5332-73-0 Specification Product Name 3-Methoxypropylamine CAS No. 5332-73-0 Appearance Colorless clear liquid Assay

Factory Supply 3-Methoxypropylamine

Cas:5332-73-0

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

3-Methoxypropylamine

Cas:5332-73-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Fandachem Co.,Ltd

Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting MOPA (3-Methoxypropylamine;3-Aminopropyl Methyl Ether;3-methoxy 1-propylamine) CAS: 5332-73-0, Please contact us by email freely. We are

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

3-Methoxy-Propylamine

Cas:5332-73-0

Min.Order:0

Negotiable

Type:Manufacturers

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s

3-Methoxy 1-Propylamine

Cas:5332-73-0

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

γ-Methoxy propyl amine

Cas:5332-73-0

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

3-Methoxypropylamine

Cas:5332-73-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Fonlynn Health Technology Co., Ltd.

Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd

3-Methoxypropylamine

Cas:5332-73-0

Min.Order:0

Negotiable

Type:Trading Company

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

3-Methoxypropylamine

Cas:5332-73-0

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

3-Methoxypropylamine Manufacturer/High quality/Best price/In stock

Cas:5332-73-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Buy Top Quality3-Methoxypropylamine

Cas:5332-73-0

Min.Order:0

Negotiable

Type:Trading Company

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Synthetic route

C6H5CHNCH2CH2CH2OCH3
105427-51-8

C6H5CHNCH2CH2CH2OCH3

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
Stage #1: C6H5CHNCH2CH2CH2OCH3 With hydrogenchloride In cyclohexane at -10 - 0℃; for 14h;
Stage #2: With sodium carbonate In dichloromethane at -10 - 0℃; for 12h;
99.42%
3-Methoxypropionitrile
110-67-8

3-Methoxypropionitrile

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
With hydrogen In methanol at 105 - 110℃; under 15001.5 - 22502.3 Torr; for 0.5h; Temperature; Pressure; Solvent; Autoclave;97.2%
With hydrogen at 60 - 98℃; under 1500.15 - 22502.3 Torr; for 6h; Temperature;95%
With hydrogenchloride; platinum(IV) oxide; hydrogen In ethanol under 2280 Torr; for 4h;30%
With ammonia; hydrogen; Rh catalyst under 51485.6 Torr;
3-Methoxypropionitrile
110-67-8

3-Methoxypropionitrile

A

bis-(3-methoxy-propyl)-amine
14676-58-5

bis-(3-methoxy-propyl)-amine

B

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
With ammonia; nickel at 90℃; Hydrogenation.unter Druck;
With nickel at 110℃; Hydrogenation.unter Druck;
(3-Methoxy-propyl)-[2-methyl-prop-(Z)-ylidene]-amine
22483-13-2

(3-Methoxy-propyl)-[2-methyl-prop-(Z)-ylidene]-amine

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
In water at 35℃; Equilibrium constant;
2-<(3-methoxy)propyl>-isoindole-1,3(2H)-dione
41081-98-5

2-<(3-methoxy)propyl>-isoindole-1,3(2H)-dione

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
With hydrazine
dimethyl sulfate
77-78-1

dimethyl sulfate

propan-1-ol-3-amine
156-87-6

propan-1-ol-3-amine

A

3-(Dimethylamino)-1-propyl Methyl Ether
20650-07-1

3-(Dimethylamino)-1-propyl Methyl Ether

B

N-[3-(methoxy)propyl]-N-methylamine
55612-03-8

N-[3-(methoxy)propyl]-N-methylamine

C

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

Conditions
ConditionsYield
With calcium hydride 1.) THF, room temp., 1 h; 2.) room temp., 1 h; Yield given. Multistep reaction;
With sodium hydride 1.) THF, room temp., 1 h; 2.) room temp., 1 h; Yield given. Multistep reaction;
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

tert-butyl (3-methoxypropyl)carbamate
911300-60-2

tert-butyl (3-methoxypropyl)carbamate

Conditions
ConditionsYield
In chloroform for 16h; Heating / reflux;100%
2-hydroxy-3-(1-methyl-1-phenylethyl)benzaldehyde
165450-61-3

