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inquiryAbout Product Details 1,4-Benzenedimethanol Chemical Properties
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inquiry1,4-Benzenedimethanol Basic information Product Name: 1,4-Benzenedimethanol Synonyms: BENZENE-1,4-DIMETHANOL;1,4-PHENYLENEDIMETHANOL;1,4-PHENYLENE DICARBINOL;1,4-BIS(HYDROXYMETHYL)BENZEN
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct name 1,4-Benzenedimethanol Cas number 589-29-7 Molecular formula C8H10O2 Molecular weight 138.16 Appearance White to off-
We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At presen
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inquiry1,4-Benzenedimethanol CAS:589-29-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiry1,4-Benzenedimethanol CAS: 589-29-7 Specification melting point 116-119℃ boiling point 309.1°c at 760 mmhg flash point 147°c vapour pressur 0.000282mmhg at 25°c Welcome to c
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryPacking: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryProduct name: 1,4-Benzenedimethanol CAS No.: 589-29-7 Molecule Formula:C10H16O2 Molecule Weight:168.23 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING ITEMS
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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1,4-Benzenedimethanol Chemical Properties Melting point 114-118 °C(lit.) Boiling point 138-143 °C1 mm Hg(lit.) density 1.0742 (rough estimate) refractive index 1.5090 (estimate) Fp 138-143°C/1mm storage temp. Store
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryConditions | Yield |
---|---|
With hydrogen; sodium ethanolate In 1,4-dioxane at 80℃; under 38002.6 Torr; for 16h; | 99% |
With C13H34BFeNOP2; hydrogen In tetrahydrofuran at 100℃; under 22502.3 Torr; for 18h; Autoclave; Inert atmosphere; | 96% |
With C15H29MnNO3P2(1+)*Br(1-); potassium tert-butylate; hydrogen In 1,4-dioxane at 110℃; under 22502.3 Torr; for 24h; Inert atmosphere; Autoclave; | 95% |
Conditions | Yield |
---|---|
With C48H43ClN2P2Ru; ammonium formate In water; toluene at 90℃; for 10h; Catalytic behavior; Schlenk technique; | 99% |
Stage #1: terephthalaldehyde, With [HC{(Me)CN(2,6-iPr2C6H3)}2MgnBu]; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In toluene at 20℃; for 8h; Inert atmosphere; Stage #2: With hydrogenchloride; water In methanol; toluene for 1h; Inert atmosphere; Reflux; | 97% |
With hydrogen In methanol at 130℃; under 11251.1 Torr; for 2h; Catalytic behavior; Autoclave; | 96.3% |
1,4-di(t-butyldimethylsiloxymethyl)benzene
p-xylylene glycol
Conditions | Yield |
---|---|
With low-loading and alkylated polystyrene-supported-SO3H In water at 40℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With [Ru(2-(methylthio)-N-[(pyridin-2-yl)methyl]ethan-1-amine)(triphenylphosphine)Cl2]; potassium tert-butylate; hydrogen In toluene at 80℃; under 30003 Torr; for 3h; | 99% |
With sodium tetrahydroborate In ethanol UV-irradiation; |
A
p-xylylene glycol
B
[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]methanol
Conditions | Yield |
---|---|
With MCM-41 In methanol for 8h; Ambient temperature; Yields of byproduct given; | A n/a B 97% |
With mesoporous silica MCM-41 In methanol at 20℃; for 8h; | A n/a B 97% |
Conditions | Yield |
---|---|
With C30H34Cl2N2P2Ru; potassium methanolate; hydrogen In tetrahydrofuran at 100℃; under 38002.6 - 76005.1 Torr; for 10h; Glovebox; Autoclave; | 97% |
With potassium borohydride; lithium chloride for 0.0833333h; microwave irradiation; | 85 % Chromat. |
Conditions | Yield |
---|---|
With [Zn(BH4)2(py)] In tetrahydrofuran for 7h; Heating; | 95% |
With zirconium(IV) borohydride In tetrahydrofuran at 25℃; for 1h; Reduction; | 91% |
