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Cas:6125-24-2
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Min.Order:1 Gram
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Cas:6125-24-2
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inquiryMelting point 56-58℃ Boiling point 250℃ density 1.122 g/cm3 (25℃) refractive index 1.5270 (589.3 nm 20℃) pka
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Min.Order:10 Gram
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryR & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
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Benzene,(2-nitroethyl)- cas 6125-24-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiry6125-24-2 Application:intermediate
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl
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Min.Order:10 Milligram
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inquiryHenan Sunlake Enterprise Corporation Our Advantages 1, Any inquiry about ch
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Best quality & Attractive price & Professional service; Trial & Pilot & CommercialHenan Fine Chemicals Co., LTD. is a diversified technology - oriented integrated company, which mainly concentrates on fine chemicals. Our company is committed to becom
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United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
Conditions | Yield |
---|---|
With polymer-bound NADH (2a) | 100% |
With magnesium(II) perchlorate; "grafted NADH model" reagent In acetonitrile; benzene at 80℃; for 120h; | 100% |
With tri(1-naphthyl)phosphonium tris(pentafluorophenyl)borohydride In dichloromethane-d2 for 12h; Reagent/catalyst; Glovebox; Sealed tube; | 100% |
Conditions | Yield |
---|---|
With magnesium(II) perchlorate; model of NADH grafted on silica matrix In acetonitrile at 65℃; for 120h; | 100% |
With sodium tetrahydroborate; silica gel In chloroform; isopropyl alcohol at 0 - 23℃; for 1.33333h; Inert atmosphere; | 99% |
With hydrogen; tris(triphenylphosphine)rhodium(l) chloride In benzene at 50℃; under 2585.81 Torr; for 14h; | 98% |
nitrostyrene
5-carbamoyl thieno<2,3-b>pyridine
bromo-8 octyl dimethylchlorosilane
2-Phenylnitroethane
Conditions | Yield |
---|---|
With magnesium(II) perchlorate; silice (Merck Kieselgel Art.:7734) Product distribution; multistep reaction; 1.) grafting on a silica matrix, reflux, in toluene, 12 h, 2.) reflux, toluene, 5 days. 3.) acetonitrile, 65 deg C, 5 days; reagent quqntity, reaction time varied; | 100% |
2-nitro-1-phenylethan-1-ol
2-Phenylnitroethane
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride In water at 80℃; for 0.166667h; Microwave irradiation; Green chemistry; | 96% |
(i) Ac2O, H2SO4, (ii) NaBH4, DMSO; Multistep reaction; | |
Multi-step reaction with 3 steps 1: pyridine / 2 h / Ambient temperature 2: sodium carbonate / benzene / 5 h / Heating 3: 84 percent / 3,5-bis(ethoxycarbonyl)-2,6-dimethyl-1,4-dihydropyridine, silica gel / benzene / 0.5 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: hydrogenchloride / water 2: sodium tetrahydroborate; silica gel / chloroform; isopropyl alcohol View Scheme |
Conditions | Yield |
---|---|
With benzaldehyde | 95% |
With benzaldehyde | 95% |
nitrostyrene
A
1,3-dinitro-2,4-diphenyl-butane
B
2-Phenylnitroethane
Conditions | Yield |
---|---|
With methanol; sodium tetrahydroborate In water at 25℃; for 1h; | A 1.92 %Spectr. B 92.7% |
C14H23NO2Si
2-Phenylnitroethane
Conditions | Yield |
---|---|
With sodium cyanide; magnesium(II) perchlorate In dichloromethane; N,N-dimethyl-formamide at 20℃; for 2h; | 72% |
<2-nitro-2-(phenylsulfonyl)ethyl>-benzene
2-Phenylnitroethane
Conditions | Yield |
---|---|
With 1-Benzyl-1,4-dihydronicotinamide In benzene for 42h; Irradiation; | 62% |
With sodium dithionite; potassium carbonate; 1,1′-dioctyl-4,4′-bipyridinium In dichloromethane; water at 35℃; for 3h; | 62% |
