CAS No.593-80-6,dimethyl telluride Suppliers

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ZHEJIANG JIUZHOU CHEM CO.,LTD

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Molekula Limited

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Molekula GmbH

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Allorachem Srl

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Synthetic route

: 74-88-4
methyl iodide

: 593-80-6
dimethyltellurium

Conditions

Conditions	Yield
With potassium hydroxide; tellurium; tin(ll) chloride In dimethyl sulfoxide at 70℃; for 2h;	97%
With potassium hydroxide; tellurium; hydrazine hydrate at 60 - 70℃;	85%

: 93-58-3
benzoic acid methyl ester

A: 593-80-6
dimethyltellurium

B: 65-85-0
benzoic acid

Conditions

Conditions	Yield
With tellurium; sodium tetrahydroborate; tert-butyl alcohol In N,N-dimethyl-formamide at 80 - 90℃; for 0.25h; also other alkyl carboxylates and tellurium reagents;	A n/a B 95%

: 18987-26-3
trimethyltelluronium iodide

: 593-80-6
dimethyltellurium

Conditions

Conditions	Yield
With triphenylphosphine at 160℃; for 0.0833333h;	90%
at 100℃;
at 100℃;

: 55642-42-7
bis(trifluoromethyl)tellurium

: 544-97-8
dimethyl zinc(II)

A: 593-80-6
dimethyltellurium

B: 57365-42-1
Trifluoro-methyltellanyl-methane

C: C6H14O3*C2F6Zn

Conditions

Conditions	Yield
With diethylene glycol dimethyl ether In acetonitrile for 24h;	A n/a B 78% C n/a

...Expand

: 74-88-4
methyl iodide

A: 75-18-3
dimethylsulfide

B: 593-80-6
dimethyltellurium

Conditions

Conditions	Yield
With potassium disulfide; potassium ditelluride; hydrazine hydrate at 20 - 25℃;	A 42% B 74%

: 74-86-2
acetylene

: 74-88-4
methyl iodide

A: 593-80-6
dimethyltellurium

B: 63000-06-6
divinyltellane

C: 94718-60-2
methyl vinyl telluride

Conditions

Conditions	Yield
With potassium hydroxide; tellurium; tin(ll) chloride In N,N,N,N,N,N-hexamethylphosphoric triamide; water at 105 - 115℃; under 6080 - 11400 Torr; for 5h; Product distribution; var. allyl halide, var.: without HMPA;	A 8% B 55% C 20%
With potassium hydroxide; tellurium; tin(ll) chloride In N,N,N,N,N,N-hexamethylphosphoric triamide; water at 105 - 115℃; under 6080 - 11400 Torr; for 5h;	A 8% B 55% C 20%
With potassium hydroxide; tellurium; tin(ll) chloride In N,N,N,N,N,N-hexamethylphosphoric triamide; water at 105 - 115℃; under 10640 Torr; for 5h;	A 8% B 55% C 20%

...Expand

: 74-86-2
acetylene

A: 593-80-6
dimethyltellurium

B: 63000-06-6
divinyltellane

C: 94718-60-2
methyl vinyl telluride

Conditions

Conditions	Yield
With potassium hydroxide; tellurium; tin(ll) chloride; methyl iodide In N,N,N,N,N,N-hexamethylphosphoric triamide; water at 105 - 115℃; under 10640 Torr; for 5h;	A 8% B 55% C 20%
With potassium hydroxide; tellurium; tin(ll) chloride; methyl iodide In N,N,N,N,N,N-hexamethylphosphoric triamide; water at 105 - 115℃; under 6080 - 11400 Torr; for 5h; var. allyl halide, without HMPA;	A 8% B n/a C 20%

