img heightAppearance:detailed see specifications Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:Used in Synthesis, Pharmaceuticals and other fields Transportation:by air or by sea Port:Shan
Cas:106-42-3
Min.Order:1 Metric Ton
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Cas:106-42-3
Min.Order:1 Metric Ton
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inquiryHebei yanxi chemical co. LTD. has expanded a compositive entity from initially only as a small manufacturer. The company dedicated to the development, production and marketing of chemicals. After many years of efforts, we have established stable
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Product Name P-XYLENE Synonyms 14-Dimethylbenzene CAS: 106-42-3 MF: - MW: - EINECS: - Product Categories
1,4-Dimethylbenzene CAS:106-42-3 Specification Item Standard Test Results Identification A.H-NMR:Comply with the structure Complies B.LC-MS:Comply with the structure Co
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:106-42-3
Min.Order:10 Gram
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inquirySuperior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
We are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
Cas:106-42-3
Min.Order:1 Kilogram
FOB Price: $5.0
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
Our advantage:Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scient
Cas:106-42-3
Min.Order:1 Kilogram
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inquiryp-XyleneAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Cas:106-42-3
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inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:106-42-3
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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p-Xylene Application:p-Xylene
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl
p-XyleneAppearance:white powder Storage:store cold at 2--8 degree in refrigerator Package:10iu*10vials*1kits Application:for injection Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:106-42-3
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryP-XYLENE Basic information Product Name: P-XYLENE Synonyms: 1,4-Xylene p-Xylene;1,4-DIMETHYLBENZENE;'LGC' (2031);1,4-dimethyl-benzen;1,4-Xylene;4-Methyltolu
Cas:106-42-3
Min.Order:21 Metric Ton
Negotiable
Type:Trading Company
inquiryConditions | Yield |
---|---|
With hydrogen In water; ethyl acetate at 50℃; under 15001.5 Torr; for 5h; | 99% |
With hydrogen In water at 25℃; for 1h; | 99% |
With hydrogen at 350℃; under 760.051 Torr; | 95% |
Conditions | Yield |
---|---|
With solid acid catalyst tin phosphate In n-heptane at 300℃; under 15001.5 Torr; for 12h; Reagent/catalyst; Solvent; Pressure; Temperature; | 90% |
With copper(II) bis(trifluoromethanesulfonate) at 250 - 270℃; under 26892.4 - 82745.9 Torr; for 5h; Inert atmosphere; | 44% |
Conditions | Yield |
---|---|
With P-containing zeolite Beta In n-heptane at 250℃; under 46504.7 Torr; Reagent/catalyst; Diels-Alder Cycloaddition; | 97% |
With benzoic acid anhydride In acetic acid at 280℃; under 63006.3 Torr; for 8h; Pressure; Reagent/catalyst; Solvent; Temperature; Time; | 92.3% |
With copper(II) bis(trifluoromethanesulfonate) In tetrahydrofuran at 270℃; under 26892.4 - 82745.9 Torr; for 5h; Catalytic behavior; Reagent/catalyst; Solvent; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
In n-heptane at 249.84℃; under 37503.8 Torr; for 24h; Reagent/catalyst; Autoclave; Inert atmosphere; | A 75% B n/a |
In acetic acid at 280℃; under 63006.3 Torr; for 4h; Pressure; Reagent/catalyst; Solvent; Temperature; Time; | A 68.5% B 12.1% |