With sodium dithionite; potassium carbonate; 1,1′-dioctyl-4,4′-bipyridinium In dichloromethane; water at 35℃; for 3h; other α-nitro sulfones; other reaction conditions; also without viologen; | 62% |
2-phenethyl iodide
2-Phenylnitroethane
Conditions | Yield |
---|---|
With silver(I) nitrite In water at 60℃; for 1.5h; Darkness; | 60% |
With silver(I) nitrite; diethyl ether |
nitromethane
N-benzyl-2,4,6-triphenylpyridinium tetrafluoroborate
A
2-Phenylnitroethane
B
2,4,6-triphenylpyridine
Conditions | Yield |
---|---|
With sodium hydride In methanol; dimethyl sulfoxide at 25℃; for 2h; | A 58% B n/a |
sodium nitromethane
N-benzyl-2,4,6-triphenylpyridinium tetrafluoroborate
A
2-Phenylnitroethane
B
2,4,6-triphenylpyridine
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 25℃; for 2h; Rate constant; Mechanism; | A 58% B n/a |
Conditions | Yield |
---|---|
With 1,3-bis-(diphenylphosphino)propane; caesium carbonate; bis(1,5-cyclooctadiene)diiridium(I) dichloride In toluene at 150℃; for 72h; | 54% |
2-nitroacetophenone
A
2-Phenylnitroethane
B
2-nitro-1-phenylethan-1-ol
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In hydrogenchloride; ethanol at 50℃; under 760 Torr; | A 37% B 14% |
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In chloroform for 3h; Heating; | 30% |
With 3-chloro-benzenecarboperoxoic acid In 1,2-dichloro-ethane Heating; | |
With 3-chloro-benzenecarboperoxoic acid |
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride; 3-chloro-benzenecarboperoxoic acid 1.) methylene chloride; Multistep reaction; | A 10% B n/a |
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride; ozone 1.) methylene chloride; Multistep reaction; | A 10% B n/a |
(2-nitroethenyl)benzene
A
1,3-dinitro-2,4-diphenyl-butane
B
2-Phenylnitroethane
Conditions | Yield |
---|---|
With sodium tetrahydroborate; ethanol | |
With tetrahydrofuran; diethyl ether; Trimethyl borate; sodium | |
With sodium hydroxide; sodium tetrahydroborate In ethanol at 0 - 5℃; for 2h; | |
With sodium hydroxide; sodium tetrahydroborate In water; acetonitrile at 0 - 5℃; for 2h; |
nitromethane
N-benzyl-2,4,6-triphenylpyridinium tetrafluoroborate
2-Phenylnitroethane
Conditions | Yield |
---|---|
(i) NaOEt, EtOH, (ii) /BRN= 4225599/, DMSO; Multistep reaction; |
1-benzyl-2,4,6-triphenylpyridinium cation
nitromethane anion
A
2-Phenylnitroethane
B
2,4,6-triphenylpyridine
Conditions | Yield |
---|---|
In pentan-1-ol at 25℃; also in DMSO; | |
In pentan-1-ol at 25℃; Kinetics; Rate constant; Mechanism; also in DMSO; |
Conditions | Yield |
---|---|
With 1-Benzyl-1,4-dihydronicotinamide In acetonitrile at 80℃; Yield given; |
acetic anhydride
A
2-Phenylnitroethane
B
anhydride N-acetyl phenyl-acetohydroxamique-acetique
Conditions | Yield |
---|---|
In diethyl ether for 65h; | A 13 % Spectr. B 82 % Spectr. |
Conditions | Yield |
---|---|
With samarium diiodide; water; isopropylamine In tetrahydrofuran | 99% |
With trichlorosilane; N-ethyl-N,N-diisopropylamine In acetonitrile at 0 - 20℃; for 18h; Inert atmosphere; | 98% |
With poly(p-aminostyrene)-palladium(II); hydrogen In N,N-dimethyl-formamide at 70℃; under 760 Torr; for 6h; | 91% |
2-fluoro-ethane-1,1-diol
2-Phenylnitroethane
1-Fluoro-2-hydroxy-3-nitro-4-phenylbutane
Conditions | Yield |
---|---|
potassium carbonate at 50℃; for 6h; | 95% |
2,2-difluoro-ethane-1,1-diol
2-Phenylnitroethane
1,1-Difluoro-3-nitro-4-phenyl-butan-2-ol
Conditions | Yield |
---|---|
potassium carbonate at 50℃; for 6h; | 95% |
2,2,2-trifluoro-1,1-ethanediol
2-Phenylnitroethane
3-nitro-4-phenyl-1,1,1-trifluorobutan-2-ol
Conditions | Yield |
---|---|
potassium carbonate at 50℃; for 6h; | 95% |
Conditions | Yield |
---|---|
With acetic acid; sodium nitrite In dimethyl sulfoxide at 35℃; for 6h; | 95% |
With acetic acid; sodium nitrite In water; dimethyl sulfoxide at 65℃; | 75% |
