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inquiryLead acetate trihydrate Basic information Product Name: Lead acetate trihydrate Synonyms: PLATINIZING SOLUTION;PLATINIZING SOLUTION, ASTM;Lead(Ⅱ) acetate trihydrate;LEAD(II) ACETATE TRIHYDRATE, REAGENTPLUS , 99.99+%;LEAD ACETATE-3-HYDRATE R. G.
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inquiryLead acetate trihydrate Chemical Properties Melting point 75 °C (dec.)(lit.) Boiling point 280°C density 2,55 g/cm3 storage temp. 2-8°C solubility 443g/l form Solid Specific Gravity 2.55 color White or color
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inquiryConditions | Yield |
---|---|
With sodium carbonate In acetic acid preparation of PbCO3 by treatment of PbCl2 with 1.5fold excess Na2CO3, treatment with acetic acid;; | 86.5% |
With Na2CO3 In acetic acid aq. acetic acid; preparation of PbCO3 by treatment of PbCl2 with 1.5fold excess Na2CO3, treatment with acetic acid;; | 86.5% |
Conditions | Yield |
---|---|
With lead | |
With lead(II) oxide | |
With lead; air |
Conditions | Yield |
---|---|
In acetic acid 20% acetic acid, 380°C, stirring until a pH of 5.5 results, treatment of soln. with activated coal, further treatment at 30°C with activated coal and salicylic acid, thiosalicylic acid or thiocyanates;; product contains less than 5E-6% Fe(3+);; | |
In acetic acid aq. acetic acid; dissolving PbO in dild. acetic acid;; | |
In acetic acid aq. acetic acid; 20% acetic acid, 380°C, stirring until a pH of 5.5 results, treatment of soln. with activated coal, further treatment at 30°C with activated coal and salicylic acid, thiosalicylic acid or thiocyanates;; product contains less than 5E-6% Fe(3+);; |
Conditions | Yield |
---|---|
In ethyl acetate treatment with ethyl acetate in presence of H2O;; | |
In ethyl acetate treatment with ethyl acetate in presence of H2O;; |
Conditions | Yield |
---|---|
With air In acetic acid aq. acetic acid; treatment of Pb with aq. acetic acid in presence of air;; |
Conditions | Yield |
---|---|
With sodium hydroxide In acetic acid separation of sulfate with hot NaOH, react. with acetic acid;; | |
With NaOH In acetic acid aq. acetic acid; separation of sulfate with hot NaOH, react. with acetic acid;; |
Conditions | Yield |
---|---|
In acetic acid dissolving in hot dild. acetic acid, crystn. on cooling;; | |
In acetic acid aq. acetic acid; dissolving in hot dild. acetic acid, crystn. on cooling;; |
lead(II) carbonate
water
acetic acid
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
In acetic acid | |
In acetic acid aq. acetic acid; |
Conditions | Yield |
---|---|
In water | |
In water with concd. alk. acetate soln. at 25°C;; | |
In water with concd. alk. acetate soln. at 25°C;; | |
In water |
Conditions | Yield |
---|---|
In water | |
In water |
Conditions | Yield |
---|---|
In neat (no solvent) over H2SO4 in 7d;; | 100% |
In neat (no solvent) loss of 3mol H2O in vac. over BaO;; | |
In neat (no solvent) complete loss of H2O in vac. over H2SO4 within 8d at 0°C, in 2d at 22°C;; | >99 |
lead(II) acetate trihydrate
(1,1’-(pyridine-2,6-diyl)bis(ethan-1-yl-1-ylidene))dibenzohydrazine
Conditions | Yield |
---|---|
With triethylamine In methanol for 2h; | 99% |
lead(II) acetate trihydrate
{Pb(1,2-bis(3,5-di(t-butyl)-2-mercaptophenylthio)ethane)(2-)}
Conditions | Yield |
---|---|
With C4H9Li In methanol under N2, BuLi added to t-bu-S4-H2 in THF at -78°C, warmed to 25°C, solvent removed, CH3OH added, solution added to Pb(CH3COO)2 in CH3OH, stirred for 2 h; filtered, washed (cold CH3OH), dried in vacuo for 12 h; elem. anal., NMR, mass spectroscopy; | 98% |
ammonium diphenyldithiophosphinate
lead(II) acetate trihydrate
