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inquiryProduct Name: Manganese(II) Acetate Tetrahydrate CAS No.: 6156-78-1 Specification: Analysis pure, Chemical pure Molecular Formula: Mn (CH3COO) 2.4H2O Properties: Light red crystal.With a relative density of 1.59 and a melting point of 80
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inquiryProduct name: Manganese Acetate Tetrahydrate CAS No.:6156-78-1 Molecule Formula:C4H14MnO8 Molecule Weight:245.09 Purity: 99.0% Package: 25kg/drum Description:White or almost white powder Manufacture Standards:Enterprise Standard
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inquiryConditions | Yield |
---|---|
With manganese(IV) oxide; alkali cetate at 80℃; | |
With manganese(IV) oxide; alkaline earth acetate at 80℃; |
Conditions | Yield |
---|---|
In ethanol xanthene-compound was added to Mn(CH3CO2)2*4H2O in abs. ethanol, the soln. was refluxed in air for 2 h, cooled, aq. satd. NaCl was added, the mixt. was stirred for 10 min; extd. with CH2Cl2, the organic layer was washed with water, dried over MgSO4, the solid was rotary evapd.; elem. anal.; | 100% |
manganese (II) acetate tetrahydrate
Mn[5-[2-chloro-6-[(18-crown-6)methyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin](1+)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide stirring under reflux (4 h); solvent evapn. (vac.), dissolving in CH2Cl2, washing (water), chromy. (silica gel, CHCl3/EtOH), dissolving in CH2Cl2, stirring with NaCl soln., org. phase drying (MgSO4), solvent evapn.; | 100% |
manganese (II) acetate tetrahydrate
Mn[5-[2-chloro-6-[9-(18-crown-6)nonyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin](1+)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide stirring under reflux (4 h); solvent evapn. (vac.), dissolving in CH2Cl2, washing (water), chromy. (silica gel, CHCl3/EtOH), dissolving in CH2Cl2, stirring with NaCl soln., org. phase drying (MgSO4), solvent evapn.; | 100% |
manganese (II) acetate tetrahydrate
Mn[5-[2,6-dichloro-3-[9-(18-crown-6)nonyloxy]phenyl]-10,15,20-tri-(2,6-dichlorophenyl) porphyrin](1+)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide stirring under reflux (4 h); solvent evapn. (vac.), dissolving in CH2Cl2, washing (water), chromy. (silica gel, CHCl3/EtOH), dissolving in CH2Cl2, stirring with NaCl soln., org. phase drying (MgSO4), solvent evapn.; | 100% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide stirring under reflux (4 h); solvent evapn. (vac.), dissolving in CH2Cl2, washing (water), chromy. (silica gel, CHCl3/EtOH), dissolving in CH2Cl2, stirring with NaCl soln., org. phase drying (MgSO4), solvent evapn.; | 100% |
water
manganese (II) acetate tetrahydrate
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide soln. of K4(Re6Se8(CN)6)*3.5H2O (0.08 mmol) in H2O/DMF added to soln. ofMn(CH3COO)2*4H2O (0.18 mmol) in H2O/DMF under stirring, mixt. refluxed for 1 h, cooled; ppt. filtered off, washed twice with H2O/DMF and CH3CN, air-dried; elem.anal.; | 100% |
water
manganese (II) acetate tetrahydrate
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water mixt. of H2O/DMF (75/1) added dropwise to aq. soln. of K4(Re6S8(CN)6) (0.029 mmol) and Mn(CH3COO)2*4H2O (0.068 mmol) under stirring; soln. concd., stored in air for a week, crystals filtered off, washed twice (CH3CN), air-dried; elem. anal.; | 100% |
