CAS No.123-54-6,Acetylacetone Suppliers,MSDS download

Jinan Finer Chemical Co., Ltd

Product description: Product name 2,4-Pentanedione CAS number 123-54-6 Assay ≥99.5% Appearance Colorless transparent liquid Capacity 2000mt/year Application Oranic solvent

2,4-Pentanedione

Cas:123-54-6

Min.Order:1 Kilogram

FOB Price: $12.0

Type:Lab/Research institutions

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Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

2,4-Pentanedione 123-54-6

Cas:123-54-6

Min.Order:0

Negotiable

Type:Trading Company

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Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

Amadis Chemical offer CAS#123-54-6;CAT#A805117

Cas:123-54-6

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

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Synthetic route

: 79510-57-9
3-<1-phenyl-2-(3-methyl-4-nitro-5-isoxazolyl)-ethyl>pentane-2,4-dione

A: 51978-94-0, 53557-94-1
(E)-3-methyl-4-nitro-5-styrylisoxazole

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With ethylenediamine In acetic acid for 0.5h; Heating; other substrates with o- and p-substituted phenyls as Ar;	A 100% B 100%

: 70971-86-7
diethyl 1-methyl-3-oxobut-1-enyl phosphite

: 64-19-7
acetic acid

A: 3266-66-8
acetyl diethyl phosphite

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
at 36℃; Product distribution; other vinyl phosphites;	A 72% B 94.5%
	A 72% B 94%

...Expand

: 70971-86-7
diethyl 1-methyl-3-oxobut-1-enyl phosphite

A: 3266-66-8
acetyl diethyl phosphite

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With acetic acid	A 72% B 94%

: 1313208-33-1
C8H15NOS2

: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With copper(II) choride dihydrate; water In acetonitrile at 75℃; for 2.5h;	89%

: bis(acetylacetonato)palladium(II)

: 4559-70-0
Diphenylphosphine oxide

: cis-2,4-pentanedionato-(hydrogendiphenylphosphinito-P)(diphenylphosphinito-P)Pd(II)

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
In diethyl ether under Ar, stirring for 20 h at room temp.; filtration of ppt., washing with Et2O, drying in vac.; elem. anal.;	A 88% B n/a

...Expand

: 67-64-1
acetone

polystyrylmethyl acetate: polystyrylmethyl acetate

: 123-54-6
acetylacetone

Conditions

Conditions	Yield
	87%

: 67-64-1
acetone

polystyrylmethyl benzoate: polystyrylmethyl benzoate

: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With n-butyllithium; N-tert-butyl-N-(2-polystyrylmethoxy)-ethyl)amine In tetrahydrofuran for 2h; from -78 deg C to RT;	87%

: 1825-14-5, 3950-21-8, 36402-52-5, 42075-32-1, 72345-23-4, 625-69-4
pentane-1,3-diol

: 123-54-6
acetylacetone

Conditions

Conditions	Yield
In neat (no solvent) at 20℃; for 0.05h; Microwave irradiation;	87%

: bis(2,4-pentanedionato)-nickel(II)

: 4559-70-0
Diphenylphosphine oxide

: cis-2,4-pentanedionato-(hydrogendiphenylphosphinito-P)(diphenylphosphinito-P)nickel(II)

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
In diethyl ether under Ar, stirring for 20 h at room temp.; filtration of ppt., washing with Et2O, drying in vac., dissolving in hot benzene and pptn. with Et2O; elem. anal.;	A 85% B n/a

...Expand

: 22752-34-7
diethyl 1-methyl-3-oxo-1-butenylphosphonate

: 111-27-3
hexan-1-ol

A: diethyl hexyl phosphite

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
for 1h;	A 84.6% B n/a

...Expand

: 17257-79-3
3,4-epoxy-2-pentanone

: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With tetrakis(triphenylphosphine) palladium(0); 1,2-bis-(diphenylphosphino)ethane In toluene at 140℃; for 11h;	81%

: 22752-34-7
diethyl 1-methyl-3-oxo-1-butenylphosphonate

: 108-95-2
phenol

A: 4894-60-4
diethyl phenyl phosphite

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
	A 79.4% B n/a

...Expand

: 98516-50-8
5-<2-acetyl-3-oxo-1-(3-nitrophenyl)>butylamino-3-phenylisoxazole

A: 37853-11-5
5-(3-nitrobenzylideneamino)-3-phenylisoxazole

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
at 180℃; for 1h; under reduced pressure;	A 40.2% B 78.7%