Stage #1: terephthalic acid With sodium aminodiboranate In tetrahydrofuran at 20℃; Stage #2: With water | 90% |
With zinc(II) tetrahydroborate In tetrahydrofuran for 5h; Heating; | 70% |
Multi-step reaction with 2 steps 1: sulfuric acid / 3 h / 70 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 15 h / 20 °C / Inert atmosphere View Scheme |
p-xylylene glycol
Conditions | Yield |
---|---|
With sodium hydroxide In water Inert atmosphere; | 95% |
4-(hydroxylmethyl)benzaldehyde
p-xylylene glycol
Conditions | Yield |
---|---|
With formic acid; C20H29ClIrN4(1+)*Cl(1-) In water at 80℃; for 0.0833333h; | 95% |
With HNa*CHO2(1-); C63H72ClN3O5PRuS(1+)*Br(1-) In dimethylsulfoxide-d6; water-d2 at 37℃; for 12h; |
1,4-bis((methoxymethoxy)methyl)benzene
p-xylylene glycol
Conditions | Yield |
---|---|
phosphotungstic acid In ethanol for 3h; Heating; | 93% |
1,4-bis[(ethoxymethoxy)methyl]benzene
p-xylylene glycol
Conditions | Yield |
---|---|
phosphotungstic acid In ethanol for 2.5h; Heating; | 90% |
Conditions | Yield |
---|---|
Stage #1: 4-Carboxybenzaldehyde With sodium aminodiboranate In tetrahydrofuran at 20℃; Stage #2: With water | 90% |
With tributylphosphine; diphenylsilane; C45H25F12N7Ni2O9 In 1,4-dioxane at 100℃; for 16h; | 75% |
1,4-di(t-butyldimethylsiloxymethyl)benzene
A
p-xylylene glycol
B
[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]methanol
Conditions | Yield |
---|---|
With sodium tetrachloroaurate(III) dihydrate In methanol at 20℃; for 0.5h; | A n/a B 86% |
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran; diethyl ether for 4.5h; Heating; | 84% |
With zinc(II) tetrahydroborate; N,N,N,N,-tetramethylethylenediamine In diethyl ether at 40℃; for 24h; | 75% |
terephthalaldehyde,
A
p-xylylene glycol
B
4-(hydroxylmethyl)benzaldehyde
Conditions | Yield |
---|---|
With C48H43ClN2P2Ru; ammonium formate In water; toluene at 90℃; for 9h; Catalytic behavior; Schlenk technique; | A 17% B 83% |
With hydrogen; palladium on activated charcoal In ethanol Ambient temperature; | A 3% B 74% |
With Grubbs catalyst first generation; potassium hydroxide In 1,4-dioxane at 80℃; for 20h; Cannizzaro reaction; | A 36% B 40% |
Conditions | Yield |
---|---|
With water; sodium carbonate In 1,4-dioxane at 80℃; for 3h; Solvent; Reagent/catalyst; Temperature; | 80% |
With water; sodium carbonate In 1,4-dioxane at 80℃; for 3h; Solvent; Temperature; Reagent/catalyst; | 80% |
With potassium carbonate | |
With water for 5h; Reflux; | |
With water; sodium formate at 140℃; under 3040.2 Torr; for 1h; Reagent/catalyst; Pressure; |
Conditions | Yield |
---|---|
With dichloro(benzene)ruthenium(II) dimer; 2-((di-p-tolylphosphino)methyl)-1-methyl-1H-imidazole; potassium tert-butylate; hydrogen In tetrahydrofuran at 100℃; under 37503.8 Torr; for 4.5h; | 80% |
Stage #1: 4-(methoxycarbonyl)benzyl alcohol With diethoxymethylane; sodium triethylborohydride In diethyl ether; toluene at 20℃; for 8h; Inert atmosphere; Stage #2: With sodium hydroxide In methanol; diethyl ether; toluene at 20℃; for 2h; Reagent/catalyst; | 76% |
With [RuCl2(N-heterocyclic carbene)(bis[2-(diphenylphosphino)ethyl]amine)]; potassium tert-butylate; hydrogen In tetrahydrofuran; 2-methyltetrahydrofuran at 45℃; under 3750.38 Torr; for 2.5h; Autoclave; | 63% |
Multi-step reaction with 4 steps 1: 100 percent 2: 88 percent / LiAlH4 / diethyl ether; diethyl ether / 1 h / Heating 3: 87 percent 4: 17 percent / 31percent aq. H2SiF6, Et3N / acetonitrile / 1 h / 0 °C View Scheme |
terephthalaldehyde,
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
p-xylylene glycol
Conditions | Yield |
---|---|
In methanol at 20℃; for 4h; Inert atmosphere; Glovebox; | 75% |
Conditions | Yield |
---|---|