2-hydroxy-3-(1-methyl-1-phenylethyl)benzaldehyde

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

C20H25NO2
1096704-38-9

C20H25NO2

Conditions
ConditionsYield
In ethanol at 20℃; for 6h;100%
thiophene-2-carbaldehyde
98-03-3

thiophene-2-carbaldehyde

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

3-methoxy-N-(thiophen-2-ylmethylene)propanamine
1227253-60-2

3-methoxy-N-(thiophen-2-ylmethylene)propanamine

Conditions
ConditionsYield
at 60℃; for 6h; Inert atmosphere;100%
6-chloro-3H-purine
87-42-3

6-chloro-3H-purine

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

(3-methoxypropyl)(3H-purin-6-yl)amine

(3-methoxypropyl)(3H-purin-6-yl)amine

Conditions
ConditionsYield
In butan-1-ol at 100℃; for 16h;100%
(*S)-3-(3-((7'-chloro-1',1'-dioxidospiro[cyclopropane-1,4'-pyrido[2,3-b][1,4,5]oxathiazepin]-2'(3'H)-yl)methyl)-4-methylphenyl)-3-(8-methyl-3-(trifluoromethyl)-[1,2,4]triazolo[4,3-a]pyridin-7-yl)propanoic acid

(*S)-3-(3-((7'-chloro-1',1'-dioxidospiro[cyclopropane-1,4'-pyrido[2,3-b][1,4,5]oxathiazepin]-2'(3'H)-yl)methyl)-4-methylphenyl)-3-(8-methyl-3-(trifluoromethyl)-[1,2,4]triazolo[4,3-a]pyridin-7-yl)propanoic acid

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

ethyl (*S)-3-(3-((7'-((3-methoxypropyl)amino)-1‘,1‘-dioxidospiro[cyclopropane-1,4’-pyrido[2,3-b] [1 ,4,5]oxathiazepin]-2’(3’H)-yl)methyl)-4-methylphenyl)-3- (8-methyl-3-(trifluoromethyl)-[1,2,4]triazolo[4,3-a] pyridine-7-yl)propanoate

ethyl (*S)-3-(3-((7'-((3-methoxypropyl)amino)-1‘,1‘-dioxidospiro[cyclopropane-1,4’-pyrido[2,3-b] [1 ,4,5]oxathiazepin]-2’(3’H)-yl)methyl)-4-methylphenyl)-3- (8-methyl-3-(trifluoromethyl)-[1,2,4]triazolo[4,3-a] pyridine-7-yl)propanoate

Conditions
ConditionsYield
In dimethyl sulfoxide at 110℃; for 1h; Microwave irradiation;100%
4-fluoro-N-methyl-3-nitrobenzamide
475216-25-2

4-fluoro-N-methyl-3-nitrobenzamide

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

4-(3-methoxypropylamino)-3-nitrophenyl-N-methylbenzamide
658700-24-4

4-(3-methoxypropylamino)-3-nitrophenyl-N-methylbenzamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃;99%
(1R,2S)-2-{[(3aR,4R,9bR)-4-phenyl-2,3,3a,4,5,9b-hexahydro-1H-pyrrolo[3,2-c]quinolin-1-yl]carbonyl}cyclohexylamine dihydrochloride

(1R,2S)-2-{[(3aR,4R,9bR)-4-phenyl-2,3,3a,4,5,9b-hexahydro-1H-pyrrolo[3,2-c]quinolin-1-yl]carbonyl}cyclohexylamine dihydrochloride

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

N-(3-methoxypropyl)-N'-((1R,2S)-2-{[(3aR,4R,9bR)-4-phenyl-2,3,3a,4,5,9b-hexahydro-1H-pyrrolo[3,2-c]quinolin-1-yl]carbonyl}cyclohexyl)urea

N-(3-methoxypropyl)-N'-((1R,2S)-2-{[(3aR,4R,9bR)-4-phenyl-2,3,3a,4,5,9b-hexahydro-1H-pyrrolo[3,2-c]quinolin-1-yl]carbonyl}cyclohexyl)urea

