Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Quick Details ProName: High purity 2,2'-Dipyridyl CasNo: 366-18-7 Molecular Formula: C10H8N2 Appearance: white to light red crystal powder Application: Used for REDOX indicator and analysis ... DeliveryTim
Cas:366-18-7
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inquiryZhangjiagang Huamao Fine Chemical Co., Ltd. was founded in 2006. It is a Sino-US joint venture engaged in research and production. The company is situated in Yangtze River International Chemical Industrial Park, Free Trade Zone, Zhangjiagang. Based o
Items Standard Result Appearance White to pale red crystal powder Conforms Assay ≥99
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inquiryMolecular Formula C10H8N2 Molecular Weight 156.19 CAS Registry Number 366-18-7 EINECS 206-674-4 Name 2,2'-Dipyridyl Synonyms 2,2'-Bipyridine
hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
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inquiryProduct description: Product name 2,2'-Dipyridyl CAS number 366-18-7 Assay ≥99% Appearance White crystalline powder Capacity 200mt/year Application Pharmaceutical interme
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
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inquiryTIANFUCHEM--366-18-7--2,2'-Bipyridine factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business rel
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct name 2 2 -Bipyridine Synonyms 2, 2 - al pyridine;2,2'-Bipyridyl ReagentPlus(R), >=99%;2,2'-Bipyridyl Vetec(TM) reagent grade, 98%;2,2'-Bipyridine, ACS, 98.0% min.;2,2-Bipyridyl
Appearance:White crystalline powder Storage:Room temperature Package:25kg/Barrel Application:For organic synthesis, pharmaceutical intermediates Transportation:Express/Sea/Air Port:Any port in china
Cas:366-18-7
Min.Order:1 Kilogram
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inquirySynonyms: ,’-Dipyridyl;2-(2-Pyridyl)pyridine;2,2’-bipyridin;2,2’-dipyridine;2,2'-Bipyridin;2,2'-Dipyridine;AA-DP;alpha,alpha’-dipyridine CAS: 366-18-7 MF: C10H8N2 MW: 156.18 EINECS: 206-674-4 Product Categories:
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Min.Order:1 Kilogram
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inquiryBeluga chemical professional supply High quality 2,2'-Bipyridine CAS 366-18-7 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in Ch
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Min.Order:10 Gram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate In water; N,N-dimethyl-formamide at 210℃; for 24h; Catalytic behavior; Solvent; Reagent/catalyst; | 100% |
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; cesium fluoride In dimethyl sulfoxide at 120℃; for 8h; | 96% |
With bis(triphenylphosphine)nickel(II) chloride; sodium hydride; triphenylphosphine; zinc In toluene at 70 - 90℃; Ullmann-type coupling; | 93% |
ethyl(1,1,1,3,3,3-hexafluoro-2-propoxo)(2,2'-bipyridine)nickel
A
[2,2]bipyridinyl
B
1,1,1,3,3,3-hexafluoropropan-2-yl propionate
Conditions | Yield |
---|---|