: 115-20-8
1,1,1-trichloroethanol

: 22752-34-7
diethyl 1-methyl-3-oxo-1-butenylphosphonate

A: 82564-87-2
diethyl β,β,β-trichloroethyl phosphite

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
	A 75.5% B n/a

...Expand

: 174874-85-2
(2R,3S)-2-(3-acetoxy-1-benzyl-5-oxo-pyrrolidin-2-yl)-3-oxo-butyric acid methyl ester

A: 123-54-6
acetylacetone

B: acetic acid (2R,3S)-1-benzyl-5-oxo-2-(2-oxo-propyl)-pyrrolidin-3-yl ester

Conditions

Conditions	Yield
With sodium chloride In water; dimethyl sulfoxide at 100℃; for 5h;	A 75% B 9%

: 22752-34-7
diethyl 1-methyl-3-oxo-1-butenylphosphonate

: 64-19-7
acetic acid

A: 123-54-6
acetylacetone

B: 919-19-7
diethyl acetylphosphonate

Conditions

Conditions	Yield
for 1h; Ambient temperature;	A n/a B 72%

...Expand

: 2157-56-4
pentane-2,4-dione dioxime

: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With sodium bismuthate; water; silica gel for 0.0166667h;	72%

: acetylacetone disemicarbazone

: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With water; antimony(III) chloride for 0.00305556h; Substitution; microwave irradiation;	72%

: 70971-86-7
diethyl 1-methyl-3-oxobut-1-enyl phosphite

: 100-53-8
phenylmethanethiol

A: 114105-41-8
S-benzyl O,O-diethyl phosphorothioite

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
for 96h;	A 66% B n/a

...Expand

: 109-79-5
1-butanethiol

: 70971-86-7
diethyl 1-methyl-3-oxobut-1-enyl phosphite

A: 114082-04-1
S-Butyl O,O-diethyl phosphorothioite

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
for 96h;	A 64% B n/a

...Expand

: platinum(II) bis(acetylacetonate)

: 4559-70-0
Diphenylphosphine oxide

: (Pt(((C6H5)2PO)2H)2)

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
In toluene under Ar, reflux for 8 h; hot filtration, evapn. in vac., addn. of Et2O, filtration of ppt., drying in vac.;	A 60% B n/a

...Expand

: 14284-89-0
manganese(III) acetylacetonate

A: Mn(3+)*2CH3COCHCOCH3(1-)*2(CH3)2SO*ClO4(1-)=(Mn(CH3COCHCOCH3)2((CH3)2SO)2)ClO4

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With dimethyl sulfoxide In dimethyl sulfoxide Kinetics; dissolution of Mn-complex in DMSO in presence of aq. perchloric acid (1.0 M) at 30°C; monitoring spectrophotometrically at 618 nm, extn. with aq. H2SO4 and ether, drying ether soln. over Na2SO4, distn. in vacuo (139°C, 750mm);	A n/a B 60%

: 14284-89-0
manganese(III) acetylacetonate

A: Mn(3+)*2CH3COCHCOCH3(1-)*2(CH3)2NCHO*ClO4(1-)=(Mn(CH3COCHCOCH3)2((CH3)2NCHO)2)ClO4

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With N,N-dimethyl-formamide In N,N-dimethyl-formamide Kinetics; dissolution of Mn-complex in DMF in presence of aq. perchloric acid (1.0 M) at 30°C; monitoring spectrophotometrically at 618 nm, extn. with aq. H2SO4 and ether, drying ether soln. over Na2SO4, distn. in vacuo (139°C, 750mm);	A n/a B 60%

: 14284-89-0
manganese(III) acetylacetonate

A: Mn(3+)*2CH3COCHCOCH3(1-)*2HCOOH*ClO4(1-)=(Mn(CH3COCHCOCH3)2(HCOOH)2)ClO4

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With formic acid In formic acid Kinetics; dissolution of Mn-complex in formic acid in presence of aq. perchloric acid (1.0 M) at 30°C; monitoring spectrophotometrically at 618 nm, extn. with aq. H2SO4 and ether, drying ether soln. over Na2SO4, distn. in vacuo (139°C, 750mm);	A n/a B 60%