...Expand

: 74-88-4
methyl iodide

A: 593-80-6
dimethyltellurium

B: 63000-06-6
divinyltellane

C: 94718-60-2
methyl vinyl telluride

Conditions

Conditions	Yield
With potassium hydroxide; tellurium; tin(ll) chloride; acetylene In N,N,N,N,N,N-hexamethylphosphoric triamide; water at 105 - 115℃; under 6080 - 11400 Torr; for 5h;	A 8% B 55% C 20%
With potassium hydroxide; tellurium; tin(ll) chloride; acetylene In N,N,N,N,N,N-hexamethylphosphoric triamide; water at 105 - 115℃; under 10640 Torr; for 5h;	A 8% B 55% C 20%

...Expand

: 74-88-4
methyl iodide

A: 593-80-6
dimethyltellurium

B: 20334-43-4
dimethyl ditelluride

Conditions

Conditions	Yield
With potassium hydroxide; tellurium; hydrazine hydrate at 40 - 50℃;	A 48% B 37%
With sodium hydroxide; tellurium; cetyltrimethylammonim bromide; sodium glycolate Yield given. Multistep reaction;

: 20334-43-4
dimethyl ditelluride

: 75-09-2
dichloromethane

A: 593-80-6
dimethyltellurium

B: 100207-53-2
bis(methyltellanyl)methane

Conditions

Conditions	Yield
Stage #1: dimethyl ditelluride With potassium hydroxide; hydrazine hydrate at 80 - 85℃; for 2h; Stage #2: dichloromethane at 40 - 42℃; for 1h;	A 5% B 43%

...Expand

: 20334-43-4
dimethyl ditelluride

: 75-34-3
1,1-dichloroethane

A: 593-80-6
dimethyltellurium

B: 1221001-23-5
1,1-bis(methyltellanyl)ethane

C: 79971-49-6
methyl ethyl ditelluride

Conditions

Conditions	Yield
Stage #1: dimethyl ditelluride With hydrazine hydrate; potassium hydroxide at 80 - 85℃; for 2.5h; Stage #2: 1,1-dichloroethane at 30 - 35℃; for 3h;	A 8% B 27% C 36%

...Expand

Na2(Te,Po): Na2(Te,Po)

: 77-78-1
dimethyl sulfate

A: 593-80-6
dimethyltellurium

B: dimethyl polonium

Conditions

Conditions	Yield
In water with H2 satd. soln.; vac. distn. of the dark brown mass at 20 Hgmm in oil bath;	A n/a B 9.6%
In water with H2 satd. soln.; vac. distn. of the dark brown mass at 20 Hgmm in oil bath;	A n/a B 9.6%

...Expand

: 67-56-1
methanol

: 593-80-6
dimethyltellurium

Conditions

Conditions	Yield
With aluminum telluride at 320 - 335℃;

: 2229-07-4
methyl radical

: 593-80-6
dimethyltellurium

Conditions

Conditions	Yield
With hydrogen telluride

: 18879-38-4
dimethyl tellurium diiodide

: 593-80-6
dimethyltellurium

Conditions

Conditions	Yield
With water; sodium carbonate; sodium sulfite at 75℃;

: 62-49-7
choline

: 593-80-6
dimethyltellurium

Conditions

Conditions	Yield
With sodium tellurite; sodium formate

: 107-43-7
betaine

: 593-80-6
dimethyltellurium

Conditions

Conditions	Yield
With sodium tellurite; sodium formate

: 141-53-7
sodium formate

: 593-80-6
dimethyltellurium

Conditions

Conditions	Yield
With potassium tellurite; choline chloride
With potassium tellurite; betaine

: 55642-42-7
bis(trifluoromethyl)tellurium

: 544-97-8
dimethyl zinc(II)

A: 593-80-6
dimethyltellurium

B: 57365-42-1
Trifluoro-methyltellanyl-methane

C: 115367-57-2
methyl(pentafluorophenyl)tellurium

D: C6H14O3*C2H3CdF3

E: C6H14O3*C2H3F3Zn

F: C6H14O3*C2F6Zn

Conditions

Conditions	Yield
With diethylene glycol dimethyl ether In trichlorofluoromethane at 0℃; for 24h; Mechanism; Product distribution; var. ratio of perfluoroorgano-tellur/dialkylmetal compound, solvent, temp., time;