Stage #1: terephthalic acid monoethyl ester With tetrabutylammonium borohydride; ethyl iodide In dichloromethane at 25℃; for 2h; Stage #2: With dihydrogen peroxide; sodium hydroxide In water at 0 - 25℃; for 0.333333h; | 75% |
4-chlorophenyl trifluoromethanesulfonate
p-xylylene glycol
Conditions | Yield |
---|---|
With sodium carbonate; bis(dibenzylideneacetone)-palladium(0); ruphos In 1,4-dioxane; water for 48h; Suzuki-Miyaura cross-coupling; Inert atmosphere; Reflux; | 73.1% |
4-Carboxybenzaldehyde
A
p-xylylene glycol
B
4-(hydroxylmethyl)benzaldehyde
Conditions | Yield |
---|---|
With phenylsilane; C34H30CoO6; potassium In tetrahydrofuran at 20℃; for 20h; Inert atmosphere; Schlenk technique; Glovebox; | A n/a B 73% |
Conditions | Yield |
---|---|
With carbon monoxide; hydrogen In tetrahydrofuran (N2), CO/H2 (1:1), in an autoclave, mixture heated at 70°C for 3.5 h, cooled, gases vented; filtered, solvent removed (reduced pressure), hexane added, filtered, solvent removed, IR, NMR, mass spectra; | A 71% B 69% |
Conditions | Yield |
---|---|
With C23H29Cl2N2OPRuS; potassium tert-butylate; hydrogen In tetrahydrofuran at 110℃; under 37503.8 Torr; for 18h; Reagent/catalyst; Temperature; Inert atmosphere; Schlenk technique; Autoclave; | 71% |
4-<(tert-butyldimethylsiloxy)methyl><(triisopropylsiloxy)methyl>benzene
A
p-xylylene glycol
B
[4-({[tert-butyl(dimethyl)silyl]oxy}methyl)phenyl]methanol
C
(4-(((triisopropylsilyl)oxy)methyl)phenyl)methanol
Conditions | Yield |
---|---|
With fluorosilicic acid; triethylamine In acetonitrile at 0℃; for 1h; | A 17% B 7% C 70% |
Conditions | Yield |
---|---|
With hydrogen bromide; dihydrogen peroxide In 1,2-dichloro-ethane at 5℃; for 12h; Irradiation; | 70% |
Conditions | Yield |
---|---|
In sulfuric acid at 40℃; for 14h; electroreduction; | 68% |
1,4-benzenedicarboxylic acid dimethyl ester
A
p-xylylene glycol
B
4-(methoxycarbonyl)benzyl alcohol
Conditions | Yield |
---|---|
With dichloro(benzene)ruthenium(II) dimer; 2-((di-p-tolylphosphino)methyl)-1-methyl-1H-imidazole; potassium tert-butylate; hydrogen In tetrahydrofuran at 100℃; under 37503.8 Torr; for 4.5h; | A 67% B 13% |
With dichlorido-bis[(2-diphenylphosphino)ethyl]amine-cobalt(II); hydrogen; sodium methylate In 1,4-dioxane at 120℃; under 37503.8 Torr; for 48h; Autoclave; | |
With tris((2-(diphenylphosphino)ethyl)amino)ruthenium monocarbonyl; hydrogen; phenol In toluene under 45004.5 Torr; for 18h; Glovebox; Inert atmosphere; Heating; Autoclave; | A 9 %Spectr. B 88 %Spectr. |
ethyl 4-(aminocarbonyl)benzoate
p-xylylene glycol
Conditions | Yield |
---|---|
With C24H20ClN2OPRu; potassium tert-butylate; hydrogen In tetrahydrofuran at 110℃; under 10640.7 Torr; for 36h; Inert atmosphere; Schlenk technique; | 63% |
(C7H7(CH3)2CHOHC2CH2O)2C6H4
dicobalt octacarbonyl
p-xylylene glycol
Conditions | Yield |
---|---|
Stage #1: (C7H7(CH3)2CHOHC2CH2O)2C6H4; dicobalt octacarbonyl In dichloromethane at 20℃; Nicholas Reaction; Inert atmosphere; Stage #2: p-xylylene glycol With boron trifluoride diethyl etherate In dichloromethane at -78 - 20℃; Nicholas Reaction; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With manganese(IV) oxide; molecular sieve In hexane for 3h; Heating; | 99% |
With dihydrogen peroxide In water at 100℃; for 5.5h; chemoselective reaction; | 99% |
With 1-methyl-1H-imidazole; copper(I) oxide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical In acetonitrile at 25℃; for 24h; | 99% |
Conditions | Yield |
---|---|
With ammonium hydroxide; iodine at 60℃; for 2h; | 99% |
With ammonium hydroxide; iodine at 60℃; for 2h; | 99% |
Stage #1: p-xylylene glycol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tert-butylhypochlorite In dichloromethane at 20℃; for 0.5h; Inert atmosphere; Stage #2: With ammonia; iodine In dichloromethane; water at 20℃; for 2h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: p-xylylene glycol With monopotassium naphthalene In tetrahydrofuran at 22℃; for 2h; Stage #2: oxirane In tetrahydrofuran at 40℃; for 20h; Stage #3: With acetic acid In tetrahydrofuran | 99% |