: 14284-89-0
manganese(III) acetylacetonate

A: Mn(3+)*2CH3COCHCOCH3(1-)*2CH3OH*ClO4(1-)=(Mn(CH3COCHCOCH3)2(CH3OH)2)ClO4

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With methanol In methanol Kinetics; dissolution of Mn-complex in methanol in presence of aq. perchloric acid (1.0 M) at 30°C; monitoring spectrophotometrically at 618 nm, extn. with aq. H2SO4 and ether, drying ether soln. over Na2SO4, distn. in vacuo (139°C, 750mm);	A n/a B 60%

: 3508-78-9
3-allyl-2,4-pentanedione

: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With sulfuric acid; iodine In dimethyl sulfoxide at 60℃; for 0.5h; Acidic conditions;	59%

: 2845-83-2
4-methoxypent-3-en-2-one

: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With acetic acid; zinc for 20h;	58%

: 19451-23-1
2,2'-dimethyl-2,2'-methanediyl-bis-[1,3]dithiolane

A: 66278-18-0
(2-methyl-[1,3]dithiolan-2-yl)-propan-2-one

B: 123-54-6
acetylacetone

Conditions

Conditions	Yield
With water; 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate In tetrahydrofuran; dichloromethane at 23℃;	A 57% B 15%

: 1-{1-(4-chlorophenyl)-4-[(4-chlorophenyl)amino]-5-(2-fluorophenyl)-5-hydroxy-2-methyl-4,5-dihydro-1H-pyrrol-3-yl}ethan-1-one

: 104-15-4
toluene-4-sulfonic acid

A: 7255-72-3
4-chloroaniline p-toluenesulfonate

B: 137684-19-6
o-fluorophenylglyoxal

C: 123-54-6
acetylacetone

Conditions

Conditions	Yield
In toluene at 80℃; for 2h;	A 57% B n/a C n/a

...Expand

: 74-86-2
acetylene

A: 629-20-9
1,3,5,7-cyclooctatetraene

B: 108-88-3
toluene

C: 123-54-6
acetylacetone

D: 71-43-2
benzene

Conditions

Conditions	Yield
bis(acetylacetonate)nickel(II); calcium carbide In tetrahydrofuran at 85 - 90℃; Further byproducts given;	A 56% B n/a C n/a D 33%

...Expand

: 98-01-1
furfural

: 123-54-6
acetylacetone

: 4728-04-5
3-(furan-2-ylmethylene)pentane-2,4-dione

Conditions

Conditions	Yield
With piperidine; acetic acid In dichloromethane at 0 - 20℃; Michael Addition; Molecular sieve;	100%
With L-Lysine hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 3h; Knoevenagel Condensation;	98.3%
With cross-linked polystyrene-titanium tetrachloride complex In neat (no solvent) at 60℃; for 2h; Knoevenagel Condensation;	98%

: 619-67-0
4-Hydrazinobenzoic acid

: 123-54-6
acetylacetone

: 81282-82-8
4-(3,5-dimethyl-1H-pyrazol-1-yl)benzoic acid

Conditions

Conditions	Yield
In isopropyl alcohol for 15h; Reflux;	100%
In isopropyl alcohol for 15h; Heating / reflux;	99%
With sulfuric acid In methanol at 20℃;	90%

: 102-96-5
(2-nitroethenyl)benzene

: 123-54-6
acetylacetone

: 72709-61-6
(+/-)-3-(2-nitro-1-phenylethyl)pentane-2,4-dione

Conditions

Conditions	Yield
With N,N-dimethyl-3-trimethoxysilylpropanamine:N-(3,5-bistrifluoromethylphenyl)-N'-(3-trimethoxysilyl-1-propyl)thiourea (1:1) mesoporous silica nanoparticles at 20℃; for 3h;	100%
With squaramide-containing Dawson organo-polyoxotungstates In dichloromethane for 13h; Reagent/catalyst; Heating;	99%
With C27H18F15N7O3 In dimethyl sulfoxide at 20℃; for 3h; Michael Addition;	98%