With carbon monoxide In tetrahydrofuran Addn. of CO (ambient pressure) to metal complex (THF, room temp.), stirring (2.5 h).; Trap-to-trap distn., GLC anal.; | A 100% B 97% |
methyl(1,1,1,3,3,3-hexafluoro-2-propoxo)(2,2'-bipyridine)nickel
A
[2,2]bipyridinyl
B
1,1,1,3,3,3-hexafluoropropan-2-yl acetate
Conditions | Yield |
---|---|
With carbon monoxide In tetrahydrofuran Addn. of CO (ambient pressure) to metal complex (THF, room temp.), stirring (2.5 h).; Trap-to-trap distn., GLC anal.; | A 100% B 98% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; johnphos; bis(dibenzylideneacetone)-palladium(0) In 1-methyl-pyrrolidin-2-one at 20℃; for 12h; | 99% |
With sodium hydroxide; triethylammonium formate; zinc In methanol for 2.5h; Heating; | 92% |
With sodium hydroxide; ammonium formate; zinc In methanol for 2.5h; Heating; | 90% |
Conditions | Yield |
---|---|
With (2-hydroxyethyl)(methyl)amine; copper(l) iodide; dichloro(1,3-bis(dicyclohexylphosphino)propane)palladium In N,N-dimethyl-formamide at 100℃; for 16h; Suzuki-Miyaura Coupling; Inert atmosphere; | 99% |
2,2'-bipyridyl N-oxide
[2,2]bipyridinyl
Conditions | Yield |
---|---|
With (4,4′-di-tert-butyl-2,2′-bipyridine)bis[(2-pyridinyl)phenyl]iridium(III) hexafluorophosphate; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate In 2,2,2-trifluoroethanol; acetonitrile at 20℃; for 3h; Inert atmosphere; Irradiation; chemoselective reaction; | 98% |
With (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; hydrazine hydrate In dimethyl sulfoxide at 20℃; for 27h; Inert atmosphere; Irradiation; chemoselective reaction; | 96% |
With N-Bromosuccinimide In chlorobenzene at 150℃; for 17h; | 20 %Spectr. |
Conditions | Yield |
---|---|
In 5,5-dimethyl-1,3-cyclohexadiene at 170℃; for 16h; | 97.4% |
With cyclooctadienyl cobalt at 140 - 190℃; for 2h; Temperature; Autoclave; | 250 g |
Conditions | Yield |
---|---|
With dmap; copper(II) ethylacetoacetate; C26H36NP; silver(I) acetate In 1,2-dichloro-ethane at 90℃; for 8h; Reagent/catalyst; | 96.7% |
Conditions | Yield |
---|---|
With potassium hydroxide In water; N,N-dimethyl-formamide at 35℃; for 12h; Reagent/catalyst; Ullmann Condensation; Inert atmosphere; | 96% |
With aluminum oxide; nickel(II) chloride hexahydrate; sodium hydroxide; zinc In methanol; water at 50℃; for 3h; Reagent/catalyst; Temperature; | 95% |
With manganese; nickel(II) bromide trihydrate In N,N-dimethyl-formamide at 20 - 60℃; for 20h; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With titanium tetrachloride; tin(ll) chloride In benzene for 0.5h; Ambient temperature; | 95% |
With titanium In tetrahydrofuran for 0.25h; Ambient temperature; | 90% |
With sodium hypophosphite; palladium on activated charcoal In acetic acid at 60℃; for 1h; | 90% |
methyl 4-iodobenzoate
2-trimethylstannylpyridine
A
[2,2]bipyridinyl
B
4-pyridin-2-yl-benzoic acid methyl ester
Conditions | Yield |
---|---|
bis-triphenylphosphine-palladium(II) chloride In tetrahydrofuran Heating; | A n/a B 95% |
cis-dichlorobis(2,2′-bipyridine)ruthenium(II)
{Ag(2,2'-bipyridine)2}ClO4
A
[2,2]bipyridinyl
Conditions | Yield |
---|---|
