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Leshan Kairuida Photoelectric Technology Co., Ltd.

High purity lead (Pb) Purity: 4N (99.99%), 5N (99.999%), 6N (99.9999% CAS number: 7439-92-1 Physical properties: External brightness, silver white Appearance:Metal filiform,External brightness, silver white Storage:Store at +5°C to +30°C. Packa

lead

Cas:7439-92-1

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Lead Manufacturer/High quality/Best price/In stock

Cas:7439-92-1

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Lead

Cas:7439-92-1

Min.Order:1

Negotiable

Type:Other

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Lead (all forms)

Cas:7439-92-1

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei yanxi chemical co.,LTD.

Chengdu words and import and export co., LTD is one specialized is engaged in pharmaceutical intermediates, fine chemical industry in the field of research. Development and production of high-tech enterprises. Appearance:Colorless, volatile liquid

Lead

Cas:7439-92-1

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

inquiry

Chongqing Changfeng Chemical Co., Ltd.

1. good quality 2. high purity 3. competitive price 4. best service Application:used for reagent analysis, industry,etc. Port:By sea, air and courier

Lead

Cas:7439-92-1

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

LeadCAS7439-92-1

Cas:7439-92-1

Min.Order:1 Kilogram

FOB Price: $20.0 / 30.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Lead 7439-92-1

Cas:7439-92-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

Lead Ingot :7439-92-1 and Pb

Cas:7439-92-1

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

Lead CAS:7439-92-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates, stero

Lead CAS:7439-92-1

Cas:7439-92-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Lead

Cas:7439-92-1

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:7439-92-1

Cas:7439-92-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Lonwin Chemical Group Limited

Lead CAS: 7439-92-1 Specification Test Item Standard: USP Identification IR spectrum similar to that of RS HPLC retention time similar to that of RS Related substance

Factory supply Lead

Cas:7439-92-1

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Lead CAS.7439-92-1

Cas:7439-92-1

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Lead

Cas:7439-92-1

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Lead, 99.999%

Cas:7439-92-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

Lead

Cas:7439-92-1

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Lead Manufacturer

Cas:7439-92-1

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:grey powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediates Tra

Lead

Cas:7439-92-1

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Lead Manufacturer/High quality/Best price/In stock

Cas:7439-92-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Best OfferLead

Cas:7439-92-1

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

Lead Basic information Product Name: Lead Synonyms: Lead rod, 5mm (0.2 in.) dia.;Lead wire, 2.0mm (0.08 in.) dia.;Lead in Isooctane standards;c.i.77575;c.i.pigmentmetal4;ci77575;PB STANDARD;Electrolytically refined lead (trace elements) CAS:

Lead

Cas:7439-92-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Lead CAS.7439-92-1

Cas:7439-92-1

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Henan Kanbei Chemical Co.,LTD

High quality, competitive price, fast delivery and first-class service we possesses have won the trust and praise of customers. Standard: BP/USP/EP The purity is equal or greater than 99%. As a supplier, we can provide high-quality products. Cle

High purity Lead nanopowder

Cas:7439-92-1

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Lead CAS.7439-92-1

Cas:7439-92-1

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Lead CAS.7439-92-1

Cas:7439-92-1

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

Product Name: Lead Synonyms: C.I. 77575;C.I. Pigment metal 4;c.i.77575;c.i.pigmentmetal4;ci77575;cipigmentmetal4;elementallead;Glover CAS: 7439-92-1 MF: Pb MW: 207.2 EINECS: 231-100-4 Product Categories: Metals;Inorganics;LeadMicro/Nanoelec

TAINFUCHEM: Lead

Cas:7439-92-1

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

Lead

Cas:7439-92-1

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Lead CAS.7439-92-1

Cas:7439-92-1

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

Lead

Cas:7439-92-1

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

lead dioxide

lead dioxide

Conditions
ConditionsYield
With H2 In water Electrolysis; electrolysis of PbO2 in acidic or alkaline suspension;; pptn.;;100%
With hydrogen sulfide In neat (no solvent) passing H2S over dry or moist PbO2;; by Pb blue coloured flame of H2S;;
With aluminium In neat (no solvent) byproducts: Al2O3; explosive mixture;;
1,2-dimethoxyethanebis(pentadeuterocyclopentadienyl)ytterbium(II)

