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Conditions | Yield |
---|---|
With potassium carbonate |
Conditions | Yield |
---|---|
With potassium carbonate | |
With potassium carbonate In acetone for 20h; Reflux; |
Conditions | Yield |
---|---|
unter Wasserstoff; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 2: alkaline aqueous H2O2 3: potassium carbonate View Scheme | |
Multi-step reaction with 3 steps 2: alkaline aqueous H2O2 3: potassium carbonate View Scheme | |
Multi-step reaction with 3 steps 1: hexan-1-amine / 6 h / Heating 2: dihydrogen peroxide; pyridine; sodium hydroxide / water / 1.5 h / 20 °C 3: potassium carbonate / acetone / 20 h / Reflux View Scheme |
5-allyl-2-hydroxy-3-methoxybenzaldehyde
myristicin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: alkaline aqueous H2O2 2: potassium carbonate View Scheme | |
Multi-step reaction with 2 steps 1: alkaline aqueous H2O2 2: potassium carbonate View Scheme | |
Multi-step reaction with 2 steps 1: dihydrogen peroxide; pyridine; sodium hydroxide / water / 1.5 h / 20 °C 2: potassium carbonate / acetone / 20 h / Reflux View Scheme |
2-allyloxy-3-methoxy-phenol
myristicin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 170 - 200 °C / unter Wasserstoff 2: potassium carbonate View Scheme | |
Multi-step reaction with 2 steps 1: 170 - 200 °C / unter Wasserstoff 2: potassium carbonate View Scheme |
2-(allyloxy)-6-methoxyphenol
myristicin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 170 - 200 °C / unter Wasserstoff 2: potassium carbonate View Scheme | |
Multi-step reaction with 2 steps 1: 170 - 200 °C / unter Wasserstoff 2: potassium carbonate View Scheme |
myristicin
2-bromo-1-(3-methoxy-4,5-methylenedioxyphenyl)propane
Conditions | Yield |
---|---|
With hydrogen bromide at 20℃; | 99.22% |
myristicin
4-methoxy-6-propyl-benzo[1,3]dioxole
Conditions | Yield |
---|---|
With 1% Pd on activated carbon; hydrogen In water at 20℃; under 760.051 Torr; for 12h; Reagent/catalyst; Green chemistry; chemoselective reaction; | 99% |
With ethanol; palladium Hydrogenation; | |
With hydrogen In methanol at 20℃; under 15001.5 Torr; for 2h; Autoclave; |
myristicin
ethyl 2-chloro-2-(hydroxyimino)acetate
ethyl 5-(3-methoxy-4,5-methylenedioxybenzyl)-4,5-dihydroisoxazole-3-carboxylate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 24h; | 69% |
myristicin
N-hydroxy-4-methoxy-benzenecarboximidoyl chloride
5-[(7-methoxy-1,3-benzodioxol-5-yl)methyl]-3-(4-methoxyphen-yl)-4,5-dihydroisoxazole
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 17h; | 68% |
With triethylamine In dichloromethane for 24h; | 67% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane for 0.25h; Reflux; | A 20% B 55% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane for 0.25h; Reflux; | A 10% B 54% |
myristicin
3-(3-methoxy-4,5-methylenedioxy-phenyl)-2-propen-1-ol
Conditions | Yield |
---|---|
With selenium(IV) oxide In 1,4-dioxane; water at 85℃; for 0.0833333h; | 24% |
myristicin
MMDA
Conditions | Yield |
---|---|
With ammonium hydroxide; Spirulina platensis phenylalanine ammonia-lyase In acetone at 37℃; for 1h; pH=8; Reagent/catalyst; Enzymatic reaction; | 15.3% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane for 0.25h; Reflux; | A 10% B 2% |
Conditions | Yield |
---|---|
With benzene |
Conditions | Yield |
---|---|
With diethyl ether im Dunkeln; |
myristicin
trans-isomyristicin
Conditions | Yield |
---|---|
With potassium hydroxide | |
With sodium under 10 Torr; beim Destillieren; |
Conditions | Yield |
---|---|
With potassium permanganate; water | |
Multi-step reaction with 3 steps 1.1: tetrabutylammomium bromide; potassium hydroxide / 0.67 h / 100 °C 2.1: pyridine; ozone / methanol; chloroform / -15 - 0 °C 3.1: ammonium hydroxide; iodine / tetrahydrofuran; water / 16 h / 20 °C 3.2: 4 h / Reflux View Scheme | |
Multi-step reaction with 3 steps 1: tetrabutylammomium bromide; potassium hydroxide / 0.67 h / 100 °C 2: pyridine; ozone / methanol; chloroform / -15 - 0 °C 3: urea hydrogen peroxide adduct; sodium hydroxide / methanol; water / Reflux View Scheme | |
Multi-step reaction with 3 steps 1: tetrabutylammomium bromide; potassium hydroxide / 0.67 h / 100 °C / Neat (no solvent) 2: pyridine; ozone / methanol; chloroform / -15 °C 3: urea hydrogen peroxide adduct; sodium hydroxide / methanol; water / 1.5 h / Reflux View Scheme | |
Multi-step reaction with 3 steps 1: potassium hydroxide / 0.67 h / 100 °C 2: ozone; pyridine / methanol; chloroform / -15 °C 3: urea hydrogen peroxide adduct / methanol / 1.5 h / Reflux View Scheme |
myristicin
A
5-methoxy-3,4-methylenedioxybenzoic acid
B
(7-methoxy-benzo[1,3]dioxol-5-yl)-acetic acid
Conditions | Yield |
---|---|
With potassium permanganate; ethanol; sodium sulfate Reagens 4: Magnesiumcarbonat; |
myristicin
2′,3′-dihydroxymyristicin
Conditions | Yield |
---|---|
With potassium hydroxide; potassium permanganate |
myristicin
Conditions | Yield |
---|---|
With ethanol; iodine; mercury(II) oxide |
myristicin
Conditions | Yield |
---|---|
With palladium on activated charcoal; Lindlar's catalyst; ozone; ethyl acetate at -12℃; Erwaermen des Reaktionsprodukts mit Methanol, Hydroxylamin-hydrochlorid und wss. Kalilauge; |
myristicin
4,6-dibromo-5-(2,3-dibromo-propyl)-7-methoxy-benzo[1,3]dioxole
Conditions | Yield |
---|---|
With bromine; acetic acid at 0℃; |
myristicin
Conditions | Yield |
---|---|
With cis-nitrous acid |
Conditions | Yield |
---|---|
With trichlorophosphate 1) chlorobenzene, 2 h, 0 deg C, 2) chlorobenzene, 80 h, r.t.; Yield given. Multistep reaction; |
myristicin
A
trans-isomyristicin
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol for 15h; Heating; Yield given. Yields of byproduct given; | |
With potassium hydroxide In ethanol for 15h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
at 0℃; |
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