In methanol byproducts: AgCl; heated to reflux for 15 min; cooled, filtered, concd., addn. of an aq. soln. of NaClO4, pptn. filtered off, washed with diethyl ether, recrystn. (water or water-methanol 9:1); elem. anal.; | A n/a B 95% |
Conditions | Yield |
---|---|
Aza-Diels-Alder reaction; | 93.3% |
2-bromo-pyridine
phenylboronic acid
A
2-phenylpyridine
B
[2,2]bipyridinyl
Conditions | Yield |
---|---|
With potassium phosphate; palladium diacetate In water at 100℃; for 4h; Suzuki Coupling; Inert atmosphere; Green chemistry; | A 92% B n/a |
With 1-(4-bromobenzyl)-3-(4-chlorobenzyl)benzimidazolium chloride; palladium diacetate; potassium carbonate In water; N,N-dimethyl-formamide at 120℃; for 0.166667h; Reagent/catalyst; Suzuki-Miyaura Coupling; Microwave irradiation; | A 67.0 %Spectr. B 27.2 %Spectr. |
Conditions | Yield |
---|---|
With potassium hydroxide; tetrabutyl-ammonium chloride; lithium chloride In tetrahydrofuran; ethanol | 91% |
cis-dichlorobis(2,2′-bipyridine)ruthenium(II)
A
[2,2]bipyridinyl
Conditions | Yield |
---|---|
With NaNO3 In methanol byproducts: AgCl; heated to reflux for 15 min; cooled, filtered, concd., addn. of an aq. soln. of NaNO3, pptn. filtered off, washed with diethyl ether, recrystn. (water or water-methanol 9:1); elem. anal.; | A n/a B 90% |
2-tri-n-butylstannylpyridine
[2,2]bipyridinyl
Conditions | Yield |
---|---|
With palladium diacetate; copper dichloride In tetrahydrofuran at 23℃; for 1h; | 89% |
With iodine; copper dichloride In N,N-dimethyl-formamide at 100℃; for 4h; | 85% |
With bis(η3-allyl-μ-chloropalladium(II)); N-(2-(diphenylphosphino)phenyl)methylene benzenamine In N,N-dimethyl-formamide at 70℃; for 72h; | 79% |
With air; Pd-organostannane In N,N-dimethyl-formamide at 70℃; for 72h; | 79% |
3-(pyridin-2-yl)-1,2,4-triazine
bicyclo[2.2.1]hepta-2,5-diene
[2,2]bipyridinyl
Conditions | Yield |
---|---|
In xylene at 90 - 120℃; Aza-Diels-Alder reaction; | 88.2% |
Conditions | Yield |
---|---|
88.2% |
Conditions | Yield |
---|---|
88.2% |
Phenylselenyl chloride
tris(2-pyridyl)phosphine oxide
A
[2,2]bipyridinyl
Conditions | Yield |
---|---|
In methanol at 20℃; for 24h; | A 12% B 88% |
In methanol at 20℃; for 24h; | A 36% B 57% |
pyridin-2-ylboronic acid
[2,2]bipyridinyl
Conditions | Yield |
---|---|
With palladium diacetate at 20℃; for 0.5h; | 87% |
With potassium phosphate In 1,4-dioxane at 85℃; for 3h; Catalytic behavior; Suzuki Coupling; Green chemistry; | 82% |
With nano-CuO-grafted triazine-functionalized covalent organic framework In methanol at 60℃; Catalytic behavior; | 59% |
A
[2,2]bipyridinyl
Conditions | Yield |
---|---|
In neat (no solvent) heated at 200°C under vacuum for 1 h; temperature increased to 300°C, and the complex sublimed over 5 h, resublimed (300°C, 1E-7 mbar), elem. anal.; | A n/a B 85% |
(pyridin-2-yl)magnesium bromide
[2,2]bipyridinyl
Conditions | Yield |
---|---|
With lithium perchlorate; palladium diacetate In toluene at 100℃; for 15h; Reagent/catalyst; Inert atmosphere; | 85% |
With 4,4'-di-tert-butylbiphenyl; lithium; iron(II) chloride In tetrahydrofuran; diethyl ether at 20℃; for 4h; Inert atmosphere; | 75% |
With C19H3F17 at 60℃; for 24h; Schlenk technique; Inert atmosphere; | 44% |