With Sn-BEA In n-heptane at 250℃; under 46504.7 Torr; for 24h; Catalytic behavior; Kinetics; Diels-Alder Cycloaddition; Autoclave; Inert atmosphere; chemoselective reaction; | A 43% B n/a |
Conditions | Yield |
---|---|
With hydrogen; P-modified ZSM-5 In water at 480 - 485℃; under 1794.37 Torr; for 23.53h; Product distribution / selectivity; | A n/a B 15.54% C n/a |
H-ZSM-5(73) at 400℃; Product distribution; further catalysts (alumosilicates, modified zeolites); | |
Na(+)x(Mg3)(Si(4-x)Alx)O10(OH)2 at 349.9℃; for 1h; Product distribution; various pillared clays and zeolites as catalysts; |
Conditions | Yield |
---|---|
With hydrogen In water at 400℃; under 3750.38 Torr; Reagent/catalyst; Pressure; Temperature; Concentration; Inert atmosphere; | 29.3% |
With hydrogen at 250℃; Kinetics; Thermodynamic data; Further Variations:; pH-values; | |
silica bound HZSM-5 zeolite at 600℃; under 3620.13 - 4137.29 Torr; for 3.25 - 7.5h; Conversion of starting material; |
4-Methylbenzyl alcohol
benzamide
A
para-xylene
B
N-(p-methylbenzyl)benzamide
Conditions | Yield |
---|---|
With barium trifluoromethanesulfonate In toluene at 150℃; for 18h; Reagent/catalyst; Glovebox; Inert atmosphere; | A 29% B 72% |
Conditions | Yield |
---|---|
With hydrogen; silicate ITQ-13, aluminium form at 360℃; under 10343.2 Torr; Product distribution / selectivity; fixed-bed downflow reactor; | 23.5% |
MTW-zeolite/Al2O3 (Catalyst B) at 280℃; under 26618.1 Torr; Conversion of starting material; Liquid phase; | |
Ga-MFI zeolite/ZrO2/Al2O3 (Catalyst C) at 300℃; under 26618.1 Torr; Conversion of starting material; Liquid phase; |
2,5-dimethylfuran
ethene
A
para-xylene
B
3,6-dimethylcyclohex-2-enone
C
2,5-hexanedione
Conditions | Yield |
---|---|
With H-BEA-25 In 1,4-dioxane at 249.84℃; under 15001.5 Torr; for 4h; Diels-Alder Cycloaddition; Autoclave; chemoselective reaction; |
Conditions | Yield |
---|---|
With palladium on activated charcoal In toluene at 130℃; under 7500.75 - 30003 Torr; for 3h; Autoclave; |
1,4-dimethyl-7-oxa-bicyclo[2.2.1]heptane-2,3-dicarboxylic acid anhydride
A
3,6-dimethyl phthalic anhydride
B
para-xylene
Conditions | Yield |
---|---|
With zeolite Y with a silica-alumina at 200℃; for 2h; Temperature; Inert atmosphere; | A 72% B 17% |
With 1 wtpercent Pd/C loaded on zeolite H-Y with a silica-alumina ratio of 40 In toluene at 200℃; under 750.075 Torr; for 4h; Inert atmosphere; |
4-Methylbenzyl alcohol
benzamide
A
para-xylene
B
N-(p-methylbenzyl)benzamide
C
N,N′‑(4‑methylbenzylidene)bisbenzamide
Conditions | Yield |
---|---|
With indium sulfate In toluene at 150℃; for 18h; Glovebox; Inert atmosphere; | A 60% B 14% C 40% |
With zinc(II) sulfate In toluene at 150℃; for 18h; Glovebox; Inert atmosphere; | A 41% B 58% C 6% |
With zinc(II) chloride In toluene at 150℃; for 18h; Glovebox; Inert atmosphere; | A 47% B 42% C 21% |
Conditions | Yield |
---|---|
With hydrogen at 480℃; under 8826.09 Torr; Leiten ueber Platin/Aluminiumoxid-Siliciumdioxid; | |
With hydrogen; 0.3 wtpercent Pt/0.1 wtpercent S/100 wtpercent MTW-zeolite (Catatalyst C) at 370 - 375℃; under 4650.47 Torr; Conversion of starting material; | |
With hydrogen; 0.3 wtpercent Pt/0.1 wtpercent S/50 wtpercent MTW/50 wtpercent mordenite (Catalyst F) at 370 - 375℃; under 4650.47 Torr; Conversion of starting material; |
methanol
toluene
benzene
A
o-xylene
B
para-xylene
C
m-xylene
Conditions | Yield |
---|---|
With hydrogen; 1/16 inch extrudates which contained 65 weight percent H-ZSM-5 and 35 weight percent silica binder at 371.101℃; under 3309.83 Torr; | |
With hydrogen; 1/16 inch extrudates which contained 65 wt. percent H-ZSM-23 having a silica to alumina mole ratio of 110:1 and 35 wt. percent of alumina binder at 499.99℃; under 7757.43 Torr; | |
