DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:646-06-0
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inquiry1,3-Dioxolane Product Name: 1,3-Dioxolane Molecular Weight: 74.07 CAS NO: 646-06-0 EC NO: 211-463-5 Molecular Formula: C3H6O2
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Hebei yanxi chemical co., LTD is a professional research, development and production Cyromazine、Azamethiphos、lead diacetate trihydrate /Lead acetate trihydrateC、 2-phenylacetamide 、 4-Aminophenyl-1-phenethylpiperidine 、Citric acid monohydrate 、
Cas:646-06-0
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inquiry1,3-Dioxolane Basic information Product Name: 1,3-Dioxolane Synonyms: 1,3-Dioxolan;1,3-Dioxole, dihydro-;1,3-dioxole,dihydro-;1,3-dixolane;dihydro-1,3-dioxole;dihydro-3-dioxole;Dioxolan;
Product Description Product website: http://www.finerchem.com Product Name 1,3-Dioxolane CAS No. 646-06-0 A
Cas:646-06-0
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inquiry[CAS NO.] 646-06-0 [Chemical name] 1,3-Dioxolane [Formula] C3H6O2 [Molecular weight] 74.08 [Appearance] colorless transparent liquid
Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:646-06-0
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Appearance:Colourless transparent liquid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common produc
Cas:646-06-0
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:646-06-0
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:646-06-0
Min.Order:10 Gram
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inquiry1,3-DioxolaneAppearance:Colourless Liquid Storage:Refrigerator Package:according to customers' requirements Application:1,3-Dioxolane is an intermediate for the preparation of Acyclovir (A192400). Also, 1,3-Dioxolane is used in the synthesis of new V
Superior quality, moderate price & quick delivery. Appearance:Colorless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum;200kg/drum as per your request Application:1,3-Dioxolane is an inter
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers285.Safe and fa
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Cas:646-06-0
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inquiryhangzhou zeerrui chemical co., ltd. located in lingang industrial areas, our plant covers an area of 6000 square meters.zeerrui dedicated to the development, production and marketing of chemicals. we have earned ourselves a good reputation at home
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:646-06-0
Min.Order:1 Kilogram
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
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low price and high purityAppearance:solid or liquid Storage:in sealed air resistant place Package:As customer require Application:Pharma;Industry;Agricultural Transportation:by sea or by airplane Port:any port in China
Cas:646-06-0
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inquiryConditions | Yield |
---|---|
With C13H22N4O6S2(2+)*2CF3O3S(1-) In water at 130℃; for 2h; Reagent/catalyst; | 95.4% |
Conditions | Yield |
---|---|
at 60 - 95℃; for 3h; Concentration; Temperature; | 94.3% |
With phosphoric acid | |
With phosphoric acid; water |
Conditions | Yield |
---|---|
With sulfur dioxide at 105 - 164℃; for 4h; | 85% |
Conditions | Yield |
---|---|
With zinc(II) chloride at 130 - 150℃; | 77% |