Conditions
ConditionsYield
Stage #1: (1R,2S)-2-{[(3aR,4R,9bR)-4-phenyl-2,3,3a,4,5,9b-hexahydro-1H-pyrrolo[3,2-c]quinolin-1-yl]carbonyl}cyclohexylamine dihydrochloride; 1,1'-carbonyldiimidazole With triethylamine In DMF (N,N-dimethyl-formamide) at 0℃; for 1h;
Stage #2: 3-methoxypropylamine With triethylamine In DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 14h;
99%
2,4-bis(benzyloxy)-5-bromobenzoic acid
912545-10-9

2,4-bis(benzyloxy)-5-bromobenzoic acid

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

2,4-bis-benzyloxy-5-bromo-N-(3-methoxypropyl)benzamide
1143623-80-6

2,4-bis-benzyloxy-5-bromo-N-(3-methoxypropyl)benzamide

Conditions
ConditionsYield
Stage #1: 2,4-bis(benzyloxy)-5-bromobenzoic acid With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide at 20℃; for 2h;
Stage #2: 3-methoxypropylamine In N,N-dimethyl-formamide at 20℃; Product distribution / selectivity;
99%
pyridine-2-carbaldehyde
1121-60-4

pyridine-2-carbaldehyde

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

3-methoxy-N-((pyridin-2-yl)methylene)propan-1-amine
1603164-14-2

3-methoxy-N-((pyridin-2-yl)methylene)propan-1-amine

Conditions
ConditionsYield
With sodium sulfate In tetrahydrofuran at 25℃; for 72h; Inert atmosphere; Sealed tube;99%
In dichloromethane at 20℃; for 24h;78%
In methanol for 12h; Reflux;
7-(2,2-difluoroethoxy)-3-oxo-2,3-dihydro-1H-indene-4-carbonitrile

7-(2,2-difluoroethoxy)-3-oxo-2,3-dihydro-1H-indene-4-carbonitrile

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

7-(2,2-difluoroethoxy)-3-((3-methoxypropyl)imino)-2,3-dihydro-1H-indene-4-carbonitrile

7-(2,2-difluoroethoxy)-3-((3-methoxypropyl)imino)-2,3-dihydro-1H-indene-4-carbonitrile

Conditions
ConditionsYield
With trifluoroacetic acid In benzene for 6h; Reflux; Dean-Stark;99%
methyl 2-((3,4-dichlorophenyl)amino)pyrimidine-4-carboxylate

methyl 2-((3,4-dichlorophenyl)amino)pyrimidine-4-carboxylate

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

N-(3-methoxypropyl) 2-((3,4-dichlorophenyl)amino)pyrimidine-4-carboxamide

N-(3-methoxypropyl) 2-((3,4-dichlorophenyl)amino)pyrimidine-4-carboxamide

Conditions
ConditionsYield
With ammonium nitrate at 20℃; for 20h;99%
acetylacetone
123-54-6

acetylacetone

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

(CH3OC3H6)NHC(CH3)CHC(CH3)O

(CH3OC3H6)NHC(CH3)CHC(CH3)O

Conditions
ConditionsYield
at 130℃; for 0.0833333h; microwave irradiation;98%
In ethanol for 24h; Heating;98%
acetylacetone
123-54-6

acetylacetone

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

4-((3-methoxypropyl)amino)pent-3-en-2-one
124747-45-1

4-((3-methoxypropyl)amino)pent-3-en-2-one

Conditions
ConditionsYield
at 20 - 130℃; for 0.0833333h; Microwave irradiation;98%
at 20 - 130℃; Inert atmosphere; Microwave irradiation;98%
In diethyl ether for 1h; Inert atmosphere; Schlenk technique; Reflux;97%
With toluene-4-sulfonic acid In ethanol Reflux;
In diethyl ether
4-Nitrobenzenesulfonyl chloride
98-74-8