With hydrogen; SAPO-11 at 499.99℃; under 7757.43 Torr; |
Conditions | Yield |
---|---|
With hydrogen; silica selectivated ZSM-5 at 371.101℃; under 10343.2 Torr; |
Conditions | Yield |
---|---|
With triethylsilane; palladium dichloride In ethanol for 0.5h; Inert atmosphere; | A 10.0 %Chromat. B 88.5 %Chromat. |
With palladium on silica; hydrogen In dodecane at 190℃; under 22502.3 Torr; for 5h; | |
With palladium on activated charcoal; hydrogen In water at 100℃; for 10h; chemoselective reaction; | A 40 %Chromat. B 60 %Chromat. |
Conditions | Yield |
---|---|
With parent microporous ZSM-5 zeolite at 250℃; for 0.25h; Reagent/catalyst; | A 27% B 10% |
With hydrogen; H-ZSM-5 at 349.9℃; under 15001.2 Torr; Product distribution; further catalysts, variation of temperature; | |
CVD boria-alumina at 450℃; Product distribution; dependence of conversion on B2O3 content of catalyst; |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; {MoPdcp[μ-(CO)2][μ3-(CO)](PPh3)}2 In benzene at 120℃; for 15h; | 98% |
Conditions | Yield |
---|---|
With hydrogen; platinum-containing ZSM-5 molecular sieve catalyst at 420℃; under 11251.1 Torr; | |
With hydrogen; alumina-phosphate-bound MFI catalyst at 560℃; under 18376.8 Torr; Gas phase; | |
With hydrogen; alumina-phosphate-bound MFI catalyst at 560℃; under 18376.8 Torr; Gas phase; |
4-Methylbenzyl alcohol
benzamide
A
para-xylene
B
N-(p-methylbenzyl)benzamide
C
bis(4-methylbenzyl) ether
Conditions | Yield |
---|---|
With tin(II) trifluoromethanesulfonate In toluene at 150℃; for 18h; Glovebox; Inert atmosphere; | A 8% B 33% C 50% |
With zinc trifluoromethanesulfonate In toluene at 150℃; for 18h; Reagent/catalyst; Glovebox; Inert atmosphere; | A 33% B 22% C 21% |
2,5-dimethylfuran
ethene
A
para-xylene
B
p-n-propyltoluene
C
2-ethyl-p-xylene
Conditions | Yield |
---|---|
With palladium-decorated gold nanoparticles anchored on amphoteric zirconia In n-heptane at 300℃; under 30402 Torr; for 6h; |
2,5-dimethylfuran
ethene
A
4,4-dimethylcyclohexenone
B
para-xylene
C
3,6-dimethylcyclohex-2-enone
Conditions | Yield |
---|---|
With Sn-BEA In n-heptane at 275℃; under 30402 Torr; for 1h; |
Conditions | Yield |
---|---|
With palladium/alumina; hydrogen In hexane at 325℃; Flow reactor; Green chemistry; | A 84.8% B 6.5% |
With hydrogen In hexane at 325℃; Flow reactor; Green chemistry; | A 19.5% B 73.2% |
Conditions | Yield |
---|---|
With copper nickel; pyrographite In 1,2-dimethoxyethane at 85℃; for 20h; | A 10% B 90% |
With nickel In 1,2-dimethoxyethane for 2h; Ambient temperature; | A 20% B 76% |
With magnesium at 600℃; | A 23% B 60% |
With water; naphthalen-1-yl-lithium In tetrahydrofuran; diethyl ether; Petroleum ether at -95℃; for 0.75h; Title compound not separated from byproducts; | A 64 % Chromat. B 36 % Chromat. |
Conditions | Yield |
---|---|
With Ga2O3 zeolite; silica gel In gas at 400℃; Product distribution; var. catalyst, var. temp.; | |
With hydrogen; Catalyst G (prepared from NH4-ZSM-5 and H3PO4) at 200 - 500℃; under 1034.32 Torr; Product distribution / selectivity; | |
With hydrogen; Catalyst H (prepared from NH4-ZSM-5 and H3PO4) at 200 - 500℃; under 1034.32 Torr; Product distribution / selectivity; |
carbon monoxide
p-xylylene glycol
A
para-xylene
B
1,4-phenylenediacetic acid
C
4-tolylacetic acid
Conditions | Yield |
---|---|
With hydrogen iodide; tetrakis(triphenylphosphine) palladium(0) In acetone at 90℃; under 68400 Torr; for 42h; Carbonylation; reduction; | A n/a B 48% C 16% |
methanol
toluene
benzene
A
o-xylene
B
para-xylene
C
ethylbenzene
D
m-xylene
Conditions | Yield |
---|---|
With hydrogen; silicon-selectivated H-ZSM-5/silica bound at 371.101℃; under 10343.2 Torr; | |