Conditions | Yield |
---|---|
With iron(III) chloride hexahydrate; sodium nitrite at 50℃; for 24h; UV-irradiation; | 71% |
Conditions | Yield |
---|---|
In toluene | 69% |
Conditions | Yield |
---|---|
With bismuth(lll) trifluoromethanesulfonate In 1,4-dioxane at 100℃; for 3h; Sealed tube; | 66% |
With iron(III) chloride | |
With phosphoric acid at 100℃; im Rohr; | |
With hydrogenchloride at 100℃; |
2-ethoxy-1,3-dioxolane
A
1,3-DIOXOLANE
B
ethanol
C
2-ethoxymethoxy-ethanol
Conditions | Yield |
---|---|
With diisobutylaluminium hydride In hexane at 35 - 40℃; | A 45% B n/a C 45% |
Conditions | Yield |
---|---|
With zinc(II) chloride at 130 - 150℃; | 31% |
Conditions | Yield |
---|---|
With H2 In decalin High Pressure; 71.5 atm H2 at room temp., heated to 200°C and stirred for 24 h; pressure realesed, detn. by GC and GC-MS; | A 27% B n/a |
Conditions | Yield |
---|---|
With zinc(II) chloride at 130 - 150℃; | 27% |
Conditions | Yield |
---|---|
With zinc(II) chloride at 130 - 150℃; | 24% |
Conditions | Yield |
---|---|
With sulfuric acid; water Erhitzen des mit Calciumchlorid versetzten Reaktionsgemisches mit Aethylenglykol unter Zusatz von wss. Salzsaeure; | |
With sulfuric acid; water Erhitzen des mit Calciumchlorid versetzten Reaktionsgemisches mit Aethylenglykol unter Zusatz von wss. Salzsaeure; |
[1,3,5,7,2,6]tetroxadithiocane 2,2,6,6-tetraoxide
ethylene glycol
1,3-DIOXOLANE
Conditions | Yield |
---|---|
With water |
2-ethoxy-1,3-dioxolane
triethylsilane
A
1,3-DIOXOLANE
B
ethoxytriethylsilane
C
1,2-bis (triethylsilyloxy) ethane
Conditions | Yield |
---|---|
With nickel at 65℃; for 2h; Yield given. Further byproducts given. Yields of byproduct given; |
1,2-di(1,3-dioxolan-2-yloxy)ethane
A
1,3-DIOXOLANE
B
2-ethoxy-1,3-dioxolane
C
[1,3]-dioxolan-2-one
D
(1,3-dioxolan-2-yloxy)ethanal
E
2-(1,3-dioxolan-2-yloxy)ethyl carbonate
F
formic acid ethyl ester
Conditions | Yield |
---|---|
With di-tert-butyl peroxide at 130℃; for 0.5h; Product distribution; | A 0.01 mol B 0.08 mol C 0.08 mol D 0.02 mol E 0.009 mol F 0.01 mol |
carbon monoxide
A
1,3-DIOXOLANE
B
propan-1-ol
C
ethanol
D
ethylene glycol
Conditions | Yield |
---|---|
With 2-hydroxypyridin; hydrogen; acetylacetonatodicarbonylrhodium(l) In various solvent(s) at 230℃; under 1499480 Torr; for 4.5h; Further byproducts given. Title compound not separated from byproducts; | A 2 mmol B 121 mmol C 191 mmol D 1000 mmol |
ethylene glycol
A
1,3-DIOXOLANE
B
2-methyl-1,3-dioxolane
C
2-hydroxymethyl-1,3-dioxolane
D
formic acid
E
acetic acid
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate; oxygen In water at 150℃; for 100h; Product distribution; other acetloacetonates, also in basic solution; |
A
1,3-DIOXOLANE
B
trans-9,10-dihydroxy-9,10-diphenyl-9,10-dihydroanthracene
Conditions | Yield |
---|---|
at 55℃; under 60 Torr; Thermodynamic data; ΔE(act.), var. temp and pressure; |
Conditions | Yield |
---|---|
With boron trifluoride-butyl ether complex In cyclohexane at 70℃; Title compound not separated from byproducts; | |
With boron trifluoride-butyl ether complex In cyclohexane at 70℃; Kinetics; | |
With boron trifluoride-butyl ether complex In cyclohexane at 70℃; | A n/a B n/a C 33 % Chromat. |
Conditions | Yield |
---|---|
at 140℃; |
[1,3,5,7,2,6]tetroxadithiocane 2,2,6,6-tetraoxide
water
ethylene glycol
1,3-DIOXOLANE
Conditions | Yield |