1,2-dimethoxyethanebis(pentadeuterocyclopentadienyl)ytterbium(II)

lead(II) chloride

lead(II) chloride

A

lead
7439-92-1

lead

B

chlorobis(cyclopentadienyl)ytterbium(III)-tetrahydrofuran(2:1)

chlorobis(cyclopentadienyl)ytterbium(III)-tetrahydrofuran(2:1)

Conditions
ConditionsYield
In tetrahydrofuran N2-atmosphere; stirring Yb-complex with 0.5 equiv. of halide (room temp., 16 h); filtration, washing (THF), evapn. (vac.), drying (vac.);A 100%
B 80%
lead(II) sulfate

lead(II) sulfate

galenite

galenite

lead oxide

lead oxide

lead(II) chloride

lead(II) chloride

Conditions
ConditionsYield
With sodium carbonate; potassium carbonate; pyrographite In melt melting of 1:1 mixt. of the two carbonates in a BeO crucible, addn. of Pb compd., addn. of wood coal, heating at 1020+/-2 K for 2 h; air cooling;99%
With sodium carbonate; potassium carbonate In melt melting of 1:1 mixt. of the two carbonates in a BeO crucible, addn. of Pb compd., heating at 1020+/-2 K for 2 h; air cooling;95%
galenite

galenite

lead oxide

lead oxide

lead(II) chloride

lead(II) chloride

Conditions
ConditionsYield
With sodium carbonate; potassium carbonate; pyrographite In melt melting of 1:1 mixt. of the two carbonates in a BeO crucible, addn. of Pb compd.,addn. of wood coal, heating at 1020+/-2 K for 2 h; air cooling;99%
With sodium carbonate; potassium carbonate In melt melting of 1:1 mixt. of the two carbonates in a BeO crucible, addn. of Pb compd., heating at 1020+/-2 K for 2 h; air cooling;90%
lead(II) sulfide

lead(II) sulfide

Conditions
ConditionsYield
With hydrogen In neat (no solvent) at 440 - 600°C; complete reduction at 600 °C;;99%
With H2 In neat (no solvent) at 440 - 600°C; complete reduction at 600 °C;;99%
With manganese In neat (no solvent)94%
lead oxide

lead oxide

Conditions
ConditionsYield
With sodium carbonate; potassium carbonate; pyrographite In melt melting of 1:1 mixt. of the two carbonates in a BeO crucible, addn. of Pb compd., addn. of wood coal, heating at 1020+/-2 K for 2 h; air cooling;99%
lead(II) chloride

lead(II) chloride

Conditions
ConditionsYield
With sodium carbonate; potassium carbonate; pyrographite In melt melting of 1:1 mixt. of the two carbonates in a BeO crucible, addn. of Pb compd., addn. of wood coal, heating at 1020+/-2 K for 2 h; air cooling;99%
With hydrogen In neat (no solvent) byproducts: HCl;
With aluminium In water reduction;;
tetrachlorosilane
10026-04-7, 53609-55-5

tetrachlorosilane

Pb(C6H3(N(CH3)2)2)2
1037195-18-8

Pb(C6H3(N(CH3)2)2)2

Conditions
ConditionsYield
In diethyl ether SiCl4 added to soln. of Sn(CH(SiMe3)2)2 in Et2O;99%
2,4,6-tris[bis(trimethylsilyl)methyl]phenylplumbylene
190316-75-7

2,4,6-tris[bis(trimethylsilyl)methyl]phenylplumbylene

Conditions
ConditionsYield
In benzene-d6 Ar-atmosphere; heating (100°C, 42 h);99%
lithiumferrocene
1271-15-4

lithiumferrocene

lead(II) chloride

lead(II) chloride

A

lead
7439-92-1

lead

B

ferrocene
102-54-5

ferrocene

Conditions
ConditionsYield
In diethyl ether byproducts: LiCl; Ar; to a suspn. of PbCl2 added a suspn. of FcLi, stirred for 2 h; ppt. (Pb) filtered, washed (H2O), dried, analyzed; Fc not isolated, detected by NMR;A 96%
B n/a
galenite

galenite

Conditions
ConditionsYield
With sodium carbonate; potassium carbonate; pyrographite In melt melting of 1:1 mixt. of the two carbonates in a BeO crucible, addn. of Pb compd., addn. of wood coal, heating at 1020+/-2 K for 2 h; air cooling;95%
With sodium carbonate; potassium carbonate In melt melting of 1:1 mixt. of the two carbonates in a BeO crucible, addn. of Pb compd., heating at 1020+/-2 K for 2 h; air cooling;85%
Pb9(4-)