...Expand

: 55642-42-7
bis(trifluoromethyl)tellurium

: 506-82-1
dimethylcadmium

A: 593-80-6
dimethyltellurium

B: 57365-42-1
Trifluoro-methyltellanyl-methane

C: 1,1-Difluoro-1-methyltellanyl-ethane

Conditions

Conditions	Yield
In trichlorofluoromethane at 0℃;

...Expand

: 57365-42-1
Trifluoro-methyltellanyl-methane

: 544-97-8
dimethyl zinc(II)

A: 593-80-6
dimethyltellurium

B: C6H14O3*C2H3F3Zn

Conditions

Conditions	Yield
With diethylene glycol dimethyl ether In trichlorofluoromethane for 24h; Yield given;

...Expand

: 57365-42-1
Trifluoro-methyltellanyl-methane

: 506-82-1
dimethylcadmium

A: 593-80-6
dimethyltellurium

B: C6H14O3*C2H3CdF3

Conditions

Conditions	Yield
With diethylene glycol dimethyl ether In trichlorofluoromethane for 24h; Yield given;

...Expand

: 57365-42-1
Trifluoro-methyltellanyl-methane

: C6H14O3*C2H3CdF3

A: 593-80-6
dimethyltellurium

B: bis(trifluoromethyl)cadmium, diglyme adduct

Conditions

Conditions	Yield
With diethylene glycol dimethyl ether In trichlorofluoromethane at 0℃; for 24h; Yield given;

...Expand

: 57365-42-1
Trifluoro-methyltellanyl-methane

: C6H14O3*C2H3F3Zn

A: 593-80-6
dimethyltellurium

B: C6H14O3*C2F6Zn

Conditions

Conditions	Yield
With diethylene glycol dimethyl ether In trichlorofluoromethane at 0℃; for 24h; Yield given;

...Expand

: dimethyltelluronium allylide

: 100-52-7
benzaldehyde

A: 20248-57-1
2-phenyl-3-vinyloxirane

B: 593-80-6
dimethyltellurium

Conditions

Conditions	Yield
In tetrahydrofuran Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

...Expand

: 89110-81-6
diisobutyl telluronium allylide

: 100-52-7
benzaldehyde

: 593-80-6
dimethyltellurium

Conditions

Conditions	Yield
In tetrahydrofuran Ambient temperature; moderate cis-selectivity;

: 20334-43-4
dimethyl ditelluride

: 536-74-3
phenylacetylene

: 74-88-4
methyl iodide

A: 593-80-6
dimethyltellurium

B: 19859-25-7
1-methyltelluro-2-phenylethyne

Conditions

Conditions	Yield
With potassium hydroxide; dibenzo-18-crown-6 In benzene for 2h; Mechanism; Ambient temperature; other substrates;

...Expand

: 115367-57-2
methyl(pentafluorophenyl)tellurium

: C6H14O3*C2H3CdF3

A: 593-80-6
dimethyltellurium

B: C12CdF10*C6H14O3

Conditions

Conditions	Yield
With diethylene glycol dimethyl ether In trichlorofluoromethane at 0℃; for 24h; Yield given;

...Expand

: 115367-57-2
methyl(pentafluorophenyl)tellurium

: C6H14O3*C2H3F3Zn

A: 593-80-6
dimethyltellurium

B: C12F10Zn*C6H14O3

Conditions

Conditions	Yield
With diethylene glycol dimethyl ether In trichlorofluoromethane at 0℃; for 24h; Yield given;

...Expand

: 593-80-6
dimethyltellurium

: (η-cyclopentadienyl)2(μ-carbonyl)(μ-η2-CF3C2CF3)dirhodium

: 253685-98-2
[(η(5)-C5H5)2Rh2(CO)(μ-η(1):η(1)-CF3C2CF3)(TeMe2)]