With hydrogen; zeolite bound zeolite at 371.101℃; under 10343.2 Torr; |
Conditions | Yield |
---|---|
catalyst contained 15.0percentw EU-1 zeolite in H form, 84.7percentw Al2O3, 0.3percentw Pt and treated with dimethyldisulphide at 390℃; under 11251.1 Torr; Product distribution / selectivity; | |
catalyst contained 15.0percentw NU-87 zeolite in H form, 84.7percentw Al2O3, 0.3percentw Pt and treated with dimethyldisulphide at 390℃; under 11251.1 Torr; Product distribution / selectivity; | |
catalyst contained 8.0percentw EU-1 zeolite in H form, 7.0percentw NU-87 zeolite in H form, 84.7percentw Al2O3, 0.15percentw Pt, 0.15percentw Re and treated with dimethyldisulphide at 390℃; under 11251.1 Torr; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With palladium dichloride In methanol at 40℃; for 18h; Inert atmosphere; Green chemistry; chemoselective reaction; | 99% |
Multi-step reaction with 2 steps 1: hydrogen; / 350 °C / 760.05 Torr 2: hydrogen; / 350 °C / 760.05 Torr View Scheme | |
With formic acid; methanesulfonic acid; 1,2-bis((di-tert-butylphosphoryl)methyl)benzene; palladium(II) acetylacetonate; 1,2-bis[di(t-butyl)phosphinomethyl]benzene In 1,2-dichloro-ethane at 100℃; for 18h; Schlenk technique; Sealed tube; Inert atmosphere; | 93 %Chromat. |
With 2,4,6-trimethyl-pyridine; 4,4'-dimethoxyphenyl disulfide; iridium(lll) bis[2-(2,4-difluorophenyl)-5-methylpyridine-N,C20]-4,40-di-tert-butyl-2,20-bipyridine hexafluorophosphate; triphenylphosphine In toluene for 24h; Irradiation; | 63 %Chromat. |
carbon monoxide
toluene
A
o-xylene
B
para-xylene
C
m-xylene
Conditions | Yield |
---|---|
With hydrogen at 400℃; under 24549.5 Torr; Temperature; Flow reactor; Inert atmosphere; |
Conditions | Yield |
---|---|
With potassium bromide; sodium nitrite In water; trifluoroacetic acid at 20℃; for 0.16h; Product distribution; under argon; | 100% |
With oxygen; potassium bromide; sodium nitrite In water; trifluoroacetic acid at 20℃; for 5h; Product distribution; | 96% |
With sulfuric acid; dihydrogen peroxide; sodium bromide In water at 49.84℃; | 94% |
Conditions | Yield |
---|---|
With zeolite ZSM-5-60; Nitrogen dioxide | 100% |
With nitric acid; sulfuric acid In dichloromethane at 25℃; for 0.7h; | 100% |
With nitric acid In toluene at 60℃; for 2h; | 98% |
Conditions | Yield |
---|---|
With oxygen; 10-methyl-9-phenylacridin-10-ium perchlorate In chloroform at 24.84℃; for 10h; Oxidation; Pyrolysis; visible light; | 100% |
With sulfuric acid; 9-mesityl-2,7,10-trimethylacridinium perchlorate; water; oxygen In acetonitrile at 24.84℃; for 1.33333h; Quantum yield; Reagent/catalyst; Irradiation; | 100% |
With N-hydroxyphthalimide; oxygen; cobalt(II) acetate; acetic acid at 20℃; under 760.051 Torr; chemoselective reaction; | 100% |
Conditions | Yield |
---|---|
With bromine In tetrachloromethane Solvent; | 100% |
With 2,4,4,6-Tetrabromo-2,5-cyclohexadien-1-one; silica gel for 4.5h; UV-irradiation; | 84% |
With bromine In tetrachloromethane for 1.5h; Ambient temperature; | 83% |
Conditions | Yield |
---|---|
With hydrogen; [(norbornadiene)rhodium(I)chloride]2; phosphinated polydiacetylene In n-heptane at 30℃; under 60800 Torr; for 1.5h; | 100% |
With Ti8O8(14+)*6C8H4O4(2-)*4O(2-)*3.3Li(1+)*0.7Co(2+)*0.7C4H8O*0.7H(1-); hydrogen In neat (no solvent) at 120℃; under 37503.8 Torr; for 18h; | 100% |
With hydrogen at 150℃; under 2280.15 Torr; for 0.5h; Kinetics; Reagent/catalyst; Temperature; | 100% |
Conditions | Yield |
---|---|
With tris(fluorosulphonyl)methane at 138℃; for 3h; | 100% |
Hf[N(SO2C8F17)2]4 In various solvent(s) at 120℃; for 3h; | 98% |
With C4F9SO3H at 138℃; for 5h; | 91% |
[Cp*Ru(CH3CN)3]OTf