Pb9(4-)

Conditions
ConditionsYield
With KI In ammonia NH3 (liquid); Electrochem. Process; electrochem. reoxidn. at 1.254 V (vs. solvated electron potential);95%
Tetramethylblei-(IV)
75-74-1

Tetramethylblei-(IV)

A

lead
7439-92-1

lead

B

ethane
74-84-0

ethane

Conditions
ConditionsYield
In gas byproducts: methane, ethylene, propane; Irradiation (UV/VIS); chain react. of decompn. of PbMe4, 22°C, 5 Torr, 10 l reaction cell, irradn. with several laser types (ArF, KrF, CO2, YAG) for investigation of laser wavelength dependence; organic products detected by gas chromy.;A n/a
B 85%
In gaseous matrix byproducts: methane, ethylene, propane; Irradiation (UV/VIS); chain react. of decompn. of TML, 22°C, 5 Torr, addn. of <7 Torr of Ar, N2 or air, 10 l reaction cell, irradn. with several laser types (ArF, KrF, CO2, YAG) for investigation of laser wavelength dependence; organic products detected by gas chromy.;
lead(II) sulfate

lead(II) sulfate

Conditions
ConditionsYield
With sodium carbonate; potassium carbonate; pyrographite In melt melting of 1:1 mixt. of the two carbonates in a BeO crucible, addn. of Pb compd., addn. of wood coal, heating at 1020+/-2 K for 2 h; air cooling;80%
With iron; pyrographite In neat (no solvent) PbSO4 is reduced to Pb with Fe in the presence of C;;
With sodium amide In neat (no solvent) reduction to PbS; further calcination leads to formation of Pb-metal;;
tetrahydrofuran
109-99-9

tetrahydrofuran

1,3-di-tert-butyl-2,2-dimethyl-1,2-3,4λ2-diazasilaplumbetidine
84806-16-6

1,3-di-tert-butyl-2,2-dimethyl-1,2-3,4λ2-diazasilaplumbetidine

bis(tert-butoxy aluminium dihydride)

bis(tert-butoxy aluminium dihydride)

A

lead
7439-92-1

lead

B

(CH3)2Si(NC(CH3)3)2Al(OC(CH3)3)(C4H8O)
875924-40-6

(CH3)2Si(NC(CH3)3)2Al(OC(CH3)3)(C4H8O)

Conditions
ConditionsYield
In tetrahydrofuran byproducts: H2; Pb complex in THF added dropwise to a stirred soln. of Al complex in dryTHF, reacted at room temp. for 24 h; concd., recrystd.(THF) at 4°C, elem. anal.;A n/a
B 57%
diethyl ether
60-29-7

diethyl ether

lead(II) bis(trimethylsilyl)amide
55147-59-6, 65455-92-7

lead(II) bis(trimethylsilyl)amide

HOC6H3-2,6-(C6H3-2,6-(i-Pr)2)2

HOC6H3-2,6-(C6H3-2,6-(i-Pr)2)2

A

lead
7439-92-1

lead

B

Pb(OC6H3-2,6-(C6H3-2,6-Pri2)2)2*0.5(diethyl ether)

Pb(OC6H3-2,6-(C6H3-2,6-Pri2)2)2*0.5(diethyl ether)

Conditions
ConditionsYield
at 0 - 20℃; for 9.33h; Inert atmosphere; Darkness;A n/a
B 56%
lead(II) oxide

lead(II) oxide

magnesium
7439-95-4

magnesium

A

lead
7439-92-1

lead

B

magnesium oxide

magnesium oxide

Conditions
ConditionsYield
In solid byproducts: Mg2Pb; in a vibration mill; yield of lead depends on duration of mechanical treatment; XRD; size distribution of powder particles; electron microscope; DTA;A 50%
B n/a
In solid mechanical treatment in a vibratory mill under N2 or Ar or vac.; XRD;
(η5-C5H5)W(CO)3PbMe3
79110-54-6

(η5-C5H5)W(CO)3PbMe3

A

lead
7439-92-1

lead

B

tricarbonyl(cyclopentadienyl)methyltungsten(II)

tricarbonyl(cyclopentadienyl)methyltungsten(II)

C

Tetramethylblei-(IV)
75-74-1

Tetramethylblei-(IV)