Conditions

Conditions	Yield
In dichloromethane stirring (30 min); evapn., chromy. (CH2Cl2 / hexane = 1 : 1), extg. (CH2Cl2), evapn.; elem.anal.;	100%

: 52741-69-2
1-(iodomethyl)silatrane

: 593-80-6
dimethyltellurium

: 120220-00-0
dimethyl(silatran-1-yl-methyl)telluronium iodide

Conditions

Conditions	Yield
In acetonitrile for 1h; Ambient temperature;	95%

: cyclopentadienyldicarbonyl(tetrahydrofuran)iron(II) tetrafluoroborate

: 593-80-6
dimethyltellurium

: {C5H5Fe(CO)2(Te(CH3)2)}(1+)*BF4(1-)={C5H5Fe(CO)2(Te(CH3)2)}BF4

Conditions

Conditions	Yield
In dichloromethane to soln. of Fe complex in CH2Cl2 added ligand under Ar, stirred at roomtemp. for several h; filtered, concd. in vac., filtered in petroleum/Et2O, ppt. washed with Et2O and petroleum, dried in high vac., recrystd. (CH2Cl2/Et2O); elem. anal.;	95%

: 593-80-6
dimethyltellurium

: {(η5-C5H5)Fe(P(OMe)3)2(NCEt)}PF6

: {(η5-C5H5)Fe(P(OMe)3)2(TeMe2)}PF6

Conditions

Conditions	Yield
In neat (no solvent) byproducts: EtCN; N2 atmosphere; refluxing (1 h); evapn. (vac.), dissoln. in CH2Cl2/ether (1:2), filtration, crystn. (-78°C, 1-4 d);	95%

: 593-80-6
dimethyltellurium

: {(η5-C5H5)Fe(P(OMe)3)2(NCMe)}PF6

: {(η5-C5H5)Fe(P(OMe)3)2(TeMe2)}PF6

Conditions

Conditions	Yield
In neat (no solvent) byproducts: acetonitrile; N2 atmosphere; refluxing (1 h); evapn. (vac.), dissoln. in CH2Cl2/ether (1:2), filtration, crystn. (-78°C, 1-4 d); elem. anal.;	95%

: 593-80-6
dimethyltellurium

: {(η5-C5H5)Fe(P(OMe)3)2(NCPr)}PF6

: {(η5-C5H5)Fe(P(OMe)3)2(TeMe2)}PF6

Conditions

Conditions	Yield
In neat (no solvent) byproducts: n-PrCN; N2 atmosphere; refluxing (1 h); evapn. (vac.), dissoln. in CH2Cl2/ether (1:2), filtration, crystn. (-78°C, 1-4 d);	95%

: {C5H5NiC5H6}(1+)*{BF4}(1-)

: 593-80-6
dimethyltellurium

: 87105-55-3
(C5H5)Ni(Te(CH3)2)2(1+)*BF4(1-)=((C5H5)Ni(Te(CH3)2)2)BF4

Conditions

Conditions	Yield
In diethyl ether byproducts: cyclopentadiene; Ni-complex and Me2Te were stirred in ether under inert atmosphere for 2h at room temp.; ppt. was filtered, washed with ether, dried under high vac.; elem. anal.;	95%

: ferrocenium hexafluorophosphate

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 593-80-6
dimethyltellurium

: 106468-27-3
[C5H5Fe(CO)2(Te(CH3)2)](1+)*PF6(1-)=[C5H5Fe(CO)2(Te(CH3)2)]PF6

Conditions

Conditions	Yield
In dichloromethane byproducts: (C5H5)2Fe; addn. of ferricinium compd. to Fe complex soln. in the presence of TeMe2 under Ar; filtration; evapn. to 1/3 the volume; addn. of ether/pentane3/1); pptn.; thoroughly washing (ether, pentane); drying (high vac.);	94%