bis(diphenyldithiophosphinato)lead(II)
Conditions | Yield |
---|---|
In water aq. solns. of starting materials are mixed, stirring at room temp. for 15 min; filtn. under vac., washing several times with distilled H2O and EtOH, vac. drying, recrystn. from hot benzene, elem. anal.; | 98% |
azelaic acid
lead(II) acetate trihydrate
lead(II) azelate
Conditions | Yield |
---|---|
In water High Pressure; placed in a bomb, heated to 220°C (3 h), held for 3 h; cooled to room temp. (3 h), crysts., washed (water), air dried; elem. anal.; | 96% |
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
In ethanol; water addn. of aq. Pb(OAc)2 to 2 equiv. ligand (in EtOH) at 45°C, stirring overnight; collection (filtration), washing (water), recrystn. (aq. EtOH), drying in air; elem. anal.; | 96% |
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
In ethanol; water byproducts: H(1+); addn. of warm (50°C) aq. soln. of PbOAc to warm soln. of phenylpyrazolone in EtOH (stirring), stirring (45°C, a few minutes; pptn.); filtration, washing (water), recrystn.(aq. EtOH), air drying; elem. anal.; | 96% |
lead(II) acetate trihydrate
3,5-di(t-butyl)benzene-1,2-dithiolate
{Pb(3,5-di(t-butyl)benzene-1,2-dithiolate)(2-)}
Conditions | Yield |
---|---|
With NaOCH3 In methanol byproducts: CH3COO(1-); under N2, t-bu-S2-H2 in MeOH and NaOMe in MeOH added to Pb(CH3COO)2 in MeOH at 25°C; filtered after 2 h, washed (MeOH), dried in vacuo for 12 h; elem. anal.,NMR, mass spectroscopy; | 95% |
Conditions | Yield |
---|---|
With NaB(C6H5)4 In methanol; N,N-dimethyl-formamide N,N'-propane-1,3-diylbis(3-formyl-5-methylsalicylideneiminato)copper(II) and lead(II) acetate in hot dmf, stirring at 25°C 10 min., then with butane-1,4-diamine in methanol at 25°C for 30 min; washed with methanol and ether, dried in air, elem. anal.; | 95% |
lead(II) acetate trihydrate
1,5-naphthyridine-4,8-diol
Pb(2+)*C8H4N2O2(2-) = Pb(C8H4N2O2)
Conditions | Yield |
---|---|
With sodium carbonate In water organic compound dissolved in warm water by addn. of Na2CO3, soln. added to aq. soln. of Pb(CH3COO)2*3H2O; precipitate collected after several hours, washed with water, dried over P2O5 in vacuo at room temp., ground to powder, elem. anal.; | 95% |
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
In ethanol; water ppt. boiling iu aq. EtOH, air-drying; elem. anal.; | 95% |
α-mercapto-β-(2-furyl) acrylic acid
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
In ethanol; water for 1h; | 95% |
3-(4-methoxyphenyl)-2-sulfanylpropenoic acid
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
In ethanol; water | 95% |
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
In methanol; chloroform at 25℃; for 1.5h; | 95% |
1,6-bis(5-hydroxy-1-phenyl-3-methyl-1H-pyrazol-4-yl)hexane-1,6-dione
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
In ethanol; water ppt. boiling iu aq. EtOH, air-drying; elem. anal.; | 94% |
Conditions | Yield |
---|---|
With sodium hydroxide In water at 140℃; for 0.0833333h; | 94% |
Conditions | Yield |
---|---|
In water aq. soln. of Pb salt added to warm aq. mixt. of org. compds.; volume reduced, crystd. at room temp., filtered, dried in air, elem. anal.; | 93% |
N,N'-bis-(2-mercaptoethyl)isophthalamide
lead(II) acetate trihydrate
C6H4(CONHCH2CH2S)2Pb
Conditions | Yield |
---|---|
In ethanol; water aq. soln. Pb(OAc)2*3H2O was added to soln. ligand in EtOH; ppt. was filtered and dried in vacuo; elem. anal.; | 93% |
Conditions | Yield |
---|---|
In ethanol; water High Pressure; (N2); Pb(OAc)2*3H2O was dissolved in H2O-EtOH (3:2), PbO was added, resulting slurry was sonicated for 20 min, heated in vessel at 120°C for 12 h, cooled to room temp.; supernatant was removed, dried in vac. without heating in Abderhalden drying pistol for 12 h; | 93% |