water
manganese (II) acetate tetrahydrate
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide soln. of Cs4(Re6Te8(CN)6) (0.08 mmol) in H2O/DMF slowly added to soln. of Mn(CH3COO)2*4H2O (0.18 mmol) in H2O/DMF under stirring, mixt. refluxedfor 1 h, cooled; ppt. filtered off, washed with H2O/DMF and CH3CN, air-dried; elem. anal.; | 100% |
manganese (II) acetate tetrahydrate
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide soln. of K4(Re6Se8(CN)6)*3.5H2O in H2O/DMF added to soln. of Mn(CH3COO)2*4H2O in H2O/DMF with vigorous stirring, mixt. stirred for 2 h; ppt. filtered off, washed twice with H2O/DMF (1/1) and CH3CN, air-dried;elem. anal.; | 100% |
manganese (II) acetate tetrahydrate
bis(tetrabutylammonium)oxalate
Conditions | Yield |
---|---|
In water; dimethyl sulfoxide at 20℃; for 730.5h; | 100% |
Conditions | Yield |
---|---|
In water at 500℃; Green chemistry; | 100% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide stirred for 10 min; filtered, washed with DMF, acetone and diethyl ether, dried in vac.; elem. anal.; | 99% |
manganese (II) acetate tetrahydrate
meso-tetrakis(pentafluorophenyl)-β-octachloroporphyrinatomanganese(III) azide
Conditions | Yield |
---|---|
In methanol; acetone (N2); soln. stiring (room temp., 12 h); filtration, solvent removal (rotary evapn.), solid redissolving (CH2Cl2), washing (water), org. layer drying (Na2SO4), solvent removal (rotary evapn.), drying (vac., overnight, room temp.); | 99% |
manganese (II) acetate tetrahydrate
Conditions | Yield |
---|---|
In methanol; acetone byproducts: H2O; inert atmosphere; dropwise addn. of metal acetate (in MeOH) to 0.5 equiv. Mn-complex (in Me2CO), stirring for 1 h; solvent removal (vac.), dissoln. in THF/CH2Cl2=10:1, pptn. on Et2O addn., standing overnight; | 99% |
manganese (II) acetate tetrahydrate
Conditions | Yield |
---|---|
In acetonitrile evacuated sealed ampoule (150°C, 6 weeks); elem. anal.; | 99% |
In acetonitrile High Pressure; Mn(CH3COO)2*4H2O dehydrated in acetonitrile at 150°C for 6 weeks; | 99% |
manganese (II) acetate tetrahydrate
5-{2-(OOC-methoxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide a soln. of porphyrin-compd. in DMF is stirred at reflux with Mn(OAc)2*4H2O for 6 h; evapn. under reduced pressure, the residue is dissolved in in CH2Cl2 and washed with water, evapn., the residue is dissolved in EtOH and NaOH and refluxed for 2 h, evapn., addn. of H2O and HCl, extn. with CH2Cl2, column chromy., dried over MgSO4; | 99% |
Conditions | Yield |
---|---|
With air In methanol Mn compd. added to soln. of ligand (molar ratio 2:1) in MeOH; stirred for 30 min at 50°C; brine added; stirred for 30 min at 50°C; solvent evapd. in vac.; dissolved in CH2Cl2; washed with brine and H2O; org. phase dried over Na2SO4; evapd. in vac.; | 99% |
Conditions | Yield |
---|---|
With air In methanol Mn compd. added to soln. of ligand (molar ratio 2:1) in MeOH; stirred for 30 min at 50°C; brine added; stirred for 30 min at 50°C; solvent evapd. in vac.; dissolved in CH2Cl2; washed with brine and H2O; org. phase dried over Na2SO4; evapd. in vac.; | 99% |
Conditions | Yield |
---|---|
With air In methanol Mn compd. added to soln. of ligand (molar ratio 2:1) in MeOH; stirred for 30 min at 50°C; brine added; stirred for 30 min at 50°C; solvent evapd. in vac.; dissolved in CH2Cl2; washed with brine and H2O; org. phase dried over Na2SO4; evapd. in vac.; | 99% |