benzyltri(2-(4-methylpyridyl))phosphonium bromide
A
picoline
B
[2,2]bipyridinyl
C
4,4'-dimethyl-2,2'-bipyridines
Conditions | Yield |
---|---|
With hydrogenchloride In water for 0.5h; Product distribution; Ambient temperature; variation of pH, temp. and time; | A 17% B n/a C 84% |
Conditions | Yield |
---|---|
With oxygen; palladium diacetate; toluene-4-sulfonic acid In tetrahydrofuran for 12h; Reflux; | 84% |
With hydrogenchloride; iodine; oxygen In dimethyl sulfoxide at 80℃; for 4h; | 82% |
With oxygen; copper(II) bis(trifluoromethanesulfonate); toluene-4-sulfonic acid In hexan-1-ol at 110℃; for 24h; Sealed tube; Schlenk technique; | 27% |
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; cesium fluoride In 2-pentanol at 100℃; for 12h; Inert atmosphere; | A 16.5% B 83.5% |
Conditions | Yield |
---|---|
In tetrahydrofuran for 5h; Heating; | 82% |
Conditions | Yield |
---|---|
With phenyllithium In tetrahydrofuran at -78℃; for 0.25h; | A 82% B 53% |
Conditions | Yield |
---|---|
With 2,2′-sulfinyldipyridine In tetrahydrofuran at -78℃; for 0.25h; | A 82% B 53% |
[2,2]bipyridinyl
2,2'-bipyridyl N-oxide
Conditions | Yield |
---|---|
With water; dihydrogen peroxide; trifluoroacetic acid for 2h; Ambient temperature; | 100% |
With dihydrogen peroxide; trifluoroacetic acid at 10 - 20℃; for 3h; | 100% |
With dihydrogen peroxide In trifluoroacetic acid at 10 - 20℃; for 3h; | 100% |
[2,2]bipyridinyl
1,3-dibromo-propane
6H-7,8-dihydropyrido<1,2-a:2,1-c><1,4>diazepine-5,9-diium dibromide
Conditions | Yield |
---|---|
In acetone Heating; | 100% |
for 12h; Reflux; | 90% |
In acetonitrile |
Conditions | Yield |
---|---|
In tetrachloromethane under N2; soln. of SnCl4 in CCl4 mixed with ligand (molar ratio 1:2); stirred for several h; filtered; solid washed with petroleum ether; dried in vac.; stored in desiccator over CaCl2; elem. anal.; | 100% |
[2,2]bipyridinyl
(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonylmolybdenum(0)
A
tetracarbonyl(2,2'-bipyridine)molybdenum
B
bicyclo[2.2.1]hepta-2,5-diene
Conditions | Yield |
---|---|
In tetrahydrofuran reaction in a calorimeter under argon; | A 100% B n/a |
[2,2]bipyridinyl
diphenylboronchloride
(C5H4N)2B(C6H5)2(1+)*Cl(1-)={(C5H4N)2B(C6H5)2}Cl
Conditions | Yield |
---|---|
In benzene | 100% |
In nitrobenzene | 78% |
In not given | |
In not given |
[2,2]bipyridinyl
bromine pentafluoride
Conditions | Yield |
---|---|
In trichlorofluoromethane addn. of CCl3F to 1.00 mmol BrF5 at -78°C; dissolving; addn. of 1 mmol C5H4NC5H4N at -45°C; pptn.; heating to -40°C in 2h; filtration;; washing twice with CCl3F at -40°C; drying in high vac. at -30°C;; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran (Ar); stirring (1 h); washing (hexane), drying (vac.); elem. anal.; | 100% |
[2,2]bipyridinyl
[palladium(II)(μ-Cl)(C6H4-2-PPh2NPh-κC,N)]2
palladium(II)(C6H4-2-PPh2NPh-κC,N)(2,2'-bipyridine)perchlorate
Conditions | Yield |
---|---|
In acetone byproducts: AgCl; suspn. of Pd complex in acetone treated with AgClO4, stirred at room temp. for 30 min (exclusion of light), filtered, treated with ligand, stirred at room temp. for 4 h; evapd., treated with Et2O, filtered, dried, elem. anal.; | 100% |