...Expand

: 593-80-6
dimethyltellurium

: 100-39-0
benzyl bromide

: benzyldimethyltelluronium bromide

Conditions

Conditions	Yield
In methanol at 20℃; for 2h;	92%

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 1282-37-7
ferrocenium(III) tetrafluoroborate

: 593-80-6
dimethyltellurium

: {C5H5Fe(CO)2(Te(CH3)2)}(1+)*BF4(1-)={C5H5Fe(CO)2(Te(CH3)2)}BF4

Conditions

Conditions	Yield
In dichloromethane byproducts: (C5H5)2Fe; addn. of ferricinium compd. to Fe complex soln. in the presence of TeMe2 under Ar; filtration; evapn. to 1/3 the volume; addn. of ether/pentane3/1); pptn.; thoroughly washing (ether, pentane); drying (high vac.);	92%

...Expand

: 593-80-6
dimethyltellurium

: {(η5-C5H5)Fe(dppe)(NCEt)}PF6

: {(η5-C5H5)Fe(dppe)(TeMe2)}PF6

Conditions

Conditions	Yield
In neat (no solvent) byproducts: EtCN; N2 atmosphere; refluxing (1 h); evapn. (vac.), dissoln. in CH2Cl2/ether (1:2), filtration, crystn. (-78°C, 1-4 d);	92%

: 593-80-6
dimethyltellurium

: {(η5-C5H5)Fe(dppe)(NCPr)}PF6

: {(η5-C5H5)Fe(dppe)(TeMe2)}PF6

Conditions

Conditions	Yield
In neat (no solvent) byproducts: n-PrCN; N2 atmosphere; refluxing (1 h); evapn. (vac.), dissoln. in CH2Cl2/ether (1:2), filtration, crystn. (-78°C, 1-4 d);	92%

: {(η5-C5H5)Fe(dppe)(NCMe)}PF6

: 593-80-6
dimethyltellurium

: {(η5-C5H5)Fe(dppe)(TeMe2)}PF6

Conditions

Conditions	Yield
In neat (no solvent) byproducts: acetonitrile; N2 atmosphere; refluxing (1 h); evapn. (vac.), dissoln. in CH2Cl2/ether (1:2), filtration, crystn. (-78°C, 1-4 d); elem. anal.;	92%

: 15226-74-1, 61091-28-9, 61117-58-6
dicobalt octacarbonyl

: 1282-37-7
ferrocenium(III) tetrafluoroborate

: 593-80-6
dimethyltellurium

: 106453-63-8
[Co(CO)3(Te(CH3)2)2](1+)*BF4(1-)=[Co(CO)3(Te(CH3)2)2]BF4

Conditions

Conditions	Yield
In dichloromethane byproducts: (C5H5)2Fe; addn. of ferricinium compd. to Co complex soln. in the presence of TeMe2 under Ar; filtration; evapn. to 1/3 the volume; addn. of ether/pentane(3/1); pptn.; thoroughly washing (ether, pentane); drying (high vac.); elem. anal.;	91%

...Expand

: 593-80-6
dimethyltellurium

: η5-cyclopentadienyliodobis(dimethyl sulfide)cobalt(III) tetrafluoroborate

: η5-cyclopentadienylbis(dimethyltelluride)iodocobalt(III) tetrafluoroborate

Conditions

Conditions	Yield
In acetone byproducts: S(CH3)2; under Ar, soln. of (CpCo(SMe2)2I)BF4 (1 mmol) in acetone stirred with TeMe2 (2.2 mmol) for 5 min; solid pptd. by addn. of ether, filtered, recrystd. from CH2Cl2/ether, dried in vac.; elem. anal.;	90%

: 14516-54-2
bromopentacarbonylmanganese(I)

: 593-80-6
dimethyltellurium

: 96665-33-7
MnBr(CO)4(Te(CH3)2)

Conditions

Conditions	Yield
In hexane under N2 or Ar; the Te compd was added to a soln. of the Mn complex in hexane, heated at 50°C for 1 h; removal of solvent under reduced pressure, recrystd. from pentane;	89%