Conditions
ConditionsYield
In hexane refluxed for 100 h; solvent was removed under vac., yellow solid was purified by sublimation;A n/a
B 16%
C n/a
(η5-C5H5)Mo(CO)3PbMe3
12093-28-6

(η5-C5H5)Mo(CO)3PbMe3

A

lead
7439-92-1

lead

B

methyl-tricarbonyl(η-cyclopentadienyl)molybdenum

methyl-tricarbonyl(η-cyclopentadienyl)molybdenum

C

Tetramethylblei-(IV)
75-74-1

Tetramethylblei-(IV)

Conditions
ConditionsYield
In hexane refluxed for 100 h; solvent was removed under vac., purified by sublimation;A n/a
B 15%
C n/a
manganese(IV) oxide
1313-13-9

manganese(IV) oxide

antimony(III) trioxide

antimony(III) trioxide

lead(II) oxide

lead(II) oxide

lead dioxide

lead dioxide

A

lead
7439-92-1

lead

B

lead(II) antimonate

lead(II) antimonate

C

Pb5Sb2MnO11

Pb5Sb2MnO11

Conditions
ConditionsYield
In neat (no solvent, solid phase) by a solid-state react. from the 4PbO2+PbO+MnO2+Sb2O3 mixt. in an evacuated sealed silica tube; annealing at 650°C for 50 h; subsequent annealing for 50 h after regrinding; detd. by powder XRD;A 1%
B n/a
C n/a
lead(II) azide

lead(II) azide

A

lead
7439-92-1

lead

B

nitrogen
7727-37-9

nitrogen

Conditions
ConditionsYield
In neat (no solvent) Kinetics;
In neat (no solvent) Kinetics; Irradiation (UV/VIS); photolysis with light at 380 nm; monitored by mass spectrophotometry and spectrophotometry;
With cadmium In neat (no solvent) Kinetics; Irradiation (UV/VIS); PbN6 mixed with Cd in EtOH in air, pressed into tablet, or Cd deposited onto surface of PbN6 tablet; irradiated with 380-nm light; monitored by UV-vis spectra;
lead(II) azide

lead(II) azide

Conditions
ConditionsYield
Kinetics; byproducts: N2; other Radiation; X-ray irradiation for different time, at 78 and 300 K; detected by changes in optical density;
In solid byproducts: N2; Irradiation (UV/VIS); PbN6 was photolyzed in vac.;
In neat (no solvent) other Radiation; radiation with electrons;;
Kinetics; byproducts: N2; Irradiation (UV/VIS); irradiation for different times, cooling from 300 to 78 K;
In neat (no solvent) Irradiation (UV/VIS); laser puls irradiation (1064 nm, 20 mJ); not isolated; chemiluminescence spectroscopy;
chloride
16887-00-6

chloride

iodine
7553-56-2

iodine

hydrogen cation

hydrogen cation

lead(II) chloride

lead(II) chloride

A

hydrogenchloride
7647-01-0

hydrogenchloride

B

lead
7439-92-1

lead

C

Iodine monochloride
7790-99-0

Iodine monochloride

Conditions
ConditionsYield
In diethyl ether; water Electrochem. Process;
lead(II) sulfide

lead(II) sulfide

water
7732-18-5

water

A

lead
7439-92-1

lead

B

lead(II) oxide

lead(II) oxide

Conditions
ConditionsYield
In neat (no solvent) byproducts: H2, SO2; under exclusion of air at light red heat;;
lead(II) sulfide

lead(II) sulfide

water
7732-18-5

water

Conditions
ConditionsYield
In neat (no solvent) byproducts: S;
In neat (no solvent) byproducts: S;
water
7732-18-5

water

lead(II) chloride

lead(II) chloride

A

lead
7439-92-1

lead

B

hydrogen
1333-74-0

hydrogen

C

hydrogen cation

hydrogen cation

Conditions
ConditionsYield
With calcium silicon alloy In water byproducts: Ca(2+), Si(IV); redn. of (10.0-30.0)-matom*dm**-3 soln. of Pb(2+) at initial pH of 4.0 with Ca-Si alloy by procedure reported in S. Tokunaga, Bull. Chem. Soc. Jpn., 57, 2832 (1984);
lead(II) oxide

lead(II) oxide

triethylstannane
997-50-2

triethylstannane

A

lead
7439-92-1

lead

B

water
7732-18-5

water

C

hydrogen
1333-74-0

hydrogen

D

hexaethyldistannoxane
1112-63-6

hexaethyldistannoxane

Conditions
ConditionsYield
boiling to reflux at 146°C; 30min;;
boiling to reflux at 146°C; 30min;;
lead

lead

(2S,3R)-1-tert-Butoxycarbonyl-3-(3-hydroxypropyn-1-yl)-2-phenylpiperidin-3-ol
200956-10-1