4-Nitrobenzenesulfonyl chloride

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

N-(3-methoxypropyl)-4-nitro-benzenesulfonamide
349397-17-7

N-(3-methoxypropyl)-4-nitro-benzenesulfonamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 1h;97.8%
With potassium carbonate In acetonitrile at 30℃; for 4h;
carbon monoxide
201230-82-2

carbon monoxide

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

N,N'-bis(3-methoxypropyl)urea
82138-38-3

N,N'-bis(3-methoxypropyl)urea

Conditions
ConditionsYield
Stage #1: carbon monoxide; 3-methoxypropylamine With sulfur at 80℃; under 760.051 Torr; for 4h;
Stage #2: With oxygen at 20℃; under 760.051 Torr; for 1h; Further stages.;
97%
With sulfur at 120℃;
tert-butyl (3R)-6-cyclohexyl-3-[3-({[(4-methylphenyl)sulfonyl]oxy}methyl)-1,2,4-oxadiazol-5-yl]hexanoate
348623-96-1

tert-butyl (3R)-6-cyclohexyl-3-[3-({[(4-methylphenyl)sulfonyl]oxy}methyl)-1,2,4-oxadiazol-5-yl]hexanoate

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

A

tert-butyl (3R)-6-cyclohexyl-3-{3-[(methylamino)methyl]-1,2,4-oxadiazol-5-yl}hexanoate
438630-56-9

tert-butyl (3R)-6-cyclohexyl-3-{3-[(methylamino)methyl]-1,2,4-oxadiazol-5-yl}hexanoate

B

tert-butyl (3R)-6-cyclohexyl-3-(3-{[(3-methoxypropyl)amino]methyl}-1,2,4-oxadiazol-5-yl)hexanoate

tert-butyl (3R)-6-cyclohexyl-3-(3-{[(3-methoxypropyl)amino]methyl}-1,2,4-oxadiazol-5-yl)hexanoate

Conditions
ConditionsYield
A n/a
B 97%
C19H16FN3O4
1373257-36-3

C19H16FN3O4

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

C23H26N4O5
1373257-44-3

C23H26N4O5

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 20℃;97%
aniline
62-53-3

aniline

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

N-(3-methoxypropyl)cyclohexanamine

N-(3-methoxypropyl)cyclohexanamine

Conditions
ConditionsYield
With hydrogen In neat (no solvent) at 50℃; under 760.051 Torr; for 38h;97%
4-chloro-7-(3',5'-di-O-benzoyl-2'-deoxy-2'-fluoro-β-D-arabinofuranosyl)pyrrolo<2,3-d>pyrimidine
169516-55-6

4-chloro-7-(3',5'-di-O-benzoyl-2'-deoxy-2'-fluoro-β-D-arabinofuranosyl)pyrrolo<2,3-d>pyrimidine

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

4-(3-methoxypropylamino)-9-(2'-deoxy-2'-β-fluoro-β-D-ribofuranosyl)pyrrole[2,3-d]pyrimidine

4-(3-methoxypropylamino)-9-(2'-deoxy-2'-β-fluoro-β-D-ribofuranosyl)pyrrole[2,3-d]pyrimidine

Conditions
ConditionsYield
Stage #1: 4-chloro-7-(3',5'-di-O-benzoyl-2'-deoxy-2'-fluoro-β-D-arabinofuranosyl)pyrrolo<2,3-d>pyrimidine; 3-methoxypropylamine In tetrahydrofuran at 90℃; for 12h; Sealed tube;
Stage #2: With ammonia In methanol
96.59%
2-amino-3-hydroxy-propionaldehyde
21228-53-5

2-amino-3-hydroxy-propionaldehyde

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

3-methoxypropylformamide
71172-42-4

3-methoxypropylformamide

Conditions
ConditionsYield
In carbon monoxide96%
1-tert-butyl 3-methyl (3R,5S)-5-{[(2-tert-butyl-4-chloropyrimidin-5-yl)carbonyl](2-methylpropyl)amino}piperidine-1,3-dicarboxylate
1145745-34-1

1-tert-butyl 3-methyl (3R,5S)-5-{[(2-tert-butyl-4-chloropyrimidin-5-yl)carbonyl](2-methylpropyl)amino}piperidine-1,3-dicarboxylate