---|---|
at 140℃; |
Conditions | Yield |
---|---|
In n-heptane at 20℃; Equilibrium constant; Thermodynamic data; 1/K=0.85 l/mole ΔH=3.0 kcal/mole; |
1,3-DIOXOLANE
Conditions | Yield |
---|---|
With CO; H2 In decalin in presence of 34 atm CO; | 0% |
Conditions | Yield |
---|---|
With H5V2Mo10O40*34H2O In sulfolane Kinetics; Mechanism; Temperature; Time; Inert atmosphere; |
carbon dioxide
ethylene glycol
A
1,3-DIOXOLANE
B
2,2'-methanediyldioxy-bis-ethanol
C
ethylene glycol monoformate
Conditions | Yield |
---|---|
With aluminium(III) triflate; [Ru(1,1,1-tris(diphenylphosphinomethyl)ethane)(trimethylenemethane)]; hydrogen In 1,4-dioxane at 80℃; under 60006 Torr; for 18h; Catalytic behavior; Solvent; Autoclave; Schlenk technique; |
Conditions | Yield |
---|---|
With aluminium(III) triflate; [Ru(1,1,1-tris(diphenylphosphinomethyl)ethane)(trimethylenemethane)]; hydrogen In 1,4-dioxane at 80℃; under 60006 Torr; for 18h; Catalytic behavior; Autoclave; Schlenk technique; |
Conditions | Yield |
---|---|
With zinc(II) chloride In diethyl ether at 19 - 27℃; for 5.33333h; | 100% |
Stage #1: 1,3-DIOXOLANE With zinc(II) chloride at 20℃; for 0.5h; Inert atmosphere; Stage #2: acetyl chloride at 20 - 80℃; for 22h; Inert atmosphere; | 92% |
With zinc(II) chloride | 83% |
Conditions | Yield |
---|---|
at 0 - 20℃; | 100% |
for 2h; | 93% |
at 0℃; | 88% |
1,3-DIOXOLANE
acetaldehyde enolate
Conditions | Yield |
---|---|
With amide at 24.9℃; OH-; | 100% |
1,3-DIOXOLANE
(S)-α,α-(2-thiophenylethylamino)(2-chlorophenyl)acetonitrile hydrochloride
(S)-2-(2-chlorophenyl)-2-(6,7-dihydrothieno[3,2-c]pyridin-5(4H)-yl)acetonitrile
Conditions | Yield |
---|---|
at 90℃; for 11h; | 100% |
1,3-DIOXOLANE
homoveratrylamine hydrochloride
6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
Conditions | Yield |
---|---|
With hydrogenchloride | 99.8% |
1,3-DIOXOLANE
(S,E)-3-(p-tolylsulfinyl)-3-pentene-2-one
Conditions | Yield |
---|---|
With benzophenone for 0.166667h; Addition; Irradiation; | 99% |
Conditions | Yield |
---|---|
With (Bu4N)2S2O8 at 25℃; for 3h; Inert atmosphere; regioselective reaction; | 99% |
With 1-(tert-butylperoxy)-1,2-benziodoxol-3(1H)-one at 50℃; for 24h; | 76% |
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate) In benzene at 80℃; for 4h; | 99% |
With dirhodium tetraacetate at 60℃; for 2h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
-80°C; | 98.8% |
1,3-DIOXOLANE
(S,E)-3-[(2,4,6-triisopropylphenyl)sulfinyl]-3-pentene-2-one
(3R,4R,RS)-5,5-ethylenedioxy-4-methyl-3-[(2,4,6-triisopropylphenyl)sulfinyl]-2-pentanone
Conditions | Yield |
---|---|
With benzophenone for 0.166667h; Addition; Irradiation; | 98% |
1,3-DIOXOLANE
methyl crotonate
methyl 4,4-ethylenedioxy-3-methyl-butanoate
Conditions | Yield |
---|---|
With (Bu4N)2S2O8 at 25℃; for 15h; Inert atmosphere; regioselective reaction; | 98% |
1,3-DIOXOLANE
dimethyl cis-but-2-ene-1,4-dioate
2-(1,3-dioxolan-2-yl)butanedioic acid 1,4-dimethyl ester
Conditions | Yield |
---|---|
With (Bu4N)2S2O8 at 25℃; for 1.5h; Inert atmosphere; regioselective reaction; | 98% |
With 1-hydroxy-pyrrolidine-2,5-dione; dimethylglyoxal at 20℃; for 3h; Irradiation; Sealed tube; Inert atmosphere; | 96% |
1,3-DIOXOLANE
1,4-dimethyl but-2-enedioate
2-(1,3-dioxolan-2-yl)butanedioic acid 1,4-dimethyl ester
Conditions | Yield |
---|---|
With (Bu4N)2S2O8 at 25℃; for 1.5h; Inert atmosphere; regioselective reaction; | 98% |