(2S,3R)-1-tert-Butoxycarbonyl-3-(3-hydroxypropyn-1-yl)-2-phenylpiperidin-3-ol

Z-(2S,3R)-1-tert-butoxycarbonyl-3-(3-hydroxyprop-1-en-1-yl)-2-phenylpiperidin-3-ol
200956-75-8

Z-(2S,3R)-1-tert-butoxycarbonyl-3-(3-hydroxyprop-1-en-1-yl)-2-phenylpiperidin-3-ol

(2S,3R)-1-tert-butoxycarbonyl-3-(3-hydroxypropyn-1yl)-2-phenylpiperidin-3-ol

(2S,3R)-1-tert-butoxycarbonyl-3-(3-hydroxypropyn-1yl)-2-phenylpiperidin-3-ol

Z-(2S,3R)-1-tert-butoxycarbonyl-3-(3-hydroxyprop-1-en-1-yl)-2-phenylpiperidin-3-ol
200956-75-8

Z-(2S,3R)-1-tert-butoxycarbonyl-3-(3-hydroxyprop-1-en-1-yl)-2-phenylpiperidin-3-ol

Conditions
ConditionsYield
In ethyl acetate100%
In ethyl acetate100%
caesium
7440-46-2

caesium

4Cs(1+)*Pb9(4-)=Cs4Pb9

4Cs(1+)*Pb9(4-)=Cs4Pb9

Conditions
ConditionsYield
In neat (no solvent) stoich. amts., 650°C, 2 d; cooling to room temp. at 4°C/h;100%
With Hg In neat (no solvent) molar ratio Cs:Pb:Hg=4:8.5:12, 650°C, 12 h; cooling to room temp.at 5°C/h;
tricarbonylcyclopentadienylmolybdenum(II) chloride
12128-23-3

tricarbonylcyclopentadienylmolybdenum(II) chloride

A

cyclopentadienylmolybdenum tricarbonyl dimer

cyclopentadienylmolybdenum tricarbonyl dimer

B

lead(II) chloride

lead(II) chloride

Conditions
ConditionsYield
In dimethyl sulfoxide Pb was reacted with Mo-complex in DMSO;A 99%
B n/a
In N,N-dimethyl-formamide Pb was reacted with Mo-complex in DMF;A 99%
B n/a
sulfur
7704-34-9

sulfur

lead(II) sulfide

lead(II) sulfide

Conditions
ConditionsYield
In ammonia (safety screen); pressure tube (room temp., 12 h);99%
In solid equimolar amts. of elements ground for 60 min; detected by XRD analysis;
In melt mixt. of Pb and S sealed in quartz ampoules (pressure 1E-6 Torr); ampoules heated to 800°, maintained at this temp. for 10 h with rocking; ampoules cooled to room temp.; XRD;
selenium
7782-49-2

selenium

lead(II) selenide

lead(II) selenide

Conditions
ConditionsYield
In ammonia (safety screen); pressure tube (room temp., 12 h);99%
With sodium hydroxide In water stoich. amt. of Se and Pb were mixed in a steel autoclave, 1 M aq. NaOH and 50 %, heating at 100-160 °C for 18-72 h without stirring or shaking; cooling to room temp., ppt. was collected, washed with distd. water, dried in vac. at 60 °C for 4 h;50%
In neat (no solvent) mixt. of high purity elements Pb and Se melted for 8 h in quartz tube under vac.; annealed at 300°C for 4 wk;
tricarbonylcyclopentadienyltungsten(II) chloride
12128-24-4

tricarbonylcyclopentadienyltungsten(II) chloride

A

bis(tricarbonyl(η-cyclopentadienyl)tungsten)

bis(tricarbonyl(η-cyclopentadienyl)tungsten)