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

1-tert-butyl 3-methyl (3R,5S)-5-[({2-tert-butyl-4-[(3-methoxypropyl)amino]pyrimidin-5-yl}carbonyl)(2-methylpropyl)amino]piperidine-1,3-dicarboxylate
1145745-37-4

1-tert-butyl 3-methyl (3R,5S)-5-[({2-tert-butyl-4-[(3-methoxypropyl)amino]pyrimidin-5-yl}carbonyl)(2-methylpropyl)amino]piperidine-1,3-dicarboxylate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 80℃; for 1.5h;96%
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 80℃; for 1.5h;
2-chloro-3-nitrobenzoic acid methyl ester
53553-14-3

2-chloro-3-nitrobenzoic acid methyl ester

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

methyl 2-(3-methoxypropylamino)-3-nitrobenzoate
958032-64-9

methyl 2-(3-methoxypropylamino)-3-nitrobenzoate

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran for 12h; Reflux;96%
N4-p-bromobenzoyl-2',3'-O-isopropylidene-O2,5'-cyclocytidine
1386977-60-1

N4-p-bromobenzoyl-2',3'-O-isopropylidene-O2,5'-cyclocytidine

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

N4-p-bromobenzoyl-N2-(3-methoxypropyl)amino-N1-(2',3'-O-isopropylidene-β-D-ribofuranosyl)-2(1H)-pyrimidinamine hydrochloride
1386977-61-2

N4-p-bromobenzoyl-N2-(3-methoxypropyl)amino-N1-(2',3'-O-isopropylidene-β-D-ribofuranosyl)-2(1H)-pyrimidinamine hydrochloride

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride In tetrahydrofuran at 0℃; for 0.75h;96%
3,5-di-tert-butyl-2-hydroxybenzaldehyde
37942-07-7

3,5-di-tert-butyl-2-hydroxybenzaldehyde

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

C19H31NO2

C19H31NO2

Conditions
ConditionsYield
In methanol at 20℃; Inert atmosphere; Schlenk technique;96%
3-methoxy-2-hydroxybenzaldehyde
148-53-8

3-methoxy-2-hydroxybenzaldehyde

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

C12H17NO3

C12H17NO3

Conditions
ConditionsYield
In methanol for 4h; Reflux;96%
4-chloro-6,7-dihydro-5H-pyrimido<5,4-d><1>benzazepine
105895-97-4

4-chloro-6,7-dihydro-5H-pyrimido<5,4-d><1>benzazepine

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

(6,7-Dihydro-5H-benzo[b]pyrimido[4,5-d]azepin-4-yl)-(3-methoxy-propyl)-amine

(6,7-Dihydro-5H-benzo[b]pyrimido[4,5-d]azepin-4-yl)-(3-methoxy-propyl)-amine

Conditions
ConditionsYield
at 65 - 70℃; for 2h;95%
3,5-di-tert-butyl-2-hydroxybenzaldehyde
37942-07-7

3,5-di-tert-butyl-2-hydroxybenzaldehyde

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

(E)-2,4-di-tert-butyl-6-(((3-methoxypropyl)imino)methyl)phenol

(E)-2,4-di-tert-butyl-6-(((3-methoxypropyl)imino)methyl)phenol

Conditions
ConditionsYield
In methanol for 18h; Inert atmosphere; Schlenk technique; Reflux;95%
1-[4-(i-propyl)phenyl]-pentane-1,4-dione
1033280-93-1

1-[4-(i-propyl)phenyl]-pentane-1,4-dione

3-methoxypropylamine
5332-73-0

3-methoxypropylamine

2-(4-isopropylphenyl)-1-(3-methoxypropyl)-5-methyl-1H-pyrrole

2-(4-isopropylphenyl)-1-(3-methoxypropyl)-5-methyl-1H-pyrrole

Conditions
ConditionsYield
With toluene-4-sulfonic acid In ethanol at 160℃; under 7757.43 Torr; for 0.5h; Sealed tube; Microwave irradiation;95%
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