para-xylene
Conditions | Yield |
---|---|
In tetrahydrofuran byproducts: CH3CN; under N2; addn. of Ru-complex to p-xylene and THF (benzene-free), mixt. stirred (30°C); addn. of hexane, solid filtered, washed twice (hexane), dried (vac.), elem. anal.; | 100% |
para-xylene
3-nitro-benzaldehyde
allyl-trimethyl-silane
tetrahydro-4-(2,5-dimethylphenyl)-2,6-bis(3-nitrophenyl)-2H-pyran
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate at 0 - 20℃; for 2h; Sakurai-Hosomi-Prins-Friedel-Crafts reaction; stereoselective reaction; | 100% |
Conditions | Yield |
---|---|
at 40℃; for 480h; Gas phase; | 100% |
Conditions | Yield |
---|---|
With (diethylamino)difluorosulfonium tetrafluoroborate In dichloromethane at 20℃; for 4h; Inert atmosphere; | 100% |
para-xylene
Conditions | Yield |
---|---|
With methanesulfonic acid at 100℃; for 1h; | 100% |
para-xylene
2-bromo-5-chlorobenzyl bromide
Conditions | Yield |
---|---|
With indium(III) bromide In dichloromethane for 6h; Schlenk technique; Inert atmosphere; Molecular sieve; | 100% |
Conditions | Yield |
---|---|
With ammonium acetate; water; hydrogen bromide; oxygen; manganese(II) acetate; cobalt(II) diacetate tetrahydrate; 1-n-butyl-3-methylimidazolim bromide; acetic acid at 200℃; under 30753.1 Torr; for 10h; Time; Temperature; Reagent/catalyst; Concentration; Inert atmosphere; | 99.9% |
With oxovanadium(IV) sulfate; hydrogen bromide; oxygen; acetic acid In water at 100℃; under 750.075 Torr; for 20h; | 98% |
With oxygen; acetic acid; hydrogen bromide; cobalt(II) acetate; manganese(II) acetate In water at 200℃; under 22502.3 Torr; for 0.05h; Product distribution / selectivity; Inert atmosphere; | 98.3% |
Conditions | Yield |
---|---|
With chlorine; 3-butyl-1,2-dimethylimidazolium chloride In perfluoroheptane at 84℃; for 3h; Temperature; Solvent; | 99.11% |
With chlorine; 3-butyl-1,2-dimethylimidazolium chloride at 120℃; for 3h; Reagent/catalyst; Temperature; Ionic liquid; Irradiation; | 99.1% |
durch Chlorieren; |
para-xylene
Conditions | Yield |
---|---|
Stage #1: para-xylene With 1-dodecyl-3-methylimidazol-1-ium chloride at 110℃; Irradiation; Stage #2: With chlorine at 90 - 120℃; Reagent/catalyst; Temperature; Reflux; | 99.11% |
1,1-Diphenylmethanol
para-xylene
((2,5-dimethylphenyl)methylene)dibenzene
Conditions | Yield |
---|---|
With silica gel supported sodium hydrogen sulfate at 80℃; for 0.5h; Friedel-Crafts type alkylation; | 99% |
With H5CoW12O40 supported on rice husk ash extracted nano silica at 60℃; for 0.666667h; Reagent/catalyst; Green chemistry; | 98% |
With Fe3O4/FeO at 60℃; for 0.333333h; Green chemistry; | 92% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; water at 20℃; for 10h; Inert atmosphere; | 99% |
With N-hydroxy-tetrahydrophthalimide; oxygen; nitric acid at 50℃; under 750.075 - 1500.15 Torr; for 25h; Autoclave; Green chemistry; | 91.16% |
With MoO(O2)(8-quinolinolate)2; dihydrogen peroxide In acetonitrile for 6h; Oxidation; Heating; | 88% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In chloroform at 0 - 20℃; Inert atmosphere; | 99% |
With aluminum (III) chloride In carbon disulfide at 0 - 20℃; Friedel Crafts acylation; Inert atmosphere; | 95% |
Friedel-Crafts alkylation; | 90% |
Conditions | Yield |
---|---|
sulfated zirconia at 100℃; for 2h; Product distribution; Further Variations:; Catalysts; Friedel-Crafts acylation; | 99% |
With C4F9SO3H at 138℃; for 5h; | 93% |
Conditions | Yield |
---|---|
With indium(III) chloride; 4 A molecular sieve In dichloromethane at 20℃; for 16h; Friedel-Crafts alkylation; | 99% |
With potassium cyanide; aluminum oxide at 50℃; for 5h; | 83 % Chromat. |
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