Conditions | Yield |
---|---|
nickel at 80 - 100℃; for 1h; | 97% |
zinc(II) chloride at 140℃; for 12h; | 62% |
With zinc(II) chloride at 140℃; Product distribution; Rate constant; |
Conditions | Yield |
---|---|
for 1h; Ambient temperature; | 97% |
Conditions | Yield |
---|---|
With (Bu4N)2S2O8 at 20 - 25℃; | 97% |
With (Bu4N)2S2O8 at 25℃; for 18h; Inert atmosphere; regioselective reaction; | 97% |
With (Bu4N)2S2O8 at 25℃; Yield given; |
1,3-DIOXOLANE
(S)-2-[(2,4,6-triisopropylphenyl)sulfinyl]-2-cyclopentenone
(2R,3R,RS)-3-(1,3-dioxolan-2-yl)-2-[(2,4,6-triisopropylphenyl)sulfinyl]-1-cyclopentanone
Conditions | Yield |
---|---|
With benzophenone for 0.166667h; Addition; Irradiation; | 97% |
1,3-DIOXOLANE
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); 2,3,3,4,4,5-hexamethyl-2-hexanethiol at 80℃; for 10h; Sealed tube; Molecular sieve; | 97% |
Conditions | Yield |
---|---|
With fac-tris[2-phenylpyridinato-C2,N]iridium(III); (Bu4N)2S2O8 at 30℃; for 24h; Reagent/catalyst; Inert atmosphere; Sealed tube; Irradiation; | 97% |
Conditions | Yield |
---|---|
With hydrogenchloride at 90℃; for 8h; | 96% |
1,3-DIOXOLANE
(5S)-5-(tert-butyldiphenylsiloxymethyl)-2(5H)-furanone
Conditions | Yield |
---|---|
With (Bu4N)2S2O8 | 96% |
With (Bu4N)2S2O8 at 30℃; for 0.25h; | 96% |
1,3-DIOXOLANE
2-[(S)-(4-methylphenyl)sulfinyl]cyclopent-2-en-1-one
Conditions | Yield |
---|---|
With benzophenone for 0.166667h; Addition; Irradiation; | 96% |
1,3-DIOXOLANE
dichloro-(2-chloromethoxy-ethoxy)-borane
bis(chloromethoxyethoxy)chloroborane
Conditions | Yield |
---|---|
96% |
1,3-DIOXOLANE
C17H13ClN2O2
6-chloro-1-[(2'-hydroxyethoxy)methyl]-N-[(phenyl)methyl]-1,4-dihydro-4-oxoquinoline-3-carboxamide
Conditions | Yield |
---|---|
Stage #1: C17H13ClN2O2 With chloro-trimethyl-silane; N,O-Bis(trimethylsilyl)trifluoroacetamide In acetonitrile for 4h; Inert atmosphere; Reflux; Stage #2: 1,3-DIOXOLANE With chloro-trimethyl-silane; potassium iodide In acetonitrile at 20℃; for 24h; Stage #3: With water; sodium hydrogencarbonate In acetonitrile | 96% |
Conditions | Yield |
---|---|
Stage #1: 1,3-DIOXOLANE; glyoxylic acid ethyl ester; aniline In toluene at 20℃; for 1h; Sealed tube; Molecular sieve; Stage #2: With 2,2'-azobis(isobutyronitrile); 2,3,3,4,4,5-hexamethyl-2-hexanethiol In toluene at 80℃; for 12h; Sealed tube; Molecular sieve; regioselective reaction; | 96% |
Conditions | Yield |
---|---|
Stage #1: 1,3-DIOXOLANE; glyoxylic acid ethyl ester; 4-methoxy-aniline In toluene at 20℃; for 1h; Sealed tube; Molecular sieve; Stage #2: With 2,2'-azobis(isobutyronitrile); 2,3,3,4,4,5-hexamethyl-2-hexanethiol In toluene at 80℃; for 12h; Sealed tube; Molecular sieve; | 96% |
Conditions | Yield |
---|---|
With 1-hydroxy-pyrrolidine-2,5-dione; dimethylglyoxal at 20℃; Molecular sieve; Irradiation; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With Bromoform; (RCO2)2 at 20 - 60℃; for 3h; Irradiation; | 95% |
With 1,4-Dioxane Dibromide In tetrachloromethane at 29.9℃; Rate constant; Thermodynamic data; Mechanism; ΔH(excit.), ΔS(excit.), ΔG(excit.), lg A; further temp., kinetics; |
1,3-DIOXOLANE
1-(4-ethylphenyl)-1-propanone
piperidine hydrochloride
eperisone hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride at 90℃; for 6.5h; | 95% |
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