(C7H7(CH3)2CHOHC2CH2O)2C6H4
dicobalt octacarbonyl
p-xylylene glycol
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In 1,4-dioxane; dichloromethane ligand reacted with Co complex in CH2Cl2, treated with 1,4-benzenedimethanol in dioxane at room temp.; | 99% |
Conditions | Yield |
---|---|
With dibutyltin dilaurate In N,N-dimethyl-formamide at 20℃; for 3h; | 99% |
Conditions | Yield |
---|---|
Stage #1: p-xylylene glycol With monopotassium naphthalene In tetrahydrofuran at 22℃; for 2h; Stage #2: oxirane In tetrahydrofuran at 40℃; for 24h; Stage #3: With acetic acid In tetrahydrofuran | 98% |
p-xylylene glycol
chromium(0) hexacarbonyl
tricarbonyl[C6H4(CH2OH)2]chromium(0)
Conditions | Yield |
---|---|
In tetrahydrofuran; dibutyl ether the mixt. of Cr(CO)6 and the alcohol in dibutyl ether and THF was heated under reflux with stirring at between 180 and 240°C for 20-48 hunder N2; filtered, washed with THF, concd., filtered, dried in vac., dissolved in THF, filtered, concd. in vac. (N2 atm.); elem. anal.; | 98% |
In tetrahydrofuran; dibutyl ether N2 atmosphere; refluxing (26 h); crystn. on cooling (ice bath), filtration off, chromy., recrystn. (CH2Cl2/hexane); elem. anal.; | 90% |
Conditions | Yield |
---|---|
With Silphos; bromine In acetonitrile for 0.166667h; Heating; | 97% |
With hydrogen bromide bei der Destillation; |
Conditions | Yield |
---|---|
With diethylene glycol dimethyl ether at 70℃; for 0.583333h; Sonication; | 97% |
With C24H33IrN4O3; water; sodium hydroxide for 18h; Reflux; | 96% |
With sodium hypochlorite; water at 25℃; for 0.5h; | 94% |
Conditions | Yield |
---|---|
With hydrogen; nickel In sodium hydroxide at 20℃; | 96% |
Multi-step reaction with 2 steps 1: pyridine 2: 76 percent / H2 / Pd/C(ethylenediamine) / methanol / 1 h / 20 °C View Scheme | |
With hydrogen In ethanol; water at 170℃; under 15001.5 Torr; for 12h; Autoclave; Sealed tube; Green chemistry; | 97.8 %Chromat. |
Conditions | Yield |
---|---|
Stage #1: p-xylylene glycol With monopotassium naphthalene In tetrahydrofuran at 22℃; for 2h; Stage #2: oxirane In tetrahydrofuran at 40℃; for 64h; Stage #3: With acetic acid In tetrahydrofuran | 96% |
Dimethoxymethane
p-xylylene glycol
{4-[(methoxymethoxy)methyl]phenyl}methanol
Conditions | Yield |
---|---|
With 12-tungstophosphoric acid immobilized on [bmim][FeCl4] at 75 - 82℃; for 0.00972222h; Microwave irradiation; | 96% |
Conditions | Yield |
---|---|
With ruthenium(II) bis(triphenylphosphine) dichloride at 190℃; for 14h; Inert atmosphere; Schlenk technique; | 96% |
p-xylylene glycol
sodium acetate
1,4-bis(hydroxymethyl)benzene diacetate
Conditions | Yield |
---|---|
In water at 100℃; for 8h; | 96% |
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane for 12h; Heating; | 95.3% |
With dicyclohexyl-carbodiimide |
p-xylylene glycol
p-bis(iodomethyl)benzene
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate; cesium iodide In acetonitrile at 20℃; for 0.416667h; | 95% |
With Silphos; iodine In acetonitrile for 0.0833333h; Heating; | 95% |
With tetrachlorosilane; sodium iodide In chloroform; acetonitrile at 20℃; for 5h; | 88% |
With hydrogen iodide |
Conditions | Yield |
---|---|
With pyridine | 95% |
p-xylylene glycol
chloromethyl methyl ether
1,4-bis((methoxymethoxy)methyl)benzene
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at -20 - 20℃; | 95% |
Conditions | Yield |
---|---|
With 12-tungstophosphoric acid immobilized on [bmim][FeCl4] at 75 - 82℃; for 0.00972222h; Microwave irradiation; | 95% |
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