In water High Pressure; (N2); Pb(OAc)2*3H2O was dissolved in H2O, PbO was added, resulting slurry was sonicated for 20 min, heated in vessel at 120°C for 12 h, cooled to room temp.; supernatant was removed, dried in vac. without heating in Abderhalden drying pistol for 12 h, elem. anal.; | 41% |
lead(II) acetate trihydrate
3-ethyl-1-methyl-1H-imidazol-3-ium bromide
1-ethyl-3-methylimidazolium acetate
Conditions | Yield |
---|---|
In water at 35℃; for 48h; Inert atmosphere; | 93% |
In methanol; water | |
In methanol; water |
(4-fluorophenyl)-2-mercaptoacrylic acid
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
In ethanol; water for 3h; | 93% |
2-Hydroxymethylpyridine
lead(II) acetate trihydrate
saccharin
[Pb(saccharine)2(2-pyridylmethanol)]
Conditions | Yield |
---|---|
In water aq. soln. of Pb salt added to warm aq. mixt. of org. compds.; volume reduced, crystd. at room temp., filtered, dried in air, elem. anal.; | 92% |
lead(II) acetate trihydrate
1,2-bis(2-mercaptophenylthio)ethane
{Pb(1,2-bis(2-mercaptophenylthio)ethane)(2-)}
Conditions | Yield |
---|---|
With NaOCH3 In methanol under N2, NaOMe in MeOH and S4-H2 in MeOH added to Pb(CH3COO)2 in MeOH, stirred for several h at 25°C; filtered, washed (CH3OH), dried in vacuo for 12 h; elem. anal., NMR, mass spectroscopy; | 91% |
1,8,15,22-tetrakis(pentan-3'-yloxy)phthalocyanine
lead(II) acetate trihydrate
[1,8,15,22-tetrakis(3-pentyloxy)phthalocyaninate]Pb(II)
Conditions | Yield |
---|---|
In pentan-1-ol mixt. of Pb compd. and ligand in n-pentanol was heated at 140°C for 8 h under N2; solvent removed (vac.); chromd. (silica gel, CHCl3); recrystd. (CHCl3/MeOH); elem. anal.; | 91% |
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
In ethanol; water byproducts: H(1+); addn. of warm (50°C) aq. soln. of PbOAc to warm soln. of phenylpyrazolone in EtOH (stirring), stirring (45°C, a few minutes; pptn.); filtration, washing (water), recrystn.(aq. EtOH), air drying; elem. anal.; | 91% |
benzene-1,4-dithiol
lead(II) acetate trihydrate
1,5-diamino-3-azapentane
[Pb(1,4-benzenedithiolato)(diethylenetriamine)]n
Conditions | Yield |
---|---|
In further solvent(s) (N2); heating a suspn. of metal salt and dithiol in diethylenetriamine to 130°C for 16 h, cooling to room temp.; filtration, washing ppt. with methanol, Et2O; elem. anal.; | 91% |
2',2'',2''',2'''-(benzene-1,2,4,5-tetrayl)tetrakis(1,1,3,3-tetramethylguanidine)
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
In ethanol at 20℃; for 2h; Inert atmosphere; Schlenk technique; | 91% |
1,10-Phenanthroline
p-Coumaric Acid
lead(II) acetate trihydrate
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) grinding of Pb(CH3COO)2*3H2O, trans-4-hydroxycinnamic acid in solid state at room temp.; dissolving in DMF soln.; filtration, evapn. at room temp.; elem. anal.; | 90% |
lead(II) acetate trihydrate
[5,10,15,20-tetrakis-triisopropylsilylethynylporphyrinato]lead(II)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide mixed, refluxed for 2 h; crystd.(water), filtered, washed (water, CH3OH), recrystd.(DCM-CH3OH), elem. anal., XRD, IR, UV, MAS; | 90% |
diselenodipropionic acid dimethyl ester
lead(II) acetate trihydrate
Conditions | Yield |
---|---|
With NaBH4 In methanol MeOH soln. of NaBH4 (1.27 mmol) added to MeOH soln. of ligand (0.57 mmol), stirred for 5 min, MeOH soln. of Pb compd. (0.56 mmol) added with stirring at room temp. under N2, mixt. stirred for 3 h; evapd., washed (cold hexane), extd. (CH2Cl2), filtered, evapd. (vac.), recrystd. (CH2Cl2/hexane), elem. anal.; | 90% |
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