: 123-54-6
acetylacetone

: 2835-77-0
(2-aminophenyl)(phenyl)methanone

: 13337-57-0
3-acetyl-2-methyl-4-phenylquinoline

Conditions

Conditions	Yield
With 3-methyl-1-sulfoimidazolium trichloroacetate; trichloroacetic acid In neat (no solvent) at 100℃; Friedlaender Quinoline Synthesis;	100%
With sulfuric acid; silica gel at 100℃; for 0.75h; Friedlaender synthesis;	99%
With trifluoroacetic acid at 100℃; for 0.116667h;	99%

: 123-54-6
acetylacetone

: 3043-28-5
3-bromopentane-2,4-dione

Conditions

Conditions	Yield
With bromine at 20℃; for 0.333333h;	100%
With N-Bromosuccinimide; toluene-4-sulfonic acid In dichloromethane at 20℃; for 0.166667h;	94%
With bromomalononitrile In N,N-dimethyl-formamide at 20℃; for 0.5h; Reagent/catalyst;	91%

: 123-54-6
acetylacetone

: 100-46-9
benzylamine

: 23652-86-0
(Z)-4-(benzylamino)-3-penten-2-one

Conditions

Conditions	Yield
In methanol for 12h; Heating;	100%
In neat (no solvent) at 120℃; for 2h;	100%
With montmorillonite K-10 for 24h; Ambient temperature;	99%

: 123-54-6
acetylacetone

: 1118-66-7
4-Aminopent-3-en-2-one

Conditions

Conditions	Yield
With ammonia In water at 20℃;	100%
With ammonia; silica gel at 20℃; for 24h;	99%
With ammonia at 20℃; for 48h;	98%

: 123-54-6
acetylacetone

: 29397-21-5
Diacetyldiazomethan

Conditions

Conditions	Yield
With 4-acetamidobenzenesulfonyl azide; triethylamine In acetonitrile at 0 - 20℃; for 1h; Inert atmosphere;	100%
With 4-acetamidobenzenesulfonyl azide; triethylamine In acetonitrile at 0 - 20℃; for 1h;	100%
With perfluorobutanesulfonyl azide; triethylamine In dichloromethane at 20℃; for 0.25h;	98%

: 118-92-3
anthranilic acid

: 123-54-6
acetylacetone

: 74568-19-7
2-(2-(2,4-dioxopentan-3-ylidene)hydrazineyl) benzoic acid

Conditions

Conditions	Yield
Stage #1: anthranilic acid With hydrogenchloride; acetic acid; sodium nitrite In water at 0℃; for 1h; Stage #2: acetylacetone With sodium acetate In ethanol; water at 20℃; for 1h;	100%
Stage #1: anthranilic acid With hydrogenchloride; sodium hydroxide; sodium nitrite In water at -0.16℃; Stage #2: acetylacetone In water at -0.16℃; for 1h;	81%
Stage #1: anthranilic acid With hydrogenchloride; sodium nitrite In water at 0 - 5℃; Stage #2: acetylacetone With sodium acetate In methanol; water at 0 - 20℃; for 1h;	78%
With sulfuric acid; sodium acetate; sodium nitrite 1) water, 0 deg C, 2) ethanol; Multistep reaction;

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 123-54-6
acetylacetone

: 18856-72-9
3-dimethylaminomethylenepentane-2,4-dione

Conditions

Conditions	Yield
for 2h; Reflux;	100%
In benzene at 20℃; for 25h; Reflux;	87%
for 1h; Heating;	86%

: 75-15-0
carbon disulfide

: 106-93-4
ethylene dibromide

: 123-54-6
acetylacetone

: 2183-30-4
3-(1,3-dithiolan-2-ylidene)pentane-2,4-dione

Conditions

Conditions	Yield
With potassium carbonate	100%
Stage #1: carbon disulfide; acetylacetone With tetrabutylammomium bromide; potassium carbonate In water at 20℃; Stage #2: ethylene dibromide In water at 20℃; for 8h;	97%
Stage #1: carbon disulfide; acetylacetone With tetrabutylammomium bromide; potassium carbonate In water at 20℃; for 1h; Stage #2: ethylene dibromide In water at 20℃; for 8.25h; Further stages.;	97%