: 593-80-6
dimethyltellurium

: {(η5-C5H5)Fe(P(OPh)3)2(NCMe)}BF4

: {(η5-C5H5)Fe(P(OPh)3)2(TeMe2)}BF4

Conditions

Conditions	Yield
In neat (no solvent) byproducts: acetonitrile; N2 atmosphere; refluxing (1 h); evapn. (vac.), dissoln. in CH2Cl2/ether (1:2), filtration, crystn. (-78°C, 1-4 d); elem. anal.;	87%

: 1282-37-7
ferrocenium(III) tetrafluoroborate

: tetracarbonyldicyclopentadienyldimolybdenum

: 593-80-6
dimethyltellurium

: {C5H5Mo(CO)2(TeMe2)2}BF4

Conditions

Conditions	Yield
In dichloromethane byproducts: ferrocene; (Ar); stirring the mixt. 10 min at room temp.; filtration; washing (diethyl ether); vacuum drying; recrystn. (CH2Cl2/(C2H5)2O); elem. anal.;	86%

...Expand

: C5H5Co(S(CH3)2)2H(1+)*BF4(1-)={C5H5Co(S(CH3)2)2H}BF4

: 593-80-6
dimethyltellurium

: C5H5Co(Te(CH3)2)2H(1+)*BF4(1-)={C5H5Co(Te(CH3)2)2H}BF4

Conditions

Conditions	Yield
In diethyl ether byproducts: S(CH3)2; stirring soln. of educts, room temp., overnight; pptn.; under Ar; washing (ether); drying in vac.; recrystn. (CH2Cl2/ether); elem. anal.;	86%

: (η5C5H5)Co(SMe2)3(BF4)2

: 593-80-6
dimethyltellurium

: (η5-cyclopentadienyl)tris(dimethyltelluride)cobalt(III) tetrafluoroborate

Conditions

Conditions	Yield
In acetone byproducts: S(CH3)2; under Ar, suspn. of (CpCo(SMe2)3)(BF4)2 (2 mmol) in acetone treated with TeMe2 (6.5 mmol), react. time 10-30 min; filtered, residue washed with CH2Cl2 and ether, dried in vac., recrystd. from MeNO2/CH2Cl2 (as required); elem. anal.;	86%

: 593-80-6
dimethyltellurium

: 79-10-7
acrylic acid

: 1246274-72-5
DMTeP*HCl

Conditions

Conditions	Yield
With hydrogenchloride In water at 80℃; for 2h;	86%

: pentacarbonyl(methyl)manganese(I)

: 593-80-6
dimethyltellurium

: 159125-25-4
Mn(CO)4(CH3CO)(Te(CH3)2)

Conditions

Conditions	Yield
In tetrahydrofuran under N2 or Ar; the Te compd. was added to a soln. of the Mn complex inTHF, stirred for 2 h at room temp.; solvent was removed under reduced pressure, chromy. on alumina (n-pentane), removal of solvent; elem. anal.;	85%

: cobalt tricarbonyl nitrosyl

: 593-80-6
dimethyltellurium

: 176704-09-9
[Co(NO)(CO)2(Te(CH3)2)]

Conditions

Conditions	Yield
In neat (no solvent) byproducts: CO; (N2); stirring (room temp., ca. 3 d); removal of volatiles (reduced pressure); elem. anal.;	81%

: 593-80-6
dimethyltellurium

: 13450-91-4
gallium(III) iodide

: 1095563-41-9
[GaI3(TeMe2)]

Conditions

Conditions	Yield
In dichloromethane (N2); addn. of dimethyltelluride to CH2Cl2 soln. of gallium compd.; evapn., elem. anal.;	80%

: 13814-74-9
oxomolybdenum(V) chloride

: 593-80-6
dimethyltellurium

: C4H12Cl6Mo2O2Te2

Conditions

Conditions	Yield
In toluene for 1h;	78%

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