pyridine
manganese (II) acetate tetrahydrate
1,3-bis-(3-oxo-3-phenyl-propionyl)-2-hydroxy-5-methylbenzene
Conditions | Yield |
---|---|
In pyridine to a stirred soln. of Mn-salt in pyridine was added a soln. of tetraketone in pyridine, stirred for a few min (inert atm.); diethyl ether was added, the flask was stopped and left undisturbed for 2 days, crystals were filtered, dried in vac.; elem. anal.; | 99% |
manganese (II) acetate tetrahydrate
Conditions | Yield |
---|---|
In ethanol refluxing; | 99% |
manganese (II) acetate tetrahydrate
Conditions | Yield |
---|---|
In ethanol refluxing; | 99% |
Conditions | Yield |
---|---|
In water; glycerol Re complex in H2O layered on top of Mn salt and ethylenediamine in glycerol, crystd. for 2 weeks; filtered, dried, elem. anal.; | 99% |
Conditions | Yield |
---|---|
In ethanol xanthene-compound was added to Mn(CH3CO2)2*4H2O in abs. ethanol, the soln. was refluxed in air for 2 h, cooled, aq. satd. NaCl was added, the mixt. was stirred for 10 min; extd. with CH2Cl2, the organic layer was washed with water, dried over MgSO4, the solid was rotary evapd.; elem. anal.; | 99% |
Conditions | Yield |
---|---|
In ethanol High Pressure; heated at 80°C for 3 h; | 99% |
titanium(IV) isopropylate
dichloromethane
manganese (II) acetate tetrahydrate
Conditions | Yield |
---|---|
Stage #1: C92H72N2O6; manganese (II) acetate tetrahydrate With air In ethanol for 0.5h; Reflux; Stage #2: lithium chloride In ethanol for 0.5h; Reflux; Stage #3: titanium(IV) isopropylate; dichloromethane Further stages; | 99% |
manganese (II) acetate tetrahydrate
(R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediamine
sodium chloride
(-)-chloro((1R,2R)-4,4',6,6'-tetra-tert-butyl-2,2'-[cyclohexane-1,2-diylbis(nitrilomethylidyne)]diphenolato)manganese(III)
Conditions | Yield |
---|---|
Stage #1: manganese (II) acetate tetrahydrate; (R,R)-N,N'-bis(3,5-di-tert-butylsalicylidene)-1,2-cyclohexanediamine In ethanol; toluene for 2.75h; Reflux; Stage #2: With air In ethanol; toluene for 1h; Reflux; Stage #3: sodium chloride In ethanol; water; toluene | 99% |
Conditions | Yield |
---|---|
Stage #1: C92H74N2O5; manganese (II) acetate tetrahydrate In ethanol for 1h; Schlenk technique; Reflux; Stage #2: lithium chloride In ethanol for 1h; Schlenk technique; Reflux; Stage #3: titanium(IV) isopropylate In ethanol at 20℃; for 12h; Schlenk technique; | 99% |
manganese (II) acetate tetrahydrate
5-{2-(7-OOC-heptyloxy)-6-chlorophenyl}-10,15,20-tris(2,6-dichlorophenyl)porphyrin Mn(III)
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide a soln. of porphyrin-compd. in DMF is stirred at reflux with Mn(OAc)2*4H2O for 6 h; evapn. under reduced pressure, the residue is dissolved in in CH2Cl2 and washed with water, evapn., the residue is dissolved in EtOH and NaOH and refluxed for 2 h, evapn., addn. of H2O and HCl, extn. with CH2Cl2, column chromy., dried over MgSO4; | 98% |
Conditions | Yield |
---|---|
In ethanol xanthene-compound was added to Mn(CH3CO2)2*4H2O in abs. ethanol, the soln. was refluxed in air for 2 h, cooled, aq. satd. NaCl was added, the mixt. was stirred for 10 min; extd. with CH2Cl2, the organic layer was washed with water, dried over MgSO4, the solid was rotary evapd.; elem. anal.; | 98% |
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