...Expand

: 62-53-3
aniline

: 123-54-6
acetylacetone

: 6134-57-2
pentane-2,3,4-trione 3-phenylhydrazone

Conditions

Conditions	Yield
Stage #1: aniline With hydrogenchloride; acetic acid; sodium nitrite In water at 0℃; for 1h; Stage #2: acetylacetone With sodium acetate In ethanol; water at 20℃; for 1h;	100%
With hydrogenchloride; sodium acetate; acetic acid; sodium nitrite In ethanol; water at 20℃; for 0.5h;	100%
Stage #1: aniline With hydrogenchloride; sodium nitrite Stage #2: acetylacetone With sodium hydroxide; sodium acetate In methanol; water at 0 - 20℃; for 1h; Further stages.;	95%

: 460-19-5
ethanedinitrile

: 123-54-6
acetylacetone

: 77097-65-5
2-(1-amino-2-acetylbut-1-enonyl)-4-carboxamido-5-acetyl-6-methyl-1,3-diazine

Conditions

Conditions	Yield
With bis(acetylacetonate)nickel(II) In 1,2-dichloro-ethane for 140h; Product distribution; different times and catalysts;	100%
bis(acetylacetonate)nickel(II) In 1,2-dichloro-ethane for 144h; Ambient temperature; further cat.: Cu(acac)2;	100%
With bis(acetylacetonate)nickel(II) In dichloromethane for 140h;	100%
copper acetylacetonate In 1,2-dichloro-ethane Mechanism; Ambient temperature; var. conc. of reactants and catalysts; further catalysts: Ni(acac)2 and bis(1-cyano-2-(1-iminoethyl)buten-1,3-dionato)copper(II); detreminetion of t1/2;

: 574-42-5
benzhydryl ether

: 123-54-6
acetylacetone

: 19672-37-8
3-benzhydryl-pentane-2,4-dione

Conditions

Conditions	Yield
With indium(III) chloride In toluene at 80℃; for 3h;	100%
CoCl2 for 1h; Heating;	97%

: 78288-57-0
1-Amino-5,6-dimethylbenzimidazole

: 123-54-6
acetylacetone

: 81889-95-4
2,4,7,8-tetramethylpyridazino<1,6-a>benzimidazole

Conditions

Conditions	Yield
With zinc(II) chloride for 4h; Cyclization; Heating;	100%
With zinc(II) chloride at 150 - 160℃; for 1.5h;	90 % Turnov.

: 34570-17-7
malonamamidine hydrochloride

: 123-54-6
acetylacetone

: 7144-20-9
2-Amino-4,6-dimethylnicotinamide

Conditions

Conditions	Yield
With potassium hydroxide In methanol at 20℃; Inert atmosphere;	100%
With potassium hydroxide In methanol Ambient temperature;	92%
With potassium hydroxide In methanol at 20℃; for 24h;	79%

: 87504-16-3
2-methyl-1,2,4-thiadiazolo[4,5-a]benzimidazole-3(2H)-one

: 123-54-6
acetylacetone

: 98154-64-4
2-(1-Acetyl-2-oxo-propylsulfanyl)-benzoimidazole-1-carboxylic acid methylamide

Conditions

Conditions	Yield
for 24h;	100%

: 87504-17-4
2-cyclohexylbenzimidazo<1,2-d><1,2,4>thiadiazol-3(2H)-one

: 123-54-6
acetylacetone

: 98183-15-4
2-(1-Acetyl-2-oxo-propylsulfanyl)-benzoimidazole-1-carboxylic acid cyclohexylamide

Conditions

Conditions	Yield
for 24h;	100%

: 304-20-1
1-hydrazinophthalazine hydrochloride

: 123-54-6
acetylacetone

: 60519-05-3
1-(3,4-dimethyl pyrazol-1-yl)phthalazine

Conditions

Conditions	Yield
	100%

: 91657-52-2
5-amino-3-methyl-1-(2,4-dinitrophenyl)pyrazole

: 123-54-6
acetylacetone

A: 116835-08-6
3,6-Dimethyl-1-(4-nitro-phenyl)-1H-pyrazolo[3,4-b]pyridine

B: 116835-11-1
1-(2,4-Dinitro-phenyl)-3,4,6-trimethyl-1H-pyrazolo[3,4-b]pyridine

Conditions

Conditions	Yield
zinc(II) chloride In hydrogenchloride; ethanol for 1h; Heating;	A 75% B 100%