[2,2]bipyridinyl
Mo(OCH2CHC(CH3)2)2O2(C(2)H3CN)2
Mo(OCH2CHC(CH3)2)2O2(C5H4NC5H4N)
Conditions | Yield |
---|---|
In [D3]acetonitrile determined by NMR; | 100% |
[2,2]bipyridinyl
Conditions | Yield |
---|---|
In toluene Ar atm.; stirring (10 min); concn., addn. of hexane, crystn. (-30°C), filtn., drying (40°C, vac.); elem. anal.; | 100% |
[2,2]bipyridinyl
Conditions | Yield |
---|---|
In toluene Ar atm.; stirring; concn., addn. of hexane, crystn. (-30°C), filtn., drying (40°C, vac.); | 100% |
[2,2]bipyridinyl
[Pd(η4-1,5-cyclooctadiene)(C6F5)2]
Conditions | Yield |
---|---|
In tetrahydrofuran Pd-complex reacted with ligand in THF, according to a) C. De Haro, G. Garcia, G. Sanchez and G. Lopez, J. Chem. Res. (S), 1986, 119; b) P. Espinet, J. M. Martinez-Ilarduya, C. Perez-Briso, A. L. Casado and A. M. Alonso, J. Organomet. Chem., 1998, 551, 9; | 100% |
[2,2]bipyridinyl
[Ir(III)(η5-pentamethylcyclopentadienyl)(H2O)3](SO4)
[Ir(III)Cp*(bpy)(OH2)](SO4)
Conditions | Yield |
---|---|
In water at 20℃; for 12h; | 100% |
In water at 20℃; for 18h; Inert atmosphere; | 100% |
[2,2]bipyridinyl
[Co(dibenzoylmethanato)2(H2O)2]
[Co(1,3-diphenylpropane-1,3-dionate)2(2,2'-bipyridine)]
Conditions | Yield |
---|---|
In tetrahydrofuran 2,2'-bipyridine (0.15 mmol) added to soln. of Co complex (0.15 mmol) (stirring); stirred (room temp., 1 h); evapd. slolwy (room temp.); elem. anal.; | 100% |
Conditions | Yield |
---|---|
Stage #1: [2,2]bipyridinyl; [(99)technetium(I)(carbonyl)3(H2O)3] With hydrogenchloride; sodium chloride In water at 40℃; for 0.5h; pH=6; Inert atmosphere; Stage #2: pyridine In water at 40℃; for 0.333333h; Inert atmosphere; | 100% |
[2,2]bipyridinyl
Conditions | Yield |
---|---|
With fluorosilicic acid In methanol; water at 20℃; | 100% |
Conditions | Yield |
---|---|
In acetonitrile at -196 - 20℃; for 6h; | 100% |
[2,2]bipyridinyl
niobium pentafluoride
trimethylsilylazide
[Nb(N3)4(2,2’-bipy)2][Nb(N3)6]
Conditions | Yield |
---|---|
In acetonitrile at -196 - 20℃; for 6h; | 100% |
Conditions | Yield |
---|---|
In acetonitrile at -196 - 20℃; for 6h; | 100% |
[2,2]bipyridinyl
tantalum pentafluoride
trimethylsilylazide
[Ta(N3)4(2,2’-bipy)2][Ta(N3)6]
Conditions | Yield |
---|---|
In acetonitrile at -196 - 20℃; for 6h; | 100% |
Conditions | Yield |
---|---|
In acetonitrile for 0.25h; Sealed tube; | 100% |
[2,2]bipyridinyl
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate
Conditions | Yield |
---|---|
at 19.84℃; for 0.25h; | 100% |
potassium hexafluorophosphate
[2,2]bipyridinyl
Conditions | Yield |
---|---|
In ethylene glycol at 160℃; for 0.25h; Microwave irradiation; | 100% |
Conditions | Yield |
---|---|
In acetonitrile at -196 - 20℃; for 1h; Autoclave; | 100% |
Conditions | Yield |
---|---|
With arsenic(III) fluoride In acetonitrile at -196 - 20℃; for 1h; Autoclave; | 100% |
Conditions | Yield |
---|---|
In acetonitrile at -196 - 20℃; for 8h; Autoclave; | 100% |
[2,2]bipyridinyl
lithium oxalate
copper(II) bis(trifluoromethanesulfonate)
Conditions | Yield |
---|---|
In water | 100% |
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