B

lead(II) chloride

lead(II) chloride

Conditions
ConditionsYield
In dimethyl sulfoxide Pb was reacted with W-complex in DMSO;A 99%
B n/a
In N,N-dimethyl-formamide Pb was reacted with W-complex in DMF;A 99%
B n/a
benzene-1,2-diol
120-80-9

benzene-1,2-diol

pyrocatechol; lead (II)-pyrocatecholate
138711-52-1

pyrocatechol; lead (II)-pyrocatecholate

Conditions
ConditionsYield
In acetonitrile Electrolysis; 3.0 h, 40 mA; elem. anal.;98%
antimony
7440-36-0

antimony

lithium sulfide

lithium sulfide

sulfur
7704-34-9

sulfur

LiPbSb3S6

LiPbSb3S6

Conditions
ConditionsYield
at 800℃; for 6h; Glovebox;98%
3,5-di-tert-butyl-1,2-benzoquinone
34105-76-5

3,5-di-tert-butyl-1,2-benzoquinone

Pb(3,6-di-tert-butylcatecholato)
948860-60-4

Pb(3,6-di-tert-butylcatecholato)

Conditions
ConditionsYield
In tetrahydrofuran (vac.); addn. with stirring of soln. of quinone deriv. in THF to lead; decantation, addn. of toluene or hexane, separating precipitate, elem. anal.;96%
indium
7440-74-6

indium

potassium
7440-09-7

potassium

K5InPb8

K5InPb8

Conditions
ConditionsYield
In neat (no solvent) (N2 or He); reacted at 900°C within a welded Ta container, annealed at 350°C for 3 wk;95%
zirconium
7440-67-7

zirconium

A

Zr5Pb3

Zr5Pb3

B

Zr5Pb4

Zr5Pb4

Conditions
ConditionsYield
In melt heating at 700°C in sealed Ta tubes, 7d;A 5%
B 95%
In melt heating at 800°C in sealed Ta tubes, 7d;A 60%
B 40%
1,10-Phenanthroline
66-71-7

1,10-Phenanthroline

2,3-naphthalenediol
92-44-4

2,3-naphthalenediol

Pb(C10H6O2)(1,10-phenanthroline)
617690-48-9

Pb(C10H6O2)(1,10-phenanthroline)

Conditions
ConditionsYield
In acetonitrile Electrolysis; 2.5 h, 40 mA; elem. anal.;95%
water
7732-18-5

water

2,6-diacetylpyridine bis(salicyloylhydrazone)
76115-25-8

2,6-diacetylpyridine bis(salicyloylhydrazone)

acetonitrile
75-05-8

acetonitrile

A

Pb(2,6-bis(1-salicyloylhydrazonoethyl)pyridine(-2H))(H2O)2

Pb(2,6-bis(1-salicyloylhydrazonoethyl)pyridine(-2H))(H2O)2

B

[Et4N][Pb(2,6-bis(1-salicyloylhydrazonoethyl)pyridine(-2H))(CN)]

[Et4N][Pb(2,6-bis(1-salicyloylhydrazonoethyl)pyridine(-2H))(CN)]

Conditions
ConditionsYield
With tetraethylammonium perchlorate In acetonitrile Electrolysis; suspn. of ligand in MeCN contg. Et4NClO4 electrolysed for 24 h, Pb plateas anode, 10 mA current; filtered; solid washed with Et2O; dried under vac. (Pb-2H2O complex); crystd. by concn. of mother liquor (Pb-CN complex); elem. anal.;A 95%
B n/a
phosphorus

phosphorus

PbP7

PbP7

Conditions
ConditionsYield
at 399.84℃; for 144h; Sealed tube;95%
phosphorus

phosphorus

silver
7440-22-4

silver

sulfur
7704-34-9

sulfur

7Ag(1+)*Pb(2+)*3PS4(3-)

7Ag(1+)*Pb(2+)*3PS4(3-)

Conditions
ConditionsYield
Stage #1: lead; phosphorus; silver; sulfur at 250℃; under 0.0001 Torr; for 24h; Sealed tube;
Stage #2: at 250 - 600℃; for 96h; Sealed tube;
95%
selenium
7782-49-2

selenium

lead(II) bromide

lead(II) bromide

Pb3Se2Br2

Pb3Se2Br2

Conditions
ConditionsYield
at 700℃; under 30003000 Torr; for 3h;95%
Tetrabromocatechol
488-47-1

Tetrabromocatechol

Pb(2+)*C6Br4O2(2-)=Pb(C6Br4O2)
618093-11-1

Pb(2+)*C6Br4O2(2-)=Pb(C6Br4O2)

Conditions
ConditionsYield
In acetonitrile Electrolysis; 3.0 h, 40 mA; elem. anal.;94%
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