...Expand

: 627-27-0
homoalylic alcohol

: 123-54-6
acetylacetone

: (Z)-4-But-3-enyloxy-pent-3-en-2-one

Conditions

Conditions	Yield
With toluene-4-sulfonic acid In toluene Heating;	100%

: 144017-77-6, 20426-47-5
1-(2-chloro-phenyl)-3-phenyl-2-propen-1-one

: 123-54-6
acetylacetone

: 2-acetyl-3-(o-chlorophenyl)-5-phenylcyclohexenone

Conditions

Conditions	Yield
With sodium ethanolate In ethanol	100%

: 61-82-5
3-amino-1,2,4-triazole

: 123-54-6
acetylacetone

: 7681-99-4
5,7-dimethyl-[1,2,4]triazolo[1,5-a]pyrimidine

Conditions

Conditions	Yield
With acetic acid for 3h; Reflux;	100%

: 123-54-6
acetylacetone

: (E)-1,3-diphenylprop-2-en-1-yl pivalate

: 104637-11-8
(R)-(E)-3-acetyl-4,6-diphenylhex-5-en-2-one

Conditions

Conditions	Yield
With (-)-9-pinanyl-BBN; lithium acetate; bis-(trimethylsilyl)acetamide; bis(dibenzylideneacetone)-palladium(0) In 1,2-dichloro-ethane at 40℃; for 48h;	100%

: 75-15-0
carbon disulfide

: 109-64-8
1,3-dibromo-propane

: 123-54-6
acetylacetone

: 55727-23-6
3‐(1,3-dithiane-2-yl)pentane-2,4-dione

Conditions

Conditions	Yield
With potassium carbonate	100%
Stage #1: carbon disulfide; acetylacetone With tetrabutylammomium bromide; potassium carbonate In water at 20℃; Stage #2: 1,3-dibromo-propane In water at 20℃; for 8h;	92%
With potassium carbonate In N,N-dimethyl-formamide for 7h;	74%

...Expand

: 2280-44-6
D-Glucose

: 123-54-6
acetylacetone

: 215510-13-7
1-(β-D-glucopyranosyl)propan-2-one

Conditions

Conditions	Yield
With sodium hydrogencarbonate In water Knoevenagel Condensation; Reflux; Green chemistry;	100%
With sodium hydrogencarbonate at 90℃; for 6h; Knoevenagel condensation;	96%
With sodium hydrogencarbonate In water at 90℃; for 8h;	96%

: 551-93-9
2-aminoacetophenone

: 123-54-6
acetylacetone

: 14428-41-2
1-(2,4-dimethyl-quinolin-3-yl)-ethanone

Conditions

Conditions	Yield
With 3-methyl-1-sulfoimidazolium trichloroacetate; trichloroacetic acid In neat (no solvent) at 100℃; Friedlaender Quinoline Synthesis;	100%
With toluene-4-sulfonic acid In ethanol at 80℃; for 12h; Reagent/catalyst; Friedlaender Quinoline Synthesis; Schlenk technique;	99%
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate; N,N-dimethyl-formamide at 90℃; Friedlaender reaction;	98%

: 115134-78-6
2,4,6-tris[bis(trimethylsilyl)methyl]aniline

: 123-54-6
acetylacetone

: 926625-25-4
(Z)-4-[2,4,6-Tris-(bis-trimethylsilanyl-methyl)-phenylamino]-pent-3-en-2-one

Conditions

Conditions	Yield
With hydrogenchloride In diethyl ether; toluene for 8h; Heating;	100%
With hydrogenchloride In diethyl ether; toluene for 8h; Heating;	99%

: 123-54-6
acetylacetone

: 301164-69-2
(1H-benzo[d][1,2,3]triazol-1-yl)(thiophen-2-yl)methanone

: 127191-99-5
(Z)-3-hydroxy-1,3-bis(2-thienyl)-2-propen-1-one

Conditions

Conditions	Yield
Stage #1: acetylacetone With sodium hydride In tetrahydrofuran at 20℃; for 0.666667h; Stage #2: (1H-benzo[d][1,2,3]triazol-1-yl)(thiophen-2-yl)methanone In tetrahydrofuran at 20℃; for 14h; Stage #3: With ammonium hydroxide; ammonium chloride In tetrahydrofuran; water for 1h; Heating;	100%

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