With (S)-1-phenyl-ethylamine; sodium nitrite; isopentyl nitrite In N,N-dimethyl-formamide for 48h; |
2-Phenylnitroethane
N-benzylidenediphenylphosphinamide
Conditions | Yield |
---|---|
N,N,N',N'-tetramethylguanidine at 20℃; for 26h; aza-Henry reaction; | 95% |
2-Phenylnitroethane
benzaldehyde N-boc imine
Conditions | Yield |
---|---|
With N-((1R,2R)-2-(3-((1R,2R)-2-(dimethylamino)cyclohexyl)thioureido)-1,2-diphenylethyl)-3,5-bis(trifluoromethyl)benzenesulfonamide In acetonitrile at -20℃; Mannich reaction; Molecular sieve; | 95% |
Conditions | Yield |
---|---|
With triethylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid In tetrahydrofuran at -30 - 50℃; for 2h; Product distribution; different dehydration reagents, solvents, reaction temperatures, times; | 91% |
With triethylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid In tetrahydrofuran at -30 - 50℃; for 2h; | 91% |
With acetic acid; sodium nitrite In dimethyl sulfoxide at 35℃; | 72% |
crotonic acid methyl ester
2-Phenylnitroethane
methyl b-methyl-g-nitrobenzenepentanoate
Conditions | Yield |
---|---|
With Aliquat 336; potassium carbonate Ambient temperature; Irradiation; | 91% |
2-Phenylnitroethane
N-[(4-methylbenzene-1-sulfonyl)(phenyl)methyl]formamide
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 0.75h; aza-Henry reaction; | 90% |
2-Phenylnitroethane
4-methoxy-benzaldehyde
1-methoxy-4-(2-nitro-3-phenyl-1-propenyl)benzene
Conditions | Yield |
---|---|
With N-butylamine In toluene for 12h; Henry reaction; Reflux; | 90% |
2-hydrazinyl-4-methylquinoline
2-Phenylnitroethane
Conditions | Yield |
---|---|
Stage #1: 2-Phenylnitroethane With polyphosphoric acid at 130℃; Stage #2: 2-hydrazinyl-4-methylquinoline at 130℃; | 90% |
2-Phenylnitroethane
1-fluoro-1-nitro-2-phenylethane
Conditions | Yield |
---|---|
Stage #1: 2-Phenylnitroethane With tetra(n-butyl)ammonium hydroxide In acetonitrile at 25℃; Stage #2: With Selectfluor In water; acetonitrile | 89% |
Stage #1: 2-Phenylnitroethane With potassium hydroxide In water; acetonitrile at -15 - -5℃; Stage #2: With Selectfluor In dichloromethane; water; acetonitrile at -15 - 10℃; Further stages.; | 83% |
Stage #1: 2-Phenylnitroethane With potassium hydroxide In water; acetonitrile at 0℃; for 1h; Stage #2: With Selectfluor In dichloromethane; water; acetonitrile at -17 - 10℃; for 0.166667h; | 80% |
2-Phenylnitroethane
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 0.75h; aza-Henry reaction; | 89% |
(2-nitroethenyl)benzene
2-Phenylnitroethane
((2R,3R)-1,3-dinitrobutane-1,3-diyl)dibenzene
Conditions | Yield |
---|---|
With N-((1R,2R)-2-(3-((1R,2R)-2-(dimethylamino)cyclohexyl)thioureido)-1,2-diphenylethyl)-3,5-bis(trifluoromethyl)benzenesulfonamide In dichloromethane at -30℃; Michael condensation; optical yield given as %ee; enantioselective reaction; | 89% |
Conditions | Yield |
---|---|
With potassium fluoride; N,N-dimethylammonium chloride In toluene at 110℃; for 12h; | 89% |
2-Phenylnitroethane
(2S)-N,N-dibenzylphenylalaninal
(S)-2-Dibenzylamino-4-nitro-1,5-diphenyl-pentan-3-ol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 0℃; for 0.333333h; Henry reaction; | 87% |
Conditions | Yield |
---|---|
With cetyltrimethylammonium hydroxide at 20℃; for 3h; Henry reaction; | 86% |
2-Phenylnitroethane
benzaldehyde
(2-nitroprop-1-ene-1,3-diyl)dibenzene
Conditions | Yield |
---|---|
With N-butylamine In toluene for 9.5h; Reflux; | 85% |
With ammonium acetate In acetic acid | |
With methylamine hydrochloride; potassium acetate; trimethyl orthoformate In methanol for 16h; Heating; | |
With hydrogenchloride; potassium fluoride; dimethyl amine In water; toluene for 24h; Reflux; Dean-Stark; |
methyl crotonate
2-Phenylnitroethane
methyl b-methyl-g-nitrobenzenepentanoate
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile for 22h; Ambient